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Here we report the superconductivity in the LaFeAsO1-xFx system prepared by high pressure synthesis. The highest onset superconducting transition temperature (Tc) in this La-based system is 41.0 K with the nominal composition of…

A safe, simple and easily scaleable one-step sintering method is proposed to fabricate newly discovered superconductors of SmO1-xFxFeAs. Superconducting transition with the onset temperature of 54.6 K and high critical fields Hc2(0) >=200 T…

超导电性 · 物理学 2009-02-20 Yanwei Ma , Zhaoshun Gao , Lei Wang , Yanpeng Qi , Dongliang Wang , Xianping Zhang

We report a systematic study on the effect of sintering temperature on the structural and superconducting properties of nominal SmO0.8F0.2FeAs fabricated by simple one-step solid state reaction method. A detailed correlation between the…

超导电性 · 物理学 2015-05-18 Chunlei Wang , Zhaoshun Gao , Lei Wang , Yanpeng Qi , Dongliang Wang , Chao Yao , Zhiyu Zhang , Yanwei Ma

The Phase diagram of SmFeAsO1-xFx in terms of x is exhibited in this study. SmFeAsO1-xFx from x = 0 to x = 0.3 were prepared by low temperature sintering with slow cooling. The low temperature sintering suppresses the formation of the…

We report on successful synthesis under high pressure of a series of polycrystalline GdFeAs O_{1-x}F_x high-Tc superconductors with different oxygen deficiency x=0.12 - 0.16 and also with no fluorine. We have found that the high-pressure…

A suppression of superconductivity in the late rare earth RFeAsO1-xFx materials is reported. The maximum critical temperature (Tc) decreases from 51 K for R = Tb to 36 K for HoFeAsO0.9F0.1, which has been synthesised under 10 GPa pressure.…

Superconducting poly- and single-crystalline samples of Sm1-xThxFeAsO with partial substitution of Sm3+ by Th4+ were synthesized and grown under high pressure and their structural, magnetic and transport properties are studied. The…

超导电性 · 物理学 2011-05-25 N. D. Zhigadlo , S. Katrych , S. Weyeneth , R. Puzniak , P. Moll , Z. Bukowski , J. Karpinski , H. Keller , B. Batlogg

We report on the synthesis and structural/ microstructural studies of iron based fluorine doped LaOFeAs superconductors. We have successfully synthesized fluorine doped superconducting LaO1-xFxFeAs materials by choosing lower temperature…

超导电性 · 物理学 2008-11-29 Chandra Shekhar , Sonal Singh , P K Siwach , H K Singh , O N Srivastava

Ag-sheathed SmFeAsO0.7F0.3 (Sm-1111) superconducting wires were prepared by a one-step solid state reaction at temperatures as low as 850~900C, instead of commonly used temperatures of 1150~1250C. The X-ray diffraction pattern of the…

超导电性 · 物理学 2015-05-18 Lei Wang , Yanpeng Qi , Dongliang Wang , Zhaoshun Gao , Xianping Zhang , Zhiyu Zhang , Chunlei Wang , Yanwei Ma

We study the effect of synthesis temperature on the phase formation in nano(n)-SiC added bulk MgB2 superconductor. In particular we study: lattice parameters, amount of carbon (C) substitution, microstructure, critical temperature (Tc),…

超导电性 · 物理学 2015-05-27 Arpita Vajpayee , R. Jha , A. K. Srivastava , H. Kishan , M. Tropeano , C. Ferdeghini , V. P. S. Awana

We report on the synthesis and microstructural studies of fluorine based iron doped superconductors. We have successfully synthesized the fluorine based new superconducting material LaO1-xFxFeAs by choosing comparatively lower temperature…

超导电性 · 物理学 2008-06-11 Chandra Shekhar , Sonal Singh , P K Siwach , H K Singh , O N Srivastava

Here, we report the synthesis and characterization of sulphur-substituted iron telluride i.e. FeTe1-xSx; (x = 0-30 %) system and study the impact of low temperature oxygen (O2) annealing as well. Rietveld analysis of room temperature x-ray…

超导电性 · 物理学 2015-05-19 V. P. S. Awana , Anand Pal , Arpita Vajpayee , Bhasker Gahtori , H. Kishan

We report the synthesis and characterization of antimony doped oxypnictide superconductor, LaO0.8F0.2FeAs1-xSbx (x = 0.05 and 0.10). The parent compound LaOFeAs with fluorine doping exhibits superconductivity at maximum transition…

超导电性 · 物理学 2009-03-23 S. J. Singh , J. Prakash , S. Patnaik , A. K. Ganguli

A series of Mn-doped CaKFe4As4 samples, CaK(Fe1-xMnx)4As4 with x values of 0, 0.005, 0.01, 0.02, 0.03, 0.04, and 0.05, are synthesized using two distinct routes: conventional synthesis process at ambient pressure (CSP), and high…

We have successfully synthesized a new superconducting phase of FeTe1-xSx with a PbO-type structure. It has the simplest crystal structure in iron-based superconductors. Superconducting transition temperature is about 10 K at x = 0.2. The…

超导电性 · 物理学 2009-01-07 Y. Mizuguchi , F. Tomioka , S. Tsuda , T. Yamaguchi , Y. Takano

A series of polycrystalline SmO1-xFxFeAs bulks (x=0.15, 0.2, 0.3 and 0.4) were prepared by the conventional solid state reaction. Resistivity, susceptibility, magnetic hysteresis, critical current density and microstructure of these samples…

超导电性 · 物理学 2009-11-13 Lei Wang , Zhaoshun Gao , Yanpeng Qi , Xianping Zhang , Dongliang Wang , Yanwei Ma

We obtained amorphous-FeAs-free SmFeAsO1-xFx using a low temperature sintering with slow cooling. SmFeAsO1-xFx is sintered at 980 {\deg}C for 40 hours and cooled slowly down to 600 {\deg}C. The low temperature sintering suppresses the…

Single crystals of SmFeAsO1-xFy of a size up to 120 micrometers have been grown from NaCl/KCl flux at a pressure of 30 kbar and temperature of 1350-1450 C using the cubic anvil high-pressure technique. The superconducting transition…

超导电性 · 物理学 2009-11-13 N. D. Zhigadlo , S. Katrych , Z. Bukowski , S. Weyeneth , R. Puzniak , J. Karpinski

we were able to develop a novel method to synthesize Fe-based oxypnictide superconductors. By using LnAs and FeO as the starting materials and a ball-milling process prior to solid-state sintering, Tc as high as 50.7 K was obtained with the…

超导电性 · 物理学 2010-04-08 Ai-Hua Fang , Fu-Qiang Huang , Xiao-Ming Xie , Mian-Heng Jiang

Polycrystalline samples with a nominal composition of NdFe1-xRhxAsO (0 <= x <= 0.25) were synthesized using a solid state reaction method. Bulk superconductivity with a maximum Tc = 13 K is observed in the x = 0.1 sample. A…

超导电性 · 物理学 2015-05-18 H. Y. Shi , X. L. Wang , T. -L. Xia , Q. M. Zhang , X. Q. Wang , T. -S. Zhao
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