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A LiFeAs single crystal with $T_c^{onset}$$\sim$19.7 K was grown successfully in a sealed tungsten crucible using the Bridgeman method. The electrical resistivity experiments revealed a ratio of room temperature to residual resistivity…

We successfully grew the high-quality single crystals of $A_{x}$Fe$_2$Se$_2$ ($A$ = K and Cs) by self-flux method. Sharp superconducting transition was observed for both types of crystals. The crystals show the onset superconducting…

超导电性 · 物理学 2011-07-07 J. J. Ying , X. F. Wang , X. G. Luo , A. F. Wang , M. Zhang , Y. J. Yan , Z. J. Xiang , R. H. Liu , P. Cheng , G. J. Ye , X. H. Chen

Single crystals of LiFeAs were successfully grown by a self-flux method using the cubic anvil high-pressure and high-temperature technique. The reaction took place in a closed boron nitride crucible at a pressure of 1 GPa and a temperature…

超导电性 · 物理学 2024-11-05 N. D. Zhigadlo

Superconducting single crystals of SmFeAsO$_{1-x}$ without fluorine doping were grown at a pressure of 3.3 GPa and a temperature of 1350-1450 $^\circ$C by using the self-flux method. Plate-like single crystals of a few-150 $\mu$m in their…

We measured resistivity and specific heat of high-quality CsFe$_2$As$_2$ single crystals, which were grown by using a self-flux method. The CsFe$_2$As$_2$ crystal shows sharp superconducting transition at 1.8 K with the transition width of…

超导电性 · 物理学 2013-06-17 A. F. Wang , B. Y. Pan , X. G. Luo , F. Chen , Y. J. Yan , J. J. Ying , G. J. Ye , P. Cheng , X. C. Hong , S. Y. Li , X. H. Chen

Single crystals of SmFeAsO1-xFy of a size up to 120 micrometers have been grown from NaCl/KCl flux at a pressure of 30 kbar and temperature of 1350-1450 C using the cubic anvil high-pressure technique. The superconducting transition…

超导电性 · 物理学 2009-11-13 N. D. Zhigadlo , S. Katrych , Z. Bukowski , S. Weyeneth , R. Puzniak , J. Karpinski

F-doped LaOBiSe$_{2}$ superconducting single crystals with typical size of 2$\times$4$\times$0.2 mm$^{3}$ are successfully grown by flux method and the superconducting properties are studied. Both the superconducting transition temperature…

超导电性 · 物理学 2014-08-12 Jifeng Shao , Zhongheng Liu , Xiong Yao , Lei Zhang , Li Pi , Shun Tan , Changjin Zhang , Yuheng Zhang

Sizable single crystals of $BaFe_2As_2$ have been grown with self-flux method. The crystals are plate-like with c-axis perpendicular to the plane. The size can be as large as 3 x 5 x 0.2 $mm^3$. The resistivity anisotropy…

超导电性 · 物理学 2009-11-13 X. F. Wang , T. Wu , G. Wu , H. Chen , Y. L. Xie , J. J. Ying , Y. J. Yan , R. H. Liu , X. H. Chen

Single crystals of the LnFeAsO (Ln1111, Ln = Pr, Nd, and Sm) family with lateral dimensions up to 1 mm were grown from NaAs and KAs flux at high pressure. The crystals are of good structural quality and become superconducting when O is…

Single crystals of the compound LaFePO were prepared using a flux growth technique at high temperatures. Electrical resistivity measurements reveal metallic behavior and a resistive transition to the superconducting state at a critical…

超导电性 · 物理学 2008-09-10 J. J. Hamlin , R. E. Baumbach , D. A. Zocco , T. A. Sayles , M. B. Maple

We successfully grew the high-quality single crystal of Rb$_{0.78}$Fe$_2$Se$_{1.78}$, which shows sharp superconducting transition in magnetic susceptibility and electrical resistivity. Resistivity measurements show the onset…

Single crystals of BaFe$_2$As$_2$ and (Ba$_{0.55}$K$_{0.45}$)Fe$_2$As$_2$ have been grown out of excess Sn with 1% or less incorporation of solvent. The crystals are exceptionally micaceous, are easily exfoliated and can have dimensions as…

Superconductivity was discovered in a Ni0:05TaS2 single crystal. A Ni0:05TaS2 single crystal was successfully grown via the NaCl/KCl flux method. The obtained lattice constant c of Ni0:05TaS2 is 1.1999 nm, which is significantly smaller…

超导电性 · 物理学 2015-05-13 X. D. Zhu , Y. P. Sun , S. B. Zhang , H. C. Lei , X. B. Zhu , Lijun Li , Z. R. Yang , W. H. Song , J. M. Dai

In this paper we present the single crystal growth of Fe0.95Se0.6Te0.4 high TC superconducting sample by the modified Bridgman technique. The x-ray diffraction pattern shows the single crystal nature of the sample, as only (00l) peaks are…

超导电性 · 物理学 2019-07-23 Anmol Shukla , Vishal K. Maurya , Rajendra S. Dhaka

Single crystals of A$_{1-x}$K$_x$Fe$_2$As$_2$ (A=Ba, Sr) with high quality have been grown successfully by FeAs self-flux method. The samples have sizes up to 4 mm with flat and shiny surfaces. The X-ray diffraction patterns suggest that…

超导电性 · 物理学 2009-11-13 Huiqian Luo , Zhaosheng Wang , Huan Yang , Peng Cheng , Xiyu Zhu , Hai-Hu Wen

We report successful growth of flux free large single crystals of superconducting FeSe1/2Te1/2 with typical dimensions of up to few cm. The AC and DC magnetic measurements revealed the superconducting transition temperature (Tc) value of…

超导电性 · 物理学 2015-09-08 Rajveer Jha , P. K. Maheshwari , Bhasker Gahtori , V. P. S. Awana

High-quality and sizable single crystals are crucial for studying the intrinsic properties of unconventional superconductors, which are lacking in the 1111 phase of the Fe-based superconductors. Here we report the successful growth of…

超导电性 · 物理学 2015-07-03 Yonghui Ma , Hui Zhang , Bo Gao , Kangkang Hu , Qiucheng Ji , Gang Mu , Fuqiang Huang , Xiaoming Xie

A review of our investigations on single crystals of LnFeAsO1-xFx (Ln=La, Pr, Nd, Sm, Gd) and Ba1-xRbxFe2As2 is presented. A high pressure technique has been applied for the growth of LnFeAsO1-xFx crystals, while Ba1-xRbxFe2As2 crystals…

Single crystals of Tl0.58Rb0.42Fe1.72Se2 are successfully grown with the superconducting transition temperatures Tconset=32K and Tczero=31.4K. The Hall coefficient exhibits a multi-band behavior, which is very similar to that of all other…

超导电性 · 物理学 2011-02-21 Hangdong Wang , Chihen Dong , Zujuan Li , Shasha Zhu , Qianhui Mao , Chunmu Feng , H. Q. Yuan , Minghu Fang

We report single-crystal growth of La$_{0.34}$Na$_{0.66}$Fe$_2$As$_2$ iron-based superconductor with the size of several millimeters. The samples were accidentally obtained in trying to grow LaFeAsO$_{1-y}$F$_y$ ( $y \geq$ 0.8 ) single…

超导电性 · 物理学 2018-11-14 Yanhong Gu , Jia-Ou Wang , Xiaoyan Ma , Huiqian Luo , Youguo Shi , Shiliang Li
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