English

Electron diffraction covering a wide angular range from Bragg diffraction to small-angle diffraction

Materials Science 2019-11-06 v1

Abstract

We construct an electron optical system to investigate Bragg diffraction (the crystal lattice plane, 10210^{-2}-10310^{-3} rad) with the objective lens turned off by adjusting the current in the intermediate lenses. A crossover was located on the selected-area aperture plane. Thus, the dark-field imaging can be performed by using a selected-area aperture to select Bragg diffraction spots. The camera length can be controlled in the range of 0.8 to 4 m without exciting the objective lens. Furthermore, we can observe the magnetic-field dependence of electron diffraction using the objective lens under weak excitation conditions. The diffraction mode for Bragg diffraction can be easily switched to a small-angle electron diffraction mode having a camera length of more than 100 m. We propose this experimental method to acquire electron diffraction patterns that depict an extensive angular range from 102^{-2} to 107^{-7} rad. This method is applied to analyze the magnetic microstructures in three distinct magnetic materials, i.e., a uniaxial magnetic structure of BaFe10.35_{10.35}Sc1.6_{1.6}Mg0.05_{0.05}O19_{19}, a martensite of a Ni-Mn-Ga alloy, and a helical magnetic structure of Ba0.5_{0.5}Sr1.5_{1.5}Zn2_{2}Fe12_{12}O22_{22}.

Keywords

Cite

@article{arxiv.1911.01677,
  title  = {Electron diffraction covering a wide angular range from Bragg diffraction to small-angle diffraction},
  author = {Hiroshi Nakajima and Atsuhiro Kotani and Ken Harada and Shigeo Mori},
  journal= {arXiv preprint arXiv:1911.01677},
  year   = {2019}
}

Comments

18 pages, 5 figures