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In the present study, low-temperature synthesis of (Cu Fe)Al2O4 and (Cu Cr Fe)Al2O4 spinels from the quasicrystalline phases was investigated with the variation of process parameters during milling and annealing. The milling of the…

材料科学 · 物理学 2008-06-17 T. P. Yadav , N. K. Mukhopadhyay , R. S. Tiwari , O. N. Srivastava

Mechanical alloying (MA) has been used to fabricate the Co2FeAl Heusler alloy with a nanocrystalline structure. The formation mechanism of the alloy has been investigated. Rietveld analysis showed that all samples that were milled for more…

材料科学 · 物理学 2015-06-04 M. Hakimi , P. Kameli , H. Salamati , Y. Mazaheri

In the present investigation the pure elemental powder mixture of Al (70 at%) Ni (15 at %), Cu (15 at %) was mechanically milled in an attritor ball mill for 10, 20, 40, 60, 80 and 100 hours in hexane medium at 400 rpm. The isothermal…

材料科学 · 物理学 2007-05-23 T. P. Yadav , N. K. Mukhopadhyay , R. S. Tiwari , O. N. Srivastava

A complex study of aging kinetics for both coarse-grained and nanostructured by severe plastic deformation Cu -- 2 wt% Be alloy is reported. It is shown that aging of a coarse-grained alloy leads to continuous formation of nanosized CuBe…

材料科学 · 物理学 2020-05-12 Ivan Lomakin , Miguel Castillo-Rodríguez , Xavier Sauvage

Polyhedral nanocrystals of <alpha>-Fe2O3 are successfully synthesized by annealing FeCl3 on silicon substrate at 1000 oC in the presence of H2 gas diluted with argon (Ar). Uniformly shaped polyhedral nanoparticles (diameter ~50-100 nm) are…

材料科学 · 物理学 2011-11-22 Rajesh Kumar , S. Gautam , In-Chul Hwang , K. H. Chae , Nagesh Thakur

Metal powders with hierarchical nanostructures are always designed and fabricated by dealloying with or without combination of other manufacturing processes. However, they are mainly nanoporous metal powder and its derivations, and their…

应用物理 · 物理学 2019-09-17 Li Chenguang , Zhang Mingwei , Ruan Mianmian , Wang Jun , Liang Jiamiao , Zhang Deliang

The (Co,Ni)Al2O4 is an aluminum transition metals oxide which falls into the category of aluminate spinels. The synthesis of nano-crystalline spinels has been investigated extensively due to their potential applications such as a…

材料科学 · 物理学 2007-05-23 T. P. Yadav , N. K. Mukhopadhyay , R. S. Tiwari , O. N. Srivastava

The aging of a nanocrystalline equiatomic ZnSe alloy produced by mechanical alloying was investigated using X-ray diffraction (XRD) and differential scanning calorimetry (DSC) techniques. The measured XRD patterns showed that Se atoms…

材料科学 · 物理学 2009-11-07 K. D. Machado , J. C. de Lima , T. A. Grandi , C. E. M. de Campos , A. A. M. Gasperini

The nucleation and structure of silicon nanocrystals formed by different preparation conditions and silicon concentration (28 - 70 area %) have been studied using Transmission Electron Microscopy (TEM), Energy Filtered TEM (EFTEM) and…

We report on the formation of lobe-lobe (bi-lobed) Au-Ge nanostructures under ultra high vacuum (UHV) conditions (\approx 3\times 10^{-10} mbar) on clean Si(100) surfaces. For this study, \approx 2.0 nm thick Au samples were grown on the…

介观与纳米尺度物理 · 物理学 2017-11-27 Ashutosh Rath , J. K. Dash , R. R. Juluri , Marco Schowalter , Knut Mueller , A. Rosenauer , P. V. Satyam

The decomposition process mechanisms have been investigated in a Fe50Au25Pd25 (at.%) alloy processed by severe plastic deformation. Phases were characterized by X-ray diffraction and microstructures were observed using transmission electron…

材料科学 · 物理学 2009-01-12 Xavier Sauvage , Abdelahad Chbihi , Dmitry Gunderov , E. V. Belozerov , A. G. Popov

Nanostructured Zinc oxide (ZnO) was synthesized via a ball milling for 10 hours using high energy planetary ball mill. Phase purity and homogeneity of all the samples have been investigated by X-ray diffraction (XRD) and Field Emission…

材料科学 · 物理学 2015-06-11 Pawan Kumar , M. Kar , Anup V. Sanchela , C. V. Tomy , Ajay D. Thakur

In this study, a single-phase nanocrystalline Al-Cu-Fe-Ni-Cr high-entropy alloy (HEA) has been synthesized by mechanical alloying and comprehensively investigated for hydrogen storage responses evaluated in details. High-energy attritor…

材料科学 · 物理学 2025-09-05 Yogesh Kumar Yadav , Mohammad Abu Shaz , Thakur Prasad Yadav

In this study, a preparation route of Co-Cu alloys with soft magnetic properties by high-pressure torsion deformation is introduced. Nanocrystalline, supersaturated single-phase microstructures are obtained after deformation of Co-Cu…

Y-type hexaferrite samples Ba2ZnxCo2-xFe12O22 with x = 0, 1 and 2 were prepared from precursors synthesized by the citrate sol-gel auto combustion method. The powders were sintered at 1100{\deg} C for four hours. X-ray diffraction, scanning…

材料科学 · 物理学 2017-07-31 M. A. Awawdeh , R. N. Al-Bashaireh , A-F. Lehlooh , S. H. Mahmood

This work gives insights into processing and characterisation of bulk nanocrystalline FeCr materials. The investigated FeCr alloys, consisting of 30, 50 and 70 at.% ferromagnetic Fe and remaining anti-ferromagnetic Cr, are processed by arc…

This work demonstrates the development of a strong and ductile medium entropy alloy by employing conventional alloying and thermomechanical processing to induce partial recrystallization (PR) and precipitation strengthening in the…

材料科学 · 物理学 2021-09-29 Nithin Baler , Abdulla Samin M , Akshat Godha , Surendra Kumar Makineni

Control of the crystallization process at the microscopic level makes it possible to generate the nanocrystalline samples with the desired structural and morphological properties, that is of great importance for modern industry. In the…

材料科学 · 物理学 2019-03-25 Bulat N. Galimzyanov , Dinar T. Yarullin , Anatolii V. Mokshin

The microstructural characteristics of a single crystalline nickel based superalloy (AM1) tested under high temperature fatigue at 950$^\circ$C are reported. For repeated fatigue (R$_\varepsilon$=0) through a range of cycle numbers N with…

材料科学 · 物理学 2021-10-13 Valerie Brien , B. Décamps

Twenty-one distinct AlxCoCrFeNi alloys were rapidly prepared by laser alloying an equiatomic CoCrFeNi substrate with Al powder to create an alloy library ranging x=0.15-1.32. Variations in crystal structure, microstructure and mechanical…

材料科学 · 物理学 2018-02-21 Mu Li , Jaume Gazquez , Albina Borisevich , Rohan Mishra , Katharine M. Flores
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