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Two different hot isostatic pressing cycles (HIPing) were investigated to synthesize bulk MgB2 samples: a "standard" cycle where a low vessel pressure is maintained while heating to the process temperature with a subsequent simultaneous…

Superconductivity · Physics 2007-05-23 S. S. Indrakanti , V. F. Nesterenko , M. B. Maple , N. A. Frederick , W. M. Yuhasz , Shi Li

Very thick, ~ 40 $\mu$m, clean, and highly textured MgB2 film was effectively grown on an Al2O3 substrate. The fabrication technique is by the hybrid physical-chemical vapor deposition (HPCVD) using B2H6 gas and Mg ingot as the sources. The…

Superconductivity · Physics 2009-11-10 Chinping Chen , Xinfeng Wang , Ying Lu , Zhang Jia , Jing-pu Guo , Xiao-nan Wang , Meng Zhu , Xiangyu Xu , Jun Xu , Qing-rong Feng

We report the effect of the sintering temperature on the superconductivity of MgB2 pellets prepared under a high pressure of 3 GPa. The superconducting properties of the non-heated MgB2 in this high pressure were poor. However, as the…

Superconductivity · Physics 2009-11-07 C. U. Jung , Min-Seok Park , W. N. Kang , Mun-Seog Kim , Kijoon H. P. Kim , S. Y. Lee , Sung-Ik Lee

Fine grained polycrystalline samples of MgB(2) superconductor were synthesized from the elements to contain < 5 % of impurity phases, according to X-ray powder diffractometry. The superconductive transition was sharp with a midpoint Tc =…

Superconductivity · Physics 2007-05-23 J. R. Thompson , M. Paranthaman , D. K. Christen , K. D. Sorge , H. J. Kim , J. G. Ossandon

The new class of Mg-B superconducting conductors was prepared using the standard in-situ powder-in-tube, PIT, method where Mg+2B mixture was used to fill the copper and silver tubes. Study of the intergranular current, grain connectivity…

Superconductivity · Physics 2015-06-24 B. A. Glowacki , M. Majoros , M. E. Vickers , B. Zeimetz

Ultrathin MgB2 superconducting films with a thickness down to 7.5 nm are epitaxially grown on (0001) Al2O3 substrate by hybrid physical-chemical vapor deposition method. The films are phase-pure, oxidation-free and continuous. The 7.5 nm…

Superconductivity · Physics 2015-05-27 Yuhao Zhang , Zhiyuan Lin , Qian Dai , Dongyao Li , Yinbo Wang , Yan Zhang , Yue Wang , Qingrong Feng

The system MgxB2 has been investigated to investigate possible nonstoichiometry in MgB2. When synthesized at 850oC, MgB2 is a line compound with a possible Mg vacancy content of about 1%. Small changes in lattice constants as a function of…

Superconductivity · Physics 2009-11-07 D. G. Hinks , J. D. Jorgensen , Hong Zheng , S. Short

The distribution of magnetic field in single-phase polycrystalline bulk MgB2 has been measured using a Magneto-Optical (MO) technique for an external magnetic field applied perpendicular to the sample surface. The MO studies indicate that…

Superconductivity · Physics 2009-11-07 K. Kawano , J. S. Abell , M. Kambara , N Hari Babu , D. A. Cardwell

Cu-stabilized 18-filament MgB2 tapes with NbZr buffer have been fabricated by using powder-in-tube technique. The phase composition and microstructure were examined by X-ray diffraction and optical microscopy. Transport critical current…

Superconductivity · Physics 2007-05-23 C. F. Liu , S. J. Du , G. Yan , Y. Feng

The powder in tube method has been used to fabricate Ag and Cu clad MgB2 wires using an in-situ reaction method. The effects of short time sintering on the critical current densities of Ag and Cu clad MgB2 wires were studied. All the…

Superconductivity · Physics 2009-11-07 S. Soltanian , X. L. Wang , J. Horvat , A. H. Li , H. K. Liu , S. X. Dou

