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Millimeter-sized single crystals of LaFeAsO, LaFeAsO1-xFx, and LaFe1-xCoxAsO were grown in NaAs flux at ambient pressure. The detailed growth procedure and crystal characterizations are reported. The as-grown crystals have typical…

Superconducting single crystals of SmFeAsO$_{1-x}$ without fluorine doping were grown at a pressure of 3.3 GPa and a temperature of 1350-1450 $^\circ$C by using the self-flux method. Plate-like single crystals of a few-150 $\mu$m in their…

High quality single crystals of heavy Fermion CeCoIn5 superconductor have been grown by flux method with a typical size of (1~2)mm x (1~2)mm x ~0.1 mm. The single crystals are characterized by structural analysis from X-ray diffraction and…

Single crystals FeSe_x have been grown in evacuated sealed quartz tube using a NaCl/KCl flux. The products include two crystal structures of tetragon and hexagon. The electronic transport and magnetic properties measurements of FeSe_x…

超导电性 · 物理学 2009-11-13 S. B. Zhang , Y. P. Sun , X. D. Zhu , X. B. Zhu , B. S. Wang , G. Li , H. C. Lei , X. Luo , Z. R. Yang , W. H. Song , J. M. Dai

We report the synthesis and basic physical properties of single crystals of CaFe2As2, an isostructural compound to BaFe2As2 which has been recently doped to produce superconductivity. CaFe2As2 crystalizes in the ThCr2Si2 structure with…

强关联电子 · 物理学 2008-07-10 F. Ronning , T. Klimczuk , E. D. Bauer , H. Volz , J. D. Thompson

We have synthesized single crystals of FeTe1-xSx and investigated the structural and physical properties. The actual S concentration was found to be significantly smaller than the starting nominal value. The solubility limit of S for the Te…

Co-doped iron arsenic single crystal of BaFe1.87Co0.13As2 with dimension up to 20 x 10 x 2 mm3 were grown by a nucleation pole: an alumina stick served as nucleation center during growth. The high quality of crystalline was illustrated by…

超导电性 · 物理学 2015-05-13 D. L. Sun , Y. Liu , J. T. Park , C. T. Lin

We measured resistivity and specific heat of high-quality CsFe$_2$As$_2$ single crystals, which were grown by using a self-flux method. The CsFe$_2$As$_2$ crystal shows sharp superconducting transition at 1.8 K with the transition width of…

超导电性 · 物理学 2013-06-17 A. F. Wang , B. Y. Pan , X. G. Luo , F. Chen , Y. J. Yan , J. J. Ying , G. J. Ye , P. Cheng , X. C. Hong , S. Y. Li , X. H. Chen

We report single-crystal growth of La$_{0.34}$Na$_{0.66}$Fe$_2$As$_2$ iron-based superconductor with the size of several millimeters. The samples were accidentally obtained in trying to grow LaFeAsO$_{1-y}$F$_y$ ( $y \geq$ 0.8 ) single…

超导电性 · 物理学 2018-11-14 Yanhong Gu , Jia-Ou Wang , Xiaoyan Ma , Huiqian Luo , Youguo Shi , Shiliang Li

Single crystals of superconducting KxFe2-ySe2 have been grown with the optical floating-zone technique under application of 8 bar of argon pressure. We found that large and high quality single crystals with dimensions of ~\varnothing6…

超导电性 · 物理学 2012-07-09 Y. Liu , Z. C. Li , W. P. Liu , G. Friemel , D. S. Inosov , R. E. Dinnebier , Z. J. Li , C. T. Lin

An eutectic AlCl$_3$/KCl molten salt method in a horizontal configuration was employed to grow millimeter-sized and composition homogeneous CuFeSe$_2$ single crystals due to the continuous growth process in a temperature gradient induced…

Resistivity, magnetic susceptibility and heat capacity measurements are reported for single crystals of Fe1+yTexSe1-x grown via a modified Bridgeman method with 0 < y < 0.15, and x= 1, 0.9, 0.75, 0. 67, 0.55 and 0.5. Although resistivity…

超导电性 · 物理学 2009-11-13 B. C. Sales , A. S. Sefat , M. A. McGuire , R. Y. Jin , D. Mandrus , Y. Mozharivskyj

We report systematic investigation of high pressure crystal structures and structural phase transition upto 46 GPa in CaFeAsF and 40 GPa in SrFeAsF at 40 K using powder synchrotron x-ray diffraction experiments and Rietveld analysis of the…

High-quality Bi$_{2+x}$Sr$_{2-x}$CuO$_{6+\delta}$(0$<$x$\leq$0.5) single crystals have been grown successfully using the travelling-solvent floating-zone(TSFZ) technique. The samples with $x >$ 0.05 are in the underdoped level. The…

超导电性 · 物理学 2009-11-11 Huiqian Luo , Lei Fang , Gang Mu , Hai-Hu Wen

We report the synthesis, and structural and physical properties of CaFe4As3 single crystals. Needle-like single crystals of CaFe4As3 were grown out of Sn flux and the compound adopts an orthorhombic structure as determined by X-ray…

超导电性 · 物理学 2015-05-27 A. B. Karki , G. T. McCandless , S. Stadler , Y. M. Xiong , J. Li , Julia Y. Chan , R. Jin

Single crystals of LiFeAs were successfully grown by a self-flux method using the cubic anvil high-pressure and high-temperature technique. The reaction took place in a closed boron nitride crucible at a pressure of 1 GPa and a temperature…

超导电性 · 物理学 2024-11-05 N. D. Zhigadlo

Superconducting Sm(O,F)BiS2 single crystals were successfully grown using KI-KCl flux. The obtained single crystals were flat-shaped and their size was 500um. The structure and composition of the obtained single crystals were obtained using…

We synthesized large superconducting single crystal Ca0.77La0.18Fe0.90As2 ('112' type) of 2 millimeter size. Scanning electron microscopy (SEM) measurements revealed that bright and dark stripes alternately spread on the surface of…

超导电性 · 物理学 2016-03-18 W. Zhou , J. C. Zhuang , F. F. Yuan , X. Li , Y. Sun , X. Z. Xing , Z. X. Shi

We report anisotropic dc magnetic susceptibility $\chi(T)$, electrical resistivity $\rho(T)$, and heat capacity $C(T)$ measurements on the single crystals of CaFe$_{2-x}$Co$_x$As$_2$ for $x$ = 0 and 0.06. Large sized single crystals were…

超导电性 · 物理学 2009-11-13 Neeraj Kumar , R. Nagalakshmi , R. Kulkarni , P. L. Paulose , A. K. Nigam , S. K. Dhar , A. Thamizhavel

R(O,F)BiS2 (R: La, Ce, Pr, Nd) superconducting single crystals with different F concentrations are grown using a CsCl/KCl flux. The obtained 1-2 mm-sized single crystals have a plate-like shape and are cleavable along the ab-plane. The…

超导电性 · 物理学 2016-01-14 Masanori Nagao