Electron diffraction covering a wide angular range from Bragg diffraction to small-angle diffraction
Abstract
We construct an electron optical system to investigate Bragg diffraction (the crystal lattice plane, - rad) with the objective lens turned off by adjusting the current in the intermediate lenses. A crossover was located on the selected-area aperture plane. Thus, the dark-field imaging can be performed by using a selected-area aperture to select Bragg diffraction spots. The camera length can be controlled in the range of 0.8 to 4 m without exciting the objective lens. Furthermore, we can observe the magnetic-field dependence of electron diffraction using the objective lens under weak excitation conditions. The diffraction mode for Bragg diffraction can be easily switched to a small-angle electron diffraction mode having a camera length of more than 100 m. We propose this experimental method to acquire electron diffraction patterns that depict an extensive angular range from 10 to 10 rad. This method is applied to analyze the magnetic microstructures in three distinct magnetic materials, i.e., a uniaxial magnetic structure of BaFeScMgO, a martensite of a Ni-Mn-Ga alloy, and a helical magnetic structure of BaSrZnFeO.
Cite
@article{arxiv.1911.01677,
title = {Electron diffraction covering a wide angular range from Bragg diffraction to small-angle diffraction},
author = {Hiroshi Nakajima and Atsuhiro Kotani and Ken Harada and Shigeo Mori},
journal= {arXiv preprint arXiv:1911.01677},
year = {2019}
}
Comments
18 pages, 5 figures