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The proneness of water to crystallize is a major obstacle to understanding its putative exotic behavior in the supercooled state. It also represents a strong practical limitation to cryopreservation of biological systems. Adding some…

The vitrification of aqueous solutions through rapid cooling is a remarkable achievement that launched the field of cryo-electron microscopy (cryo-EM) and has enabled the cryopreservation of biological specimens. For judging the feasibility…

化学物理 · 物理学 2024-07-02 Nathan J. Mowry , Constantin R. Kruger , Marcel Drabbels , Ulrich J. Lorenz

Vitrification is a promising approach for ice-free cryopreservation of biological material, but progress is hindered by the limited set of experimental tools for studying processes in the interior of the vitrified matter. Isochoric…

医学物理 · 物理学 2023-10-03 Jason T. Parker , Anthony N. Consiglio , Boris Rubinsky , Simo A. Mäkiharju

A central question concerning glass-formation has been what governs the kinetic arrest of the quenched liquid - cooling reduces the thermal energy which molecules need to surmount local potential barriers, while the accompanying volume…

软凝聚态物质 · 物理学 2007-05-23 CM Roland R Casalini

Because of the negative inclination of the solid-liquid phase separation line in water, ice Ih melts on compression. On further increase in pressure the liquid water transforms into a high density metastable glassy state, characterized by a…

软凝聚态物质 · 物理学 2021-04-22 Saumyak Mukherjee , Biman Bagchi

Recent experiments and theoretical studies strongly indicate that water exhibits a liquid-liquid phase transition (LLPT) in the supercooled domain. An open question is how the LLPT of water can affect the properties of aqueous solutions.…

Methanol-water liquid mixtures have been investigated by high-energy synchrotron X-ray and neutron diffraction at low temperatures. We are thus able to report the first complete sets of both X-ray and neutron weighted total scattering…

Many of the anomalous properties of water are amplified in the deeply supercooled region. Here we present neutron scattering measurements of the density of heavy water confined in a nanoporous silica matrix MCM-41-S (\approx15 {\AA} pore…

We study a coarse-grained model for a water monolayer that cannot crystallize due to the presence of confining interfaces, such as protein powders or inorganic surfaces. Using both Monte Carlo simulations and mean field calculations, we…

统计力学 · 物理学 2012-08-20 Marco G. Mazza , Kevin Stokely , H. Eugene Stanley , Giancarlo Franzese

The freezing of water is one of the major causes of mechanical damage in materials during wintertime; surprisingly this happens even in situations where water only partially saturates the material so that the ice has room to grow. Here we…

软凝聚态物质 · 物理学 2024-11-12 Menno Demmenie , Paul Kolpakov , Boaz van Casteren , Dirk Bakker , Daniel Bonn , Noushine Shahidzadeh

Vapor pressures were measured for the system chloroform/polyethylene oxide (peo, weight average molar mass = 1000 kg/mol) at 25 degrees centigrade as a function of the weight fraction w of the polymer by means of a combination of head space…

软凝聚态物质 · 物理学 2007-05-23 A. KHassanova , B. A. Wolf

The impact of the Corona, dielectric barrier discharge and low pressure radiofrequency air plasmas on the wettability of the medical grade polyvinylchloride was investigated. Corona plasma treatment exerted the most pronounced increase in…

The liquid-vapor critical behavior of water is strongly influenced by both ionic solutes and confinement. Molecular dynamics simulations of aqueous NaCl solutions using the TIP4P/2005 water model and the Madrid-2019 ion parameters reveal a…

化学物理 · 物理学 2026-04-02 Mayank Sharma , Peter Virnau

Differential thermal analysis has been conducted for the Al-Cu-Co alloys with the composition range of 15 at.% Co and 10 to 30 at.% Cu, and 25 at.% Co and 2.5 to 20 at.% Co. The features of the formation of solid phases have been studied…

材料科学 · 物理学 2022-12-08 Larisa V. Kamaeva , Elena N. Tsiok , Nikolay M. Chtchelkatchev

The fundamental understanding of water confined in porous coordination polymers (PCPs) is significantly important not only for their applications such as gas storage and separation, but also for exploring the confinement effects in the…

Molecular Dynamics simulations are performed on two sodium chloride solutions in TIP4P water with concentrations c=1.36 mol/kg and c=2.10 mol/kg upon supercooling. The isotherms and isochoresplanes are calculated. The temperature of maximum…

软凝聚态物质 · 物理学 2009-04-22 D. Corradini , P. Gallo , M. Rovere

Glass transition and relaxation of the glycerol-water binary mixture system are studied over the glycerol concentration range of 5 - 85 mol% using the highly sensitive technique of spin probe ESR. For the water rich mixture the glass…

软凝聚态物质 · 物理学 2015-05-13 Debamalya Banerjee , S. V. Bhat

Water vitrifies if cooled at rates above $3 \cdot 10^5$ K/s. Surprisingly, this process cannot simply be reversed by heating the resulting amorphous ice at a similar rate. Instead, we have recently shown that the sample transiently…

化学物理 · 物理学 2024-02-01 Constantin R. Krüger , Nathan J. Mowry , Marcel Drabbels , Ulrich J. Lorenz

Water can be vitrified if it is cooled at rates exceeding $3*10^5$ K/s. This makes it possible to outrun crystallization in so-called no man's land, a range of deeply supercooled temperatures where water crystallizes rapidly. One would…

Vitrification during cryopreservation requires a detailed understanding of the dynamic behavior of biological solutions. We investigate ferritin diffusion in glycerol-water mixtures at supercooled temperatures using X-ray Photon Correlation…

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