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High-pressure (HP) synthesis and sintering are promising methods for manufacturing of the bulk MgB2 superconductive material. The available high-pressure apparatuses with 100 cm3 working volume can allow us to use the bulk MgB2 for…

Highly dense MgB2 policrystalline bulk materials, obtained by reactive liquid infiltration, have been characterized in their superconducting transport and magnetic properties in magnetic field and in a temperature range of interest for the…

Superconductivity · Physics 2007-05-23 G. Giunchi , S. Ceresara , L. Martini , V. Ottoboni , S. Chiarelli , M. Spadoni

The MgB2 bulks were prepared by high energy milling of Mg and B powder. The correlations among milling times, microstructure and superconducting properties were investigated in MgB2 bulks. Samples were characterized by x-ray diffraction…

Superconductivity · Physics 2008-01-14 Y. F. Wu , Y. F. Lu , G. Yan , J. S. Li , Y. Feng , H. P. Tang , S. K. Chen , H. L. Xu , C. S. Li , P. X. Zhang

The microwave response of three high-density bulk MgB2 samples has been investigated in the linear and nonlinear regimes. The three samples, characterized by different mean size of grains, have been obtained by reactive infiltration of…

Superconductivity · Physics 2007-05-23 A. Agliolo Gallitto , G. Bonsignore , G. Giunchi , M. Li Vigni , Yu. A. Nefyodov

The Powder-In-Tube process has been employed to fabricate tape-like conductors with a strong metallic sheath and based on the newly discovered MgB2 superconducting phase. Long superconducting tapes have been prepared by packing reacted MgB2…

Superconductivity · Physics 2009-11-07 G. Grasso , A. Malagoli , C. Ferdeghini , S. Roncallo , V. Braccini , M. R. Cimberle , A. S. Siri

The high-pressure synthesis is one of the most promising methods to produce MgB2 superconductive (SC) material. The available high-pressure apparatuses have working volume up to 100 cm3 which allows samples up to 60 mm in diameter to be…

Polycrystalline MgB2 samples with GaN additions were prepared by reaction of Mg, B, and GaN powders. The presence of Ga leads to a low melting eutectic phase which allowed liquid phase sintering and produces plate-like grains. For low-level…

Superconductivity · Physics 2009-11-11 S. K. Chen , Z. Lockman , M. Wei , B. A. Glowacki , J. L. MacManus-Driscoll

MgB2 tapes and wires were fabricated by the Powder-In-Tube method. Stainless steel and Cu-Ni tubes were used as sheath materials, and no heat treatment was applied. The tapes made of stainless steel showed transport critical current density…

Superconductivity · Physics 2009-11-07 H. Kumakura , A. Matsumoto , H. Fujii , K. Togano

The critical current density of four MgB2 samples was measured inductively and for one of them also by transport. Pure phased and dense bulk samples yield a critical current density which in value, as well as in its magnetic field and…

We report on the results of a comparative investigation of highly dense bulk MgB$_2$ samples prepared by three methods: (i) hot deformation; (ii) high pressure sintering; and (iii) mechanical alloying of Mg and B powders with subsequent hot…

High-density bulk materials of a newly discovered 40K intermetallic MgB2 superconductor were prepared by high pressure sintering. Superconducting transition with the onset temperature of 39K was confirmed by both magnetic and resistive…

Superconductivity · Physics 2009-11-07 Y. Takano , H. Takeya , H. Fujii , H. Kumakura , T. Hatano , K. Togano , H. Kito , H. Ihara

We have successfully prepared the MgB2 superconducting bulk and powdered materials by the method of combustion synthesis. The starting materials used in this study were powders of Mg and B. X-ray powder diffraction pattern was well assigned…

Superconductivity · Physics 2016-08-31 Yoshihiko Takano , Nobutaka Oguro , Yoshinari Kaieda , Kazumasa Togano

Recent advances in MgB2 conductors are leading to a new level of performance. Based on the use of proper powders, proper chemistry, and an architecture which incorporates internal Mg diffusion (IMD), a dense MgB2 structure with not only a…

Powdered and sintered MgB2 samples have been characterized through magnetic measurements performed from T = 5 K up to few degrees above the transition temperature of about 39 K. We found that the sintered samples behave as well-connected…

Superconductivity · Physics 2009-11-07 M. R. Cimberle , M. Novak , P. Manfrinetti , A. Palenzona

Bulk MgB2 - based materials with the following critical current densities (jc) in 1 T field: 570 kA/cm^2 at 10 K, 350 kA/cm^2 at 20 K and 40 kA/cm^2 at 30 K and in 10 T field: 650 A/cm^2 at 10 K have been high-pressure (HP) synthesized from…

We have investigated the microstructure, normal-state electrical connectivity, and critical current density of ex-situ MgB2 polycrystalline bulks prepared by systematically varying the sintering conditions under low pressure. Samples heated…

Superconductivity · Physics 2015-06-11 Hiroya Tanaka , Akiyasu Yamamoto , Jun-ichi Shimoyama , Hiraku Ogino , Kohji Kishio

We succeeded in the fabrication of high-Jc MgB2/Fe wires applying the internal Mg diffusion (IMD) process with pure Mg core and SiC addition. A pure Mg rod with 2 mm diameter was placed at the center of a Fe tube, and the space between Mg…

Superconductivity · Physics 2009-11-13 J. M. Hur , K. Togano , A. Matsumoto , H. Kumakura , H. Wada , K. Kimura

MgB2 thick film was synthesized on the stainless steel substrate by the technique of hybrid physical-chemical vapor deposition (HPCVD), using Mg ingot and B2H6 as the raw materials. The film thickness is about 10 microns. The scanning…

Superconductivity · Physics 2015-06-24 Qing-rong Feng , Chinping Chen , Ying Lu , Zhang Zia , Jing-pu Guo , Xiao-nan Wang , Meng Zhu , Jun Xu , Yong-zhong Wang

The MgB2 superconductor synthesized in a flowing argon atmosphere using nanometer magnesium powder as the raw materials, denoted as Nano-MgB2, has been studied by the technique of in-situ high temperature resistance measurement (HT-RT…

Superconductivity · Physics 2009-11-10 Chinping Chen , Zeng-jun Zhou , Xing-guo Li , Jun Xu , Yu-hao Wang , Yong-zhong Wang , Qing-rong Feng

In this letter, we report the first successful fabrication of dense, metal-clad MgB2 superconductor wires as well as the first demonstration of high transport Jc of greater than 36,000 A/cm2 in MgB2. The fabrication technique that we…

Superconductivity · Physics 2007-05-23 S. Jin , H. Mavoori , R. B. van Dover
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