Current transport in polycrystalline magnesium diboride is highly non-uniform (percolative) due to the presence of secondary phases and also due to the intrinsic anisotropy of the material. The influence of secondary phases on the transport…

Superconductivity · Physics 2009-02-18 M. Eisterer , J. Emhofer , S. Sorta , M. Zehetmayer , H. W. Weber

We report the fabrication of MgB2 with bulk superconducting properties by conventional solid state methods at temperatures as low as 550 C. Mg deficiencies of the type Mg1-xB2 were tested. Tc was found to decrease by about 1K at large x,…

Superconductivity · Physics 2009-11-07 N. Rogado , M. A. Hayward , K. A. Regan , Yayu Wang , N. P. Ong , John M. Rowell , R. J. Cava

We succeeded in the synthesis of high-Jc MgB2 bulks via high energy ball-milling of elemental Mg and B powder at ambient temperatures. Alternatively to longtime mechanical alloying technique, the mixed powder was ball-milled for only 1h and…

Superconductivity · Physics 2008-01-14 Y. F. Wu , Y. Feng , G. Yan , J. S. Li , H. P. Tang , S. K. Chen , Y. Zhao , M. H. Pu , H. L. Xu , C. S. Li , Y. F. Lu

Fe-clad MgB2 long tapes have been fabricated using a powder-in-tube technique. An Mg + 2B mixture was used as the central conductor core and reacted in-situ to form MgB2. The tapes were sintered in pure Ar at 800 ^(o) C for 1 h at ambient…

Superconductivity · Physics 2009-11-07 S. Soltanian , X. L. Wang , I. Kusevic , E. Babic , A. H. Li , H. K. Liu , E. W. Collings , S. X. Dou

The microstructures of MgB2 wires prepared by the powder-in-tube technique and subsequent hot isostatic pressing were investigated using transmission electron microscopy. Large amount of crystalline defects including small angle twisting,…

Materials Science · Physics 2009-11-10 X. Z. Liao , A. Serquis , Y. T. Zhu , L. Civale , D. L. Hammon , D. E. Peterson , F. M. Mueller , V. F. Nesterenko , Y. Gu

We discuss the microwave second-harmonic generation in high-density bulk MgB2, prepared by the reactive liquid Mg infiltration technology. The intensity of the harmonic signal has been investigated as a function of temperature and…

Superconductivity · Physics 2007-05-23 A. Agliolo Gallitto , G. Bonsignore , G. Giunchi , M. Li Vigni

Superconducting thin films have been prepared in a two-step in-situ process, using the Mg-B plasma generated by pulsed laser ablation. The target was composed of a mixture of Mg and MgB2 powders to compensate for the volatility of Mg and…

Superconductivity · Physics 2009-11-07 D. H. A. Blank , H. Hilgenkamp , A. Brinkman , D. Mijatovic , G. Rijnders , H. Rogalla

This review paper illustrates the main normal and superconducting state properties of magnesium diboride, a material known since early 1950's, but recently discovered to be superconductive at a remarkably high critical temperature Tc=40K…

Superconductivity · Physics 2007-05-23 Cristina Buzea , Tsutomu Yamashita

We prepared and characterized monofilamentary MgB2 wires with a mechanically reinforced composite sheath of Ta(Nb)/Cu/steel, which leads to dense filaments and correspondingly high transport currents up to Jc = 10^5 A/cm^2 at 4.2 K, self…

Superconductivity · Physics 2009-11-07 W. Goldacker , S. I. Schlachter , S. Zimmer , H. Reiner

We have successfully synthesized MgB2 thick films on 4H-SiC substrate by hybrid physical-chemical deposition (HPCVD). The films have transition temperature TC above 40 K. X-ray diffraction (XRD) shows the c-axis oriented structure of MgB2,…

Superconductivity · Physics 2009-11-11 Fen Li , Tao Guo , Kaicheng Zhang , Li-ping Chen , Chinping Chen , Qing-rong Feng