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相关论文: Large single crystal growth of BaFe1.87Co0.13As2 u…

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We report a simple, reliable method to grow high quality BaFe$_{2-x}$Co$_x$As$_2$ single crystal samples without using any fluxing agent. The starting materials for the single crystal growth come from well-crystallized polycrystalline…

超导电性 · 物理学 2011-03-23 Changjin Zhang , Lei Zhang , Chuanying Xi , Langsheng Ling , Shun Tan , Yuheng Zhang

Single crystals of A$_{1-x}$K$_x$Fe$_2$As$_2$ (A=Ba, Sr) with high quality have been grown successfully by FeAs self-flux method. The samples have sizes up to 4 mm with flat and shiny surfaces. The X-ray diffraction patterns suggest that…

超导电性 · 物理学 2009-11-13 Huiqian Luo , Zhaosheng Wang , Huan Yang , Peng Cheng , Xiyu Zhu , Hai-Hu Wen

We report single-crystal growth of La$_{0.34}$Na$_{0.66}$Fe$_2$As$_2$ iron-based superconductor with the size of several millimeters. The samples were accidentally obtained in trying to grow LaFeAsO$_{1-y}$F$_y$ ( $y \geq$ 0.8 ) single…

超导电性 · 物理学 2018-11-14 Yanhong Gu , Jia-Ou Wang , Xiaoyan Ma , Huiqian Luo , Youguo Shi , Shiliang Li

Centimeter sized platelet single crystals of KFe2As2 were grown using a self-flux method. An encapsulation technique using commercial stainless steel container allowed the stable crystal growth lasting for more than 2 weeks. Ternary K-Fe-As…

High-quality and sizable single crystals are crucial for studying the intrinsic properties of unconventional superconductors, which are lacking in the 1111 phase of the Fe-based superconductors. Here we report the successful growth of…

超导电性 · 物理学 2015-07-03 Yonghui Ma , Hui Zhang , Bo Gao , Kangkang Hu , Qiucheng Ji , Gang Mu , Fuqiang Huang , Xiaoming Xie

Millimeter sized single crystals of CaFe$_{1-x}$Co$_x$AsF were grown using a self-flux method. It is found that high-quality single crystals can be grown from three approaches with different initial raw materials. The chemical compositions…

超导电性 · 物理学 2016-08-09 Yonghui Ma , Kangkang Hu , Qiucheng Ji , Bo Gao , Hui Zhang , Gang Mu , Fuqiang Huang , Xiaoming Xie

Single crystals of Ba0.6K0.4Fe2As2 with excellent quality have been successfully grown without fluxing agent through a simple one-step method for the first time. X-ray diffraction patterns demonstrate that the samples have high crystalline…

超导电性 · 物理学 2015-05-20 Chunlei Wang , Chao Yao , Lei Wang , Yanpeng Qi , Zhaoshun Gao , Dongliang Wang , Xianping Zhang , Yanwei Ma

Single crystals of superconducting KxFe2-ySe2 have been grown with the optical floating-zone technique under application of 8 bar of argon pressure. We found that large and high quality single crystals with dimensions of ~\varnothing6…

超导电性 · 物理学 2012-07-09 Y. Liu , Z. C. Li , W. P. Liu , G. Friemel , D. S. Inosov , R. E. Dinnebier , Z. J. Li , C. T. Lin

An eutectic AlCl$_3$/KCl molten salt method in a horizontal configuration was employed to grow millimeter-sized and composition homogeneous CuFeSe$_2$ single crystals due to the continuous growth process in a temperature gradient induced…

We measured resistivity and specific heat of high-quality CsFe$_2$As$_2$ single crystals, which were grown by using a self-flux method. The CsFe$_2$As$_2$ crystal shows sharp superconducting transition at 1.8 K with the transition width of…

超导电性 · 物理学 2013-06-17 A. F. Wang , B. Y. Pan , X. G. Luo , F. Chen , Y. J. Yan , J. J. Ying , G. J. Ye , P. Cheng , X. C. Hong , S. Y. Li , X. H. Chen

Boron arsenide (BAs) has been the least investigated cubic III-V compound, but it has recently attracted significant attention since the confirmation of its unusually high thermal conductivity above 1000 W/m-K. However, determining how to…

材料科学 · 物理学 2019-11-21 Geethal Amila Gamage , Ke Chen , Gang Chen , Fei Tian , Zhifeng Ren

In this letter, we report growth and characterization of bulk Bi2Se3 single crystals. The studied Bi2Se3 crystals are grown by self flux method through solid state reaction from high temperature (950C) melt of constituent elements and slow…

We grew (Hg,Re)Ba$_2$Ca$_2$Cu$_3$O$_{8+\delta}$ ((Hg,Re)1223) single crystals with good reproducibility via the single-step flux method using monoxides as raw materials. A double-sealing method using a thick-walled quartz tube and a…

Bulk single crystals of manganese arsenide (MnAs) were grown from melt at 1 GPa and 1100 {\deg}C by using a cubic-anvil, high-pressure, and high-temperature technique. The as-grown black colored crystals extracted from solidified lump…

材料科学 · 物理学 2017-11-08 Nikolai D. Zhigadlo

In this paper we present the single crystal growth of Fe0.95Se0.6Te0.4 high TC superconducting sample by the modified Bridgman technique. The x-ray diffraction pattern shows the single crystal nature of the sample, as only (00l) peaks are…

超导电性 · 物理学 2019-07-23 Anmol Shukla , Vishal K. Maurya , Rajendra S. Dhaka

We report on the first successful growth of single crystals of the noncentrosymmetric superconductor Mo$_3$Al$_2$C obtained by means of a cubic-anvil, high-pressure and high-temperature technique. Composition, structure, and normal-state…

超导电性 · 物理学 2018-06-27 N. D. Zhigadlo , D. Logvinovich , R. S. Gonnelli , V. A. Stepanov , D. Daghero

Using the self-flux technique we grew superconducting $(K_{1-z}Na_z)_{x}Fe_{2-y}Se_2$ (z = 0.3) single crystals. The EDX mapping revealed the uniform elements distribution on the crystal surface while the XRD measurements indicate that the…

Single crystals of LiFeAs were successfully grown by a self-flux method using the cubic anvil high-pressure and high-temperature technique. The reaction took place in a closed boron nitride crucible at a pressure of 1 GPa and a temperature…

超导电性 · 物理学 2024-11-05 N. D. Zhigadlo

We report the single crystal growth of Ca(Fe1-xCox)2As2 (0 <= x <= 0.082) from Sn flux. The temperature-composition phase diagram is mapped out based on the magnetic susceptibility and electrical transport measurements. Phase diagram of…

超导电性 · 物理学 2015-06-03 Rongwei Hu , Sheng Ran , S. L. Bud'ko , W. E. Straszheim , P. C. Canfield

We report the crystal growth of a new hole-doped iron-based superconductor Ba(Fe$_{0.875}$Ti$_{0.125}$)$_2$As$_2$ by substituting Ti on the Fe site. The crystals are accidentally obtained in trying to grow Ni doped…

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