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The microstructure of the MgB2 superconductor sintered at high temperature under a high pressure of about 3 GPa was investigated by using a high-resolution transmission electron microscope (HRTEM). The TEM images did not show any pores in…

The powder-in-tube MgB2 wires were prepared by high energy milling of Mg and B powder. The powder was not mechanically alloyed for 2h short milling time. However, the MgB2 grains in wires are very small (20 100nm) and resembled to the…

Superconductivity · Physics 2007-05-23 Y. F. Wu , G. Yan , J. S. Li , Y. Feng , S. K. Chen , H. P. Tang , H. L. Xu , C. S. Li , P. X. Zhang , Y. F. Lu

A commercial stainless steel tube was employed to synthesize MgB2. The specimen was prepared by a stoichiometric mixture of Mg and B. The specimen that had been enveloped in the commercial stainless steel tube was synthesized for 2 hours at…

Superconductivity · Physics 2007-05-23 H. B. Lee , Y. C. Kim , B. J. Kim , D. Y. Jeong

Bulk samples of MgB2 have been formed by hot isostatic pressing (HIPping) of commercial powder at 100MPa and 950=B0C. The resulting material is 100% dense with a sharp superconducting transition at 37.5K. Microstructural studies have…

Superconductivity · Physics 2009-11-07 T C Shields , K Kawano , D Holdom , J S Abell

We report a new in-situ reactive deposition thin film growth technique for the production of MgB2 thin films which offers several advantages over all existing methods and is the first deposition method to enable the production of…

Superconductivity · Physics 2009-11-11 Brian H. Moeckly , Ward S. Ruby

The two most common types of MgB2 conductor fabrication technique - in-situ and ex-situ - show increasing conflicts concerning the connectivity, an effective current-carrying cross-sectional area. An in-situ reaction yields a strong…

Superconductivity · Physics 2012-01-10 A. Yamamoto , H. Tanaka , J. Shimoyama , H. Ogino , K. Kishio , T. Matsushita

Highly dense nanocrystalline MgB_2 bulk superconductors with distinctly improved pinning were prepared by mechanical alloying of Mg and B powders and hot compaction at ambient temperatures. The nanocrystalline samples reveal high critical…

Superconductivity · Physics 2009-11-07 A. Gümbel , J. Eckert , G. Fuchs , K. Nenkov , K. -H. Müller , L. Schultz

The review considers bulk MgB2-based materials in terms of their structure, superconducting and mechanical properties. Superconducting transition temperatures of 34.5-39.4 K, critical current densities of 1.8-1.0 x E6 A/sq.cm in self field…

Superconductivity · Physics 2009-12-25 T. A. Prikhna

A MgB2 superconducting tape has been successfully prepared by a new way of boron diffusion into Mg tape. This tape superconductor has a Tc of 39 K with a sharp transition width of 0.4 K, high bulk critical current density jc of 6.7*10^5…

Superconductivity · Physics 2007-05-23 G. C. Che , S. L. Li , Z. A. Ren , L. Li , S. L. Jia , Y. M. Ni , H. Chen , C. Dong , J. Q. Li , H. H. Wen , Z. X. Zhao

In this paper we have investigated the effects of sintering time and temperature on the formation and critical current densities of Fe-clad MgB2 wires. MgB2 wires were fabricated using the powder-in-tube process and sintered for different…

Superconductivity · Physics 2015-06-24 X. L. Wang , S. Soltanian , J. Horvat , M. J. Qin , H. K. Liu , S. X. Dou

In the present paper we report an in-situ high-energy X-ray diffraction analysis of MgB2 tapes during the preparation process. The experiment was performed in a specifically designed furnace working in reducing atmosphere, compatible with…

We report the successful manufacture and characterization of a microwave resonant cylindrical cavity made of bulk MgB2 superconductor (Tc = 38.5 K), which has been produced by the Reactive Liquid Mg Infiltration technique. The quality…

Superconductivity · Physics 2007-05-23 G. Giunchi , A. Agliolo Gallitto , G. Bonsignore , M. Bonura , M. Li Vigni

Thin films of the recently discovered magnesium diboride (MgB2) intermetalic superconducting compound have been grown using a magnetron sputtering deposition technique followed by in-situ annealing at 830 C. High quality films were obtained…

Superconductivity · Physics 2009-11-07 R. Vaglio , M. G. Maglione , R. Di Capua

Bulk MgB2 samples were prepared under different synthesis conditions and analyzed by scanning and transmission electron microscopy. The critical current densities were determined from the magnetization versus magnetic field curves of bulk…

Materials Science · Physics 2018-07-04 A. Serquis , X. Z. Liao , L. Civale , Y. T. Zhu , J. Y. Coulter , D. E. Peterson , F. M. Mueller

The MgB2 - based material high-pressure synthesized at 2 GPa and 800 C for 1 h from Mg and B (taken in the stoichiometry ratio of MgB2) with addition of 2-10 wt% of Ti demonstrated the critical current density (jc) higher than 100 kA/cm^2…

We present electrical transport, magnetization, and specific heat measurements on bulk MgB2 samples (T_{c} = 38.5 K) synthesized under 200 MPa pressure using a process based on hot isostatic pressing with cooling under pressure. The samples…

Superconductivity · Physics 2009-11-07 N. A. Frederick , Shi Li , M. B. Maple , V. F. Nesterenko , S. S. Indrakanti

MgB2 wires and tapes suffer from a limitation of the transport current densities, especially at low field, due to an unsufficient thermal stabilization caused by hot spots from a non-homogeneous microstructure, the presence of secondary…

Superconductivity · Physics 2018-07-04 S. I. Schlachter , W. Goldacker , J. Reiner , S. Zimmer , B. Liu , B. Obst

Bulk samples of MgB2 were prepared with 5, 10, and 15% wt.% Y2O3 nanoparticles added using a simple solid-state reaction route. Transmission electron microscopy (TEM) showed a fine nanostructure consisting of ~3-5 nm YB4 nanoparticles…

High energy milling of MgB2 pre-reacted powder renders the material largely amorphous through extreme mechanical deformation and is suitable for mechanically alloying MgB2 with dopants including carbon. Bulk samples of milled C and MgB2…

Superconductivity · Physics 2009-11-10 B. J. Senkowicz , J. E. Giencke , S. Patnaik , C. B. Eom , E. E. Hellstrom , D. C. Larbalestier

The recently developed manufacturing technologies use high pressure and various doping additions to prepare bulk MgB2-based materials with a high critical current density measured by the magnetization methods. We use a contactless…

Superconductivity · Physics 2012-11-06 V. Meerovich , V. Sokolovsky , T. Prikhna , W. Gawalek , T. Habisreuther