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Measurements of the local tetragonality in Fe-C martensite at microstructural length-scale through pattern matching of electron backscatter diffraction patterns (EBSPs) and careful calibration of detector geometry are presented. It is found…

材料科学 · 物理学 2020-06-26 Tomohito Tanaka , Naoki Maruyama , Nozomu Nakamura , Angus J Wilkinson

The locally varying tetragonality in martensite grains of a high-carbon steel (1.2 mass percent C) was resolved by electron backscatter diffraction (EBSD) with a spatial resolution in the order of 100nm. Compared to spatially integrating…

材料科学 · 物理学 2020-11-23 Gert Nolze , Aimo Winkelmann , Grzegorz Cios , Tomasz Tokarski

Cleavage crack propagation has been investigated in a low-carbon lath-martensitic steel using electron back-scattered diffraction technique. The ability of different martensitic boundaries within prior-austenite grain, such as sub-block,…

材料科学 · 物理学 2016-07-19 Arya Chatterjee , A. Ghosh , A. Moitra , A. K. Bhaduri , R. Mitra , D. Chakrabarti

High angular resolution electron backscatter diffraction (HR-EBSD) affords an increase in angular resolution, as compared to 'conventional' Hough transform based EBSD, of two orders of magnitude, enabling measurements of relative…

仪器与探测器 · 物理学 2017-10-03 T Ben Britton , James L R Hickey

The determination of orientation relationships in dual or multi-phase materials is very important in the field of interface engineering for the design of materials with tailored properties. In this work, a code is developed for the…

材料科学 · 物理学 2023-04-13 Mattis Seehaus , Risheng Pei , Sandra Korte-Kerzel , Stefanie Sandlöbes-Haut

Analysis of distortions of the crystal lattice within individual mineral grains is central to the investigation of microscale processes that control and record tectonic events. These distortions are generally combinations of lattice…

材料科学 · 物理学 2019-06-04 David Wallis , Lars N. Hansen , T. Ben Britton , Angus J. Wilkinson

A formerly developed method aimed at determining the constituents of a merged X-ray pattern doublet was applied to estimate the fact that low-carbon martensite with high concentration of strong carbide-forming elements possesses abnormally…

材料科学 · 物理学 2011-08-18 L. S. Kremnev

Severe lattice distortion is suggested for high entropy alloys (HEAs), however, evidence for such effect so far is lacking, and the nature of distortion is yet to be understood. Here, we reveal the distortion in an fcc HEA, Al0.1CrFeCoNi,…

材料科学 · 物理学 2019-03-12 Yu-Tsun Shao , Renliang Yuan , Yang Hu , Qun Yang , Jian-Min Zuo

For high (angular) resolution electron backscatter diffraction (HR-EBSD), the selection of a reference diffraction pattern (EBSP0) significantly affects the precision of the calculated strain and rotation maps. This effect was demonstrated…

材料科学 · 物理学 2023-02-21 Abdalrhaman Koko , Vivian Tong , Angus J. Wilkinson , T. James Marrow

The phonon dispersion relations and elastic constants for ferromagnetic Ni$_2$MnGa in the cubic and tetragonally distorted Heusler structures are computed using density-functional and density-functional perturbation theory within the…

材料科学 · 物理学 2009-11-10 Claudia Bungaro , K. M. Rabe , A. Dal Corso

The heterogeneous evolution of microstructure in a single Cu/SAC305/Cu solder joint is investigated using in-situ thermal cycling combined with electron backscatter diffraction (EBSD). Local deformation due to thermal expansion mismatch…

材料科学 · 物理学 2019-08-30 Tianhong Gu , Christopher M. Gourlay , T. Ben Britton

Dispersion properties of electromagnetic crystals formed by small uniaxial resonant scatterers (magnetic or electric) are studied using the local field approach. The goal of the study is to determine the conditions under which the…

材料科学 · 物理学 2009-11-11 Pavel A. Belov , Constantin R. Simovski

Understanding the evolution of dislocation structures during plastic deformation is critical for predicting the mechanical performance of metallic materials. In this work, we applied in situ scanning electron microscopy/electron backscatter…

材料科学 · 物理学 2026-03-24 Mikhail Lebyodkin , Maxim Gussev , Jamieson Brechtl , Tatiana Lebedkina

Low-alloy steels are constituted of twenty-four variants of lath martensite that exhibit gradients of orientations from Kurdjumov-Sachs (KS) to Nishiyama-Wassermann (NW). They are structured into four packets on each of the common…

材料科学 · 物理学 2018-07-17 Cyril Cayron , Annick Baur , Roland Loge

Dolomite crystals in partially dolomitized limestone from the Platteville Formation are both compositionally and microstructurally heterogeneous. A single dolomite crystal usually contains three phases: the host Ca-rich dolomite…

地球物理 · 物理学 2016-08-12 Zhizhang Shen , Hiromi Konishi , Philip E Brown , Huifang Xu

In situ neutron diffraction of the uniaxial tension test was used to study the effect of the surrounding matrix microstructure on the mechanical stability of retained austenite in high-carbon bearing steels. Comparing the samples with…

材料科学 · 物理学 2018-07-18 Rohit Voothaluru , Vikram Bedekar , Dunji Yu , Qingge Xie , Ke An , R Scott Hyde

Electron backscatter diffraction (EBSD) is a well-established method of characterisation for crystalline materials. This technique can rapidly acquire and index diffraction patterns to provide phase and orientation information about the…

材料科学 · 物理学 2019-09-04 Alexander Foden , David Collins , Angus Wilkinson , Thomas Benjamin Britton

Lattice distortions associated with charge stripe order in 1/8 hole-doped La$_{1.875}$Ba$_{0.125-x}$Sr$_{x}$CuO$_{4}$ are studied using synchrotron X-ray diffraction for $x=0.05$ and $x=0.075$. The propagation wave vector and charge order…

超导电性 · 物理学 2009-11-10 H. Kimura , H. Goka , M. Fujita , Y. Noda , K. Yamada , N. Ikeda

We construct an electron optical system to investigate Bragg diffraction (the crystal lattice plane, $10^{-2}$-$10^{-3}$ rad) with the objective lens turned off by adjusting the current in the intermediate lenses. A crossover was located on…

材料科学 · 物理学 2019-11-06 Hiroshi Nakajima , Atsuhiro Kotani , Ken Harada , Shigeo Mori

The structure of low-carbon steel after twist extrusion is tested with using electron backscattered diffraction. It has been shown that warm twist extrusion results in grain refinement with conservation of a substantial part of high-angle…

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