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Measurement modalities in Bragg coherent diffraction imaging (BCDI) rely on finding signal from a single nanoscale crystal object, which satisfies the Bragg condition among a large number of arbitrarily oriented nanocrystals. However, even…

Bragg Coherent Diffraction Imaging (BCDI) is a powerful strain imaging tool, often limited by beam-induced sample instability for small particles and high power densities. Here, we devise and validate an adapted diffraction volume assembly…

Lattice defects play a key role in determining the properties of crystalline materials. Probing the 3D lattice strains that govern their interactions remains a challenge. Bragg Coherent Diffraction Imaging (BCDI) allows strain to be…

Bragg coherent diffraction imaging (BCDI) is a unique and powerful method for tracking three-dimensional strain fields non-destructively. While BCDI has been successfully applied to many scientific research fields and receives high demands,…

Applied Physics · Physics 2023-06-21 Jiangtao Zhao , Ivan A. Vartanyants , Fucai Zhang

We present a general analytic approach to spatially resolve the nano-scale lattice distortion field of strained and defected compact crystals with Bragg coherent x-ray diffraction imaging (BCDI). Our approach relies on fitting a…

Bragg coherent X-ray diffraction imaging (BCDI) is a non-destructive, lensless method for 3D-resolved, nanoscale strain imaging in micro-crystals. A challenge, particularly for new users of the technique, is accurate mapping of experimental…

Materials Science · Physics 2021-03-05 David Yang , Nicholas W. Phillips , Felix Hofmann

Bragg coherent diffraction imaging (BCDI) fails to reliably retrieve phases in micro-crystals exhibiting strong strain inhomogeneities, which restricts its applicability. Here we show that three-dimensional Bragg ptychography (3DBP)…

Bragg coherent diffraction imaging (BCDI), the well-established technique for imaging internal strain of nanoparticles, was used to image the internal compositional distribution of binary alloys in thermal equilibrium. The images…

Mesoscale and Nanoscale Physics · Physics 2019-10-23 Tomoya Kawaguchi , Wonsuk Cha , Vitalii Latyshev , Serhii Vorobiov , Vladimir Komanicky , Hoydoo You

By using phase retrieval, Bragg Coherent Diffractive Imaging (BCDI) allows tracking of three-dimensional displacement fields inside individual nanocrystals. Nevertheless, in the presence of significant (1% and higher) strains, such as in…

Materials Science · Physics 2020-02-19 Ziyi Wang , Oleg Gorobtsov , Andrej Singer

This paper addresses three-dimensional signal distortion and image reconstruction issues in x-ray Bragg coherent diffraction imaging (BCDI) in the event of a general non-orthogonal orientation of the area detector with respect to the…

Instrumentation and Detectors · Physics 2020-12-07 Siddharth Maddali , Marc Allain , Peng Li , Virginie Chamard , Stephan O. Hruszkewycz

Coherent precipitation of ordered phases is responsible for providing exceptional high temperature mechanical properties in a wide range of compositionally complex alloys (CCAs). Ordered phases are also essential to enhance the magnetic or…

Materials Science · Physics 2021-02-25 Maxime Dupraz , Steven J. Leake , Marie-Ingrid Richard

Coherent X-ray beams with energies $\geq 50$ keV can potentially enable three-dimensional imaging of atomic lattice distortion fields within individual crystallites in bulk polycrystalline materials through Bragg coherent diffraction…

This work proposes an innovative approach to improve Bragg coherent diffraction imaging (BCDI) microscopy applied to time evolving crystals and/or non-homogeneous crystalline strain fields, identified as two major limitations of BCDI…

Optics · Physics 2024-03-12 I. Calvo-Almazán , V. Chamard , T. Grünewald , M. Allain

We present a method to determine the strain tensor and local lattice rotation with Dark Field X-ray Microscopy. Using a set of at least 3 non-coplanar, symmetry-equivalent Bragg reflections, the illuminated volume of the sample can be kept…

X-ray Bragg coherent diffraction imaging has been demonstrated as a powerful three-dimensional (3D) microscopy approach for the investigation of sub-micrometer-scale crystalline particles. It is based on the measurement of a series of…

Coherent X-ray photons with energies higher than 50 keV offer new possibilities for imaging nanoscale lattice distortions in bulk crystalline materials using Bragg peak phase retrieval methods. However, the compression of reciprocal space…

Signal Processing · Electrical Eng. & Systems 2018-08-14 Siddharth Maddali , Irene Calvo-Almazan , Jonathan Almer , Peter Kenesei , Jun-Sang Park , Ross Harder , Youssef Nashed , Stephan Hruszkewycz

Electron backscatter diffraction (EBSD) is a well-established method of characterisation for crystalline materials. This technique can rapidly acquire and index diffraction patterns to provide phase and orientation information about the…

Materials Science · Physics 2019-09-04 Alexander Foden , David Collins , Angus Wilkinson , Thomas Benjamin Britton

Coherent diffraction imaging (CDI) on Bragg reflections is a promising technique for the study of three-dimensional (3D) composition and strain fields in nanostructures, which can be recovered directly from the coherent diffraction data…

High angular resolution electron backscatter diffraction (HR-EBSD) affords an increase in angular resolution, as compared to 'conventional' Hough transform based EBSD, of two orders of magnitude, enabling measurements of relative…

Instrumentation and Detectors · Physics 2017-10-03 T Ben Britton , James L R Hickey

We construct an electron optical system to investigate Bragg diffraction (the crystal lattice plane, $10^{-2}$-$10^{-3}$ rad) with the objective lens turned off by adjusting the current in the intermediate lenses. A crossover was located on…

Materials Science · Physics 2019-11-06 Hiroshi Nakajima , Atsuhiro Kotani , Ken Harada , Shigeo Mori
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