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With dark firld x-ray microscopy, it is possible to measure reciprocal space manps of localized volumes embedded deeply in a large sample. Ferroelastic materials contains elastic twins that display characteristing splitting of diffraction…

材料科学 · 物理学 2024-01-15 Mads Carlsen , Marion Hoefling , Carsten Detlefs , Hugh Simons

Many ferroelectric materials undergo thermally driven transitions between cubic and tetragonal phases. Despite being well-known for decades, such transitions still pose unresolved questions, particularly about the role of domains in shaping…

材料科学 · 物理学 2025-09-30 S. Gorfman , I. Biran , N. Zhang , Z. -G. Ye

Coherent diffraction imaging enables the imaging of individual defects, such as dislocations or stacking faults, in materials.These defects and their surrounding elastic strain fields have a critical influence on the macroscopic properties…

Visualization of internal deformation fields in crystalline materials helps bridge the gap between theoretical models and practical applications. Applying Bragg coherent diffraction imaging under X-ray dynamical diffraction conditions…

应用物理 · 物理学 2025-12-29 Longlong Wu , David Yang , Wei Wang , Shinjae Yoo , Ross J. Harder , Wonsuk Cha , Aiguo Li , Ian K. Robinson

Exploiting the emerging nanoscale periodicities in epitaxial, single-crystal thin films is an exciting direction in quantum materials science: confinement and periodic distortions induce novel properties. The structural motifs of interest…

We present a detailed single crystal x-ray diffraction study of twinned orthorhombic perovskites. The diffraction pattern can be indexed on a $2a_p$x$2a_p$x$2a_p$ lattice, but does not obey cubic symmetry relations. The data can be modelled…

凝聚态物理 · 物理学 2007-05-23 Bas B. Van Aken , Auke Meetsma , Thomas T. M. Palstra

When two-dimensional crystals are brought into close proximity, their interaction results in strong reconstruction of electronic spectrum and local crystal structure. Such reconstruction strongly depends on the twist angle between the two…

介观与纳米尺度物理 · 物理学 2025-10-27 C. R. Woods , P. Ares , H. Nevison-Andrews , M. J. Holwill , R. Fabregas , F. Guinea , A. K. Geim , K. S. Novoselov , N. R. Walet , L. Fumagalli

Under high pressures, phase transition, as well as deformation twins, are constantly reported in many BCC metals, whose interactions are of fundamental importance to understand strengthen mechanism of these metals under extreme conditions.…

材料科学 · 物理学 2017-10-11 Kun Wang , Jun Chena , Xueyang Zhang , Wenjun Zhu

By using phase retrieval, Bragg Coherent Diffractive Imaging (BCDI) allows tracking of three-dimensional displacement fields inside individual nanocrystals. Nevertheless, in the presence of significant (1% and higher) strains, such as in…

材料科学 · 物理学 2020-02-19 Ziyi Wang , Oleg Gorobtsov , Andrej Singer

Imaging of the Bragg reflected x-ray beam is proposed and validated as an in-situ method for characterization of performance of double-crystal monochromators under the heat load of intense synchrotron radiation. A sequence of images is…

光学 · 物理学 2016-01-19 Stanislav Stoupin , Zunping Liu , Steve M. Heald , Dale Brewe , Mati Meron

Understanding the mechanisms and spatial correlations of crystallographic symmetry breaking in ferroelectric materials is essential to tuning their functional properties. While optical second harmonic generation (SHG) has long been utilized…

材料科学 · 物理学 2022-08-10 Wei Li , Yunpeng Ma , Tianyi Feng , Sergei V. Kalinin , Jing-Feng Li , Qian Li

The effective piezoelectric coefficients of twin walls in tetragonal ferroelectric are calculated in the framework of decoupling approximation and Landau-Ginzburg-Devonshire theory allowing for polarization gradient terms, electrostriction…

材料科学 · 物理学 2015-06-12 Anna N. Morozovska , Eugene A. Eliseev , Olexander V. Varenyk , Sergei V. Kalinin

Very sensitive responses to external forces are found near phase transitions. However, phase transition dynamics and pre-equilibrium phenomena are difficult to detect and control. We have directly observed that the equilibrium domain…

Twinning is an important deformation mode of hexagonal close-packed metals. The crystallographic theory is based on the 150-years old concept of simple shear. The habit plane of the twin is the shear plane, it is invariant. Here we present…

材料科学 · 物理学 2018-07-17 Cyril Cayron , Roland Loge

Polarization in ferroelectric domains arises from atomic-scale structural variations that govern macroscopic functionalities. The interfaces between these domains known as domain walls host distinct physical responses, making their…

The successive phase transitions of the pyrochlore oxide Cd2Re2O7 are studied by polarizing microscopy and magnetic susceptibility measurements. The formation of twin domains is visualized in the polarizing images of a pristine (111)…

超导电性 · 物理学 2018-10-02 Yasuhito Matsubayashi , Daigorou Hirai , Masashi Tokunaga , Zenji Hiroi

Identifying the three-dimensional (3D) crystal-plane and strain-field distributions of nanocrystals is essential for optical, catalytic, and electronic applications. Here, we developed a methodology for visualizing the 3D information of…

Molecular and polymeric crystals show a wide range of functional properties that arise from the interplay between the atomic-scale structure of their constituent molecules and the organization of these molecules within the crystal lattice…

Strain engineering of perovskite oxide thin films has proven to be an extremely powerful method for enhancing and inducing ferroelectric behavior. In ferroelectric thin films and superlattices, the polarization is intricately linked to…

Deformation twinning significantly influences the microstructure, texture, and mechanical properties of metals, necessitating comprehensive studies of twin formation and interactions. While experimental methods excel at analyzing individual…

材料科学 · 物理学 2024-02-19 H. J. Ehrich , A. Dollmann , P. G. Grützmacher , C. Gachot , S. J. Eder
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