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Mechanical testing of micropillars is a field that involves new physics, as the behaviour of materials is non-deterministic at this scale. To better understand their deformation mechanisms we applied 3-dimensional high angular resolution…

The dislocation microstructure developing during plastic deformation strongly influences the stress-strain properties of crystalline materials. The novel method of high resolution electron backscatter diffraction (HR-EBSD) offers a new…

Understanding the local fracture resistance of microstructural features. such as brittle inclusions, coatings, and interfaces at the microscale under complex loading conditions is critical for microstructure-informed design of materials. In…

Metals are important structural materials for transport and the built environment. Low carbon steels can fail through strain localisation due to the role of interstitial solute atoms (such as carbon and nitrogen) interacting with mobile…

材料科学 · 物理学 2019-01-24 James L R Hickey , S Rouland , T B Britton

Analysis of distortions of the crystal lattice within individual mineral grains is central to the investigation of microscale processes that control and record tectonic events. These distortions are generally combinations of lattice…

材料科学 · 物理学 2019-06-04 David Wallis , Lars N. Hansen , T. Ben Britton , Angus J. Wilkinson

In this work hydrogen diffusion towards the fracture process zone is examined accounting for local hardening due to geometrically necessary dislocations (GNDs) by means of strain gradient plasticity (SGP). Finite element computations are…

High angular resolution electron backscatter diffraction (HR-EBSD) affords an increase in angular resolution, as compared to 'conventional' Hough transform based EBSD, of two orders of magnitude, enabling measurements of relative…

仪器与探测器 · 物理学 2017-10-03 T Ben Britton , James L R Hickey

Dislocation patterning and self-organization during plastic deformation are associated with work hardening, but the exact mechanisms remain elusive. This is partly because studies of the structure and local strain during the initial stages…

Zircaloy-4 is used extensively as nuclear fuel cladding materials and hydride embrittlement is a major failure mechanism. To explore the effect of {\delta}-hydride on plastic deformation and performance of Zircaloy-4, in situ high angular…

We carry out strain-controlled in-situ compression experiments of micron-sized tungsten (W) micropillars in the temperature range 300-900 K, together with simulations of three-dimensional discrete dislocation dynamics (DDD) at the same…

材料科学 · 物理学 2026-02-26 Yang Li , Inam Lalani , Matthew Maron , William Hixson , Biao Wang , Nasr Ghoniem , Giacomo Po

Precise and accurate determination of crystallographic orientation is crucial for engineering van der Waals heterostructures, where the twist angle between layers controls emergent electronic and optical properties. While Electron…

材料科学 · 物理学 2026-03-11 R. Bangari , M. Mosayebi , J. Buchner , J. D. Caldwell , N. Bassim , T. G. Folland

For high (angular) resolution electron backscatter diffraction (HR-EBSD), the selection of a reference diffraction pattern (EBSP0) significantly affects the precision of the calculated strain and rotation maps. This effect was demonstrated…

材料科学 · 物理学 2023-02-21 Abdalrhaman Koko , Vivian Tong , Angus J. Wilkinson , T. James Marrow

The use of Nye's dislocation tensor for calculating the density of geometrically necessary dislocations (GND) is widely adopted in the study of plastically deformed materials. The curl operation involved in finding the Nye tensor, while…

材料科学 · 物理学 2019-06-10 Suchandrima Das , Felix Hofmann , Edmund Tarleton

With decreasing system sizes, the mechanical properties and dominant deformation mechanisms of metals change. For larger scales, bulk behavior is observed that is characterized by a preservation and significant increase of dislocation…

材料科学 · 物理学 2021-12-21 Kolja Zoller , Szilvia Kalácska , Péter Dusán Ispánovity , Katrin Schulz

Plastic inhomogeneity, particularly localised strain, is one of the main mechanisms responsible for failures in engineering alloys. This work studied the spatial arrangement and distribution of microstructure and their influence in the…

材料科学 · 物理学 2023-03-21 Jalal Al-Lami , Thibaut Dessolier , Talha Pirzada , Minh-Son Pham

We study the mechanisms of slip transfer at a grain boundary, in titanium, using Differential Aperture X-ray Laue Micro-diffraction (DAXM). This 3D characterization tool enables measurement of the full (9-component) Nye lattice curvature…

Understanding the evolution of dislocation structures during plastic deformation is critical for predicting the mechanical performance of metallic materials. In this work, we applied in situ scanning electron microscopy/electron backscatter…

材料科学 · 物理学 2026-03-24 Mikhail Lebyodkin , Maxim Gussev , Jamieson Brechtl , Tatiana Lebedkina

The microstructural mechanisms governing energy storage during plastic deformation of twinning-induced plasticity (TWIP) steels remain insufficiently understood, particularly under conditions of strain localization. This study provides a…

材料科学 · 物理学 2026-03-10 Sandra Musiał , Michał Maj , Marcin Nowak

(Abriged) In the framework of the Herschel GTKP "The earliest phases of star formation", we have imaged B68 between 100 and 500 um. Ancillary (sub)mm data, spectral line maps of the 12/13CO(2-1) transitions as well as a NIR extinction map…

The plastic deformation mechanisms of tungsten carbide at room and elevated temperatures influence the wear and fracture properties of WC-Co hardmetal composite materials. The relationship between residual defect structures, including…

材料科学 · 物理学 2021-11-05 Vivian Tong , Helen Jones , Ken Mingard
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