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A method of preparing the nanoparticles of CaCu3Ti4O12 (CCTO) with the crystallite size varying from 30 to 200 nm is optimized at a temperature as low as 680 1C from the exothermic thermal decomposition of an oxalate precursor,…

材料科学 · 物理学 2013-01-18 P. Thomas , K. Dwarakanath , K. B. R. Varma , T. R. N. Kutty

A complex oxalate precursor, CaCu3(TiO)4(C2O4)8.9H2O, was synthesized and the precipitate that obtained was confirmed to be monophasic by the wet chemical analyses, X-ray diffraction, FTIR absorption and TG, DTA analyses. The thermal…

材料科学 · 物理学 2013-01-21 P. Thomas , K. Dwarakanath , K. B. R. Varma , T. R. N. Kutty

Highly crystalline TiO2 nanostructures were prepared through a facile inorganic acid-assisted hydrothermal treatment of hexagonal-structured assemblies of nanocrystalline titiania templated by cetyltrimethylammonium bromide (Hex-ncTiO2/CTAB…

材料科学 · 物理学 2012-11-20 Shuxi Dai , Yanqiang Wu , Toshio Sakai , Zuliang Du , Hideki Sakai , Masahiko Abe

The polyol route is a versatile and up-scalable method to produce large batches of iron oxide nanoparticles with well-defined structure and magnetic properties. Controlling parameters such as temperature and duration of reaction, heating…

Ti-O nanoparticles have been synthesized via hollow cathode sputtering in an Ar-O2 atmosphere using high power pulsing. It is shown that the stoichiometry and the size of the nanoparticles can be varied independently, the former through…

介观与纳米尺度物理 · 物理学 2018-10-09 Rickard Gunnarsson , Ulf Helmersson , Iris Pilch

The magnetic behavior of $Fe_{3-x}O_4$ nanoparticles synthesized either by high-temperature decomposition of an organic iron precursor or low-temperature co-precipitation in aqueous conditions, is compared. Transmission electron microscopy,…

Solution precursor thermal spray can become a breakthrough technology for the deposition of coatings with novel chemistries; however, the understanding of the process that the feedstock material undergoes is still poorly understood when…

应用物理 · 物理学 2020-12-01 Daniel Tejero-Martin , Zdenek Pala , Simon Rushworth , Tanvir Hussain

Nanoporous structures play a promising role in the development of nanomechanical, nanoelectrical and biosensing devices. In addition, nanopores can be utilized as chemical and gas sensors. TiO2 is a semiconductor material, which can have a…

材料科学 · 物理学 2012-07-30 Subhasish Chatterjee , Miriam Ginzberg , Bonnie Gersten

BiFe1-xCrxO3 (x=0.0, 0.05 and 0.1) nanoparticles are prepared by a combustion method without using any solvent. All the synthesized nanoparticles are single phase in nature, nearly spherical in shape and crystallize in distorted perovskite…

材料科学 · 物理学 2015-02-23 Samar Layek , Santanu Saha , H. C. Verma

Nanocrystalline (Th1-xFex)O2-d particles with different Fe concentrations (x = 0.0, 0.05, 0.10, 0.15, 0.20 and 0.25) have been prepared by a gel combustion method. Rietveld refinement analyses of X-ray diffraction data revealed the…

材料科学 · 物理学 2007-07-27 O. D. Jayakumar , I. K. Gopalakrishnan , A. Vinu , A. Asthana , A. K. Tyagi

Vapor deposition allows for the synthesis of metastable polymorphs with unique properties, yet polymorph selection remains largely empirical due to the lack of predictive guidelines bridging thermodynamics, kinetics, and synthesis…

材料科学 · 物理学 2026-03-23 Hyeon Woo Kim , Han Uk Lee , Rohan Mishra , Sung Beom Cho

Surface confined dehalogenation reactions are versatile bottom-up approaches for the synthesis of carbon-based nanostructures with predefined chemical properties. However, for devices generally requiring low conductivity substrates,…

V2O3 nanocrystals can be synthesized through hydrothermal reduction of VO(OH)2 using hydrazine as a reducing agent. Addition of different ligands to the reaction produces nanoparticles, nanorods and nanoplatelets of different sizes. Small…

Single phase BiFeO3 nanoparticles have been successfully synthesized for the first time by a novel citrate combustion method without using any solvent. Well mixed metal nitrates along with citric acid which is used as fuel combust to give…

材料科学 · 物理学 2015-02-23 Samar Layek , H. C. Verma

A novel design has been proposed for a facile and rapid build-up of highly tailorable nanostructured multishells on metal oxide particles (graphene/TiOx@TiO2) under a dry inert atmosphere to maximize the visible-light photocatalytic…

材料科学 · 物理学 2022-02-15 Kunihiko Kato , Yunzi Xin , Sebastien Vaucher , Takashi Shirai

This paper analyzes how the ferroelectric properties of cubic-like BiFeO$_3$ nanoparticles are affected by different terminations and charge distributions at the surface using ab-initio-based atomistic computational experiments. Our…

材料科学 · 物理学 2025-01-03 Mauro A. P. Goncalves , Monica Graf , Marek Pasciak , Jiri Hlinka

Carbon is conventionally not associated with magnetism, and much of the discussion of its nanotechnology perspectives appears to be centered on its electron transport properties. Among the few existing examples of magnetic carbon…

Thin films of (1-x)BiFeO<sub>3</sub>-xPbTiO<sub>3</sub> (BF-xPT) with x ~ 0.60 were fabricated on Pt/Si substrates by chemical solution deposition of precursor BF and PT layers alternately in three different multilayer configurations. These…

Thermal plasma has emerged as an effective approach for producing carbon nanostructures without the need for specific catalysts nor substrates. While efforts have focused on the effect of process parameters such as reaction pressure, input…

材料科学 · 物理学 2025-12-05 Taki Aissou , Jerome Menneveux , Fanny Casteignau , Nadi Braidy , Jocelyn Veilleux

We report magnetic, optical and oxidation states of oxygen deficient TiO$_{2-\delta}$ nanoparticles (NPs) synthesized by environment-friendly green route using Phyllanthus niruri (PN) whole plant extract instead of leaf extract. Rietveld…

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