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Bragg Coherent Diffraction Imaging (BCDI) is a powerful strain imaging tool, often limited by beam-induced sample instability for small particles and high power densities. Here, we devise and validate an adapted diffraction volume assembly…

Bragg coherent X-ray diffraction imaging (BCDI) allows the three-dimensional (3D) measurement of lattice strain along the scattering vector for specific microcrystals. If at least three linearly independent reflections are measured, the 3D…

Bragg coherent diffraction imaging (BCDI) is a unique and powerful method for tracking three-dimensional strain fields non-destructively. While BCDI has been successfully applied to many scientific research fields and receives high demands,…

应用物理 · 物理学 2023-06-21 Jiangtao Zhao , Ivan A. Vartanyants , Fucai Zhang

By using phase retrieval, Bragg Coherent Diffractive Imaging (BCDI) allows tracking of three-dimensional displacement fields inside individual nanocrystals. Nevertheless, in the presence of significant (1% and higher) strains, such as in…

材料科学 · 物理学 2020-02-19 Ziyi Wang , Oleg Gorobtsov , Andrej Singer

Coherent precipitation of ordered phases is responsible for providing exceptional high temperature mechanical properties in a wide range of compositionally complex alloys (CCAs). Ordered phases are also essential to enhance the magnetic or…

材料科学 · 物理学 2021-02-25 Maxime Dupraz , Steven J. Leake , Marie-Ingrid Richard

Focussed Ion Beam (FIB) milling is a mainstay of nano-scale machining. By manipulating a tightly focussed beam of energetic ions, often gallium (Ga+), FIB can sculpt nanostructures via localised sputtering. This ability to cut solid matter…

Coherent diffraction imaging (CDI) on Bragg reflections is a promising technique for the study of three-dimensional (3D) composition and strain fields in nanostructures, which can be recovered directly from the coherent diffraction data…

Bragg coherent diffraction imaging (BCDI), the well-established technique for imaging internal strain of nanoparticles, was used to image the internal compositional distribution of binary alloys in thermal equilibrium. The images…

介观与纳米尺度物理 · 物理学 2019-10-23 Tomoya Kawaguchi , Wonsuk Cha , Vitalii Latyshev , Serhii Vorobiov , Vladimir Komanicky , Hoydoo You

Bragg coherent diffraction imaging (BCDI) fails to reliably retrieve phases in micro-crystals exhibiting strong strain inhomogeneities, which restricts its applicability. Here we show that three-dimensional Bragg ptychography (3DBP)…

光学 · 物理学 2026-03-13 Peng Li , David Yang , Christoph Rau , Marc Allain , Felix Hofmann , Virginie Chamard

Measurement modalities in Bragg coherent diffraction imaging (BCDI) rely on finding signal from a single nanoscale crystal object, which satisfies the Bragg condition among a large number of arbitrarily oriented nanocrystals. However, even…

We present a general analytic approach to spatially resolve the nano-scale lattice distortion field of strained and defected compact crystals with Bragg coherent x-ray diffraction imaging (BCDI). Our approach relies on fitting a…

Nanoscale heterogeneity (including size, shape, strain, and defects) significantly impacts material properties and how they function. Bragg coherent x-ray imaging methods have emerged as a powerful tool to investigate, in three-dimensional…

材料科学 · 物理学 2018-08-02 A. Ulvestad , W. Cha , I. Calvo-Almazan , S. Maddali , S. M. Wild , E. Maxey , M. Duparaz , S. O. Hruszkewycz

Bragg coherent X-ray diffraction imaging (BCDI) is a non-destructive, lensless method for 3D-resolved, nanoscale strain imaging in micro-crystals. A challenge, particularly for new users of the technique, is accurate mapping of experimental…

材料科学 · 物理学 2021-03-05 David Yang , Nicholas W. Phillips , Felix Hofmann

Atomic level defects such as dislocations play key roles in determining the macroscopic properties of crystalline materials. Their effects are important and wide-reaching, and range from increased chemical reactivity to enhanced mechanical…

Corrosion is a major concern for many industries, as corrosive environments can induce structural and morphological changes that lead to material dissolution and accelerate material failure. The progression of corrosion depends on nanoscale…

Defects such as dislocations impact materials properties and their response during external stimuli. Defect engineering has emerged as a possible route to improving the performance of materials over a wide range of applications, including…

材料科学 · 物理学 2017-11-17 A. Ulvestad , M. Menickelly , S. M. Wild

This work proposes an innovative approach to improve Bragg coherent diffraction imaging (BCDI) microscopy applied to time evolving crystals and/or non-homogeneous crystalline strain fields, identified as two major limitations of BCDI…

光学 · 物理学 2024-03-12 I. Calvo-Almazán , V. Chamard , T. Grünewald , M. Allain

Coherent diffraction imaging enables the imaging of individual defects, such as dislocations or stacking faults, in materials.These defects and their surrounding elastic strain fields have a critical influence on the macroscopic properties…

We present an efficient method of imaging 3D nanoscale lattice behavior and strain fields in crystalline materials with a new methodology -- three dimensional Bragg projection ptychography (3DBPP). In this method, the 2D sample structure…

材料科学 · 物理学 2017-03-08 S. O. Hruszkewycz , M. Allain , M. V. Holt , C. E. Murray , J. R. Holt , P. H. Fuoss , V. Chamard

Coherent X-ray photons with energies higher than 50 keV offer new possibilities for imaging nanoscale lattice distortions in bulk crystalline materials using Bragg peak phase retrieval methods. However, the compression of reciprocal space…

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