相关论文: Single crystal growth and structural characterizat…
Here, we report self flux single crystal growth of FeTe1-xSex for x = 0 to 0.50 series via solid state reaction route,the resulted crystals as seen are shiny. X Ray diffraction performed on the surface of crystals elucidated the growth in…
We report self flux growth and characterization of FeTe1-xSx (x= 0.00 to 0.25) single crystal series. Surface X-ray diffraction (XRD) exhibited crystalline nature with growth in (00l) plane. Micro-structural (electron microscopy) images of…
Single crystals FeSe_x have been grown in evacuated sealed quartz tube using a NaCl/KCl flux. The products include two crystal structures of tetragon and hexagon. The electronic transport and magnetic properties measurements of FeSe_x…
We have synthesized polycrystalline samples and single crystals of Fe(Te1-xSx)y, and characterized their properties. Our results show that the solid solution of S in this system is limited, < 30%. We observed superconductivity at ~ 9 K in…
A series of tetragonal Fe$_{1-x}$Co${_x}$Se single crystals with a complete Co doping range (0$\leq$x$\leq$0.52) up to its solid solubility limit in FeSe have been grown by an eutectic AlCl${_3}$/KCl molten salt method. The typical lateral…
A new approach to grow FeSe1-xTex single crystals with optical zone-melting technique was successfully employed. Crystals with actual composition 0.4 < x < 1.0 all show high crystallinity with no phase separation. The ability to visually…
Millimeter sized single crystals of CaFe$_{1-x}$Co$_x$AsF were grown using a self-flux method. It is found that high-quality single crystals can be grown from three approaches with different initial raw materials. The chemical compositions…
Single crystals FeSex were grown in an evacuated sealed quartz tube using polycrystalline material by gas-transport reaction with I2 as a gas-carrier. Crystals with hexagonal-prismatic, tetragonal-prismatic, planar-square and hexagonal…
High-quality and sizable single crystals are crucial for studying the intrinsic properties of unconventional superconductors, which are lacking in the 1111 phase of the Fe-based superconductors. Here we report the successful growth of…
Centimeter sized platelet single crystals of KFe2As2 were grown using a self-flux method. An encapsulation technique using commercial stainless steel container allowed the stable crystal growth lasting for more than 2 weeks. Ternary K-Fe-As…
We have grown single crystals of Fe1+dTe by a conventional self-flux method. We obtained plate-like single crystals with dnom \geq 0.1. The value of the magnetization increased with increasing excess Fe concentration, and a broadening of…
Resistivity, magnetic susceptibility and heat capacity measurements are reported for single crystals of Fe1+yTexSe1-x grown via a modified Bridgeman method with 0 < y < 0.15, and x= 1, 0.9, 0.75, 0. 67, 0.55 and 0.5. Although resistivity…
The iron-based superconductor FeTe$_{1-x}$Se$_{x}$ has attracted considerable attention as a candidate topological superconductor owing to a unique combination of topological surface states and bulk high-temperature superconductivity. The…
We report synthesis of Co substitution at Fe site in Fe1-xCoxSe0.5Te0.5 (x=0.0 to 0.10) single crystals via vacuum shield solid state reaction route using flux free method. Single crystal XRD results showed that these crystals grow in (00l)…
We report the single crystal growth of Ca(Fe1-xCox)2As2 (0 <= x <= 0.082) from Sn flux. The temperature-composition phase diagram is mapped out based on the magnetic susceptibility and electrical transport measurements. Phase diagram of…
Superconducting single crystals of SmFeAsO$_{1-x}$ without fluorine doping were grown at a pressure of 3.3 GPa and a temperature of 1350-1450 $^\circ$C by using the self-flux method. Plate-like single crystals of a few-150 $\mu$m in their…
Single crystals of A$_{1-x}$K$_x$Fe$_2$As$_2$ (A=Ba, Sr) with high quality have been grown successfully by FeAs self-flux method. The samples have sizes up to 4 mm with flat and shiny surfaces. The X-ray diffraction patterns suggest that…
An eutectic LiCl/KCl flux method in a horizontal configuration has been used to grow a series of homogeneous Fe$_{1+\delta}$Se$_{1-x}$Te$_x$ single crystals of high quality with 0.5 $\leq$ $x$ $\leq$ 1. Compared with previously used…
We investigated the S-doping-driven phase transition from antiferromagnetic to superconducting in FeTe1-xSx single crystals. The partial substitution of Te by S suppresses antiferromagnetism in Fe-square lattice. Superconductivity is…
We report a crystal growth and physical properties of SrFe$_{2}$(As$_{1-x}$P$_{x}$)$_{2}$. The single crystals for various $x$s were grown by a self flux method. For $x = 0.35$, $T_c$ reaches the maximum value of 30\,K and the electrical…