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Convergent beam electron diffraction is routinely applied for studying deformation and local strain in thick crystals by matching the crystal structure to the observed intensity distributions. Recently, it has been demonstrated that CBED…

In this two-part article series we provide a generalized description of the scattering geometry of Bragg coherent diffraction imaging (BCDI) experiments, the shear distortion effects inherent to the resulting three-dimensional (3D) image…

Coherent X-ray photons with energies higher than 50 keV offer new possibilities for imaging nanoscale lattice distortions in bulk crystalline materials using Bragg peak phase retrieval methods. However, the compression of reciprocal space…

In this work, issues in phase retrieval in the coherent diffractive imaging (CDI) technique, from discussion on parameters for setting up a CDI experiment to evaluation of the goodness of the final reconstruction, are discussed. The…

光学 · 物理学 2018-11-01 Tatiana Latychevskaia

Bragg coherent X-ray diffraction imaging (BCDI) allows the three-dimensional (3D) measurement of lattice strain along the scattering vector for specific microcrystals. If at least three linearly independent reflections are measured, the 3D…

We perform a theoretical and numerical study of the optical properties of both direct and inverse three-dimensional (3D) chiral woodpile structures, and a corresponding chiral Bragg stack. We compute transmission spectra in the helical…

Understanding the out-of equilibrium behaviour of point defects in crystals, yields insights into the nature and fragility of the ordered state, as well as being of great practical importance. In some rare cases defects are spontaneously…

软凝聚态物质 · 物理学 2013-10-14 William T. M. Irvine , Mark J. Bowick , Paul M. Chaikin

We present an investigation of coherent backscattering of light that is multiple scattered by a photonic crystal by using a broad-band technique. The results significantly extend on previous backscattering measurements on photonic crystals…

介观与纳米尺度物理 · 物理学 2011-04-21 Otto L. Muskens , A. Femius Koenderink , Willem L. Vos

A gyroid structure is a distinct morphology that is triply periodic and consists of minimal isosurfaces containing no straight lines. We have designed and synthesized amorphous silicon (a-Si) mid-infrared gyroid photonic crystals that…

This work proposes an innovative approach to improve Bragg coherent diffraction imaging (BCDI) microscopy applied to time evolving crystals and/or non-homogeneous crystalline strain fields, identified as two major limitations of BCDI…

光学 · 物理学 2024-03-12 I. Calvo-Almazán , V. Chamard , T. Grünewald , M. Allain

A structural understanding of whole cells in three dimensions at high spatial resolution remains a significant challenge and, in the case of X-rays, has been limited by radiation damage. By alleviating this limitation, cryogenic coherent…

Atomic level defects such as dislocations play key roles in determining the macroscopic properties of crystalline materials. Their effects are important and wide-reaching, and range from increased chemical reactivity to enhanced mechanical…

Coherent diffractive imaging (CDI) provides new opportunities for high resolution X-ray imaging with simultaneous amplitude and phase contrast. Extensions to CDI broaden the scope of the technique for use in a wide variety of experimental…

光学 · 物理学 2016-01-20 Matthew H. Seaberg , Alexandre d'Aspremont , Joshua J. Turner

Twinning is a common crystallographic phenomenon, which usually occurs in crystals during symmetry-lowering phase transition. Once formed, twin domains play an important role in defining physical properties: for example, twin domains…

材料科学 · 物理学 2021-10-28 Semen Gorfman , David Spirito , Guanjie Zhang , Carsten Detlefs , Nan Zhang

We have developed a 3 dimensional Coherent Diffraction Imaging (CDI) algorithm to retrieve phases of diffraction patterns of samples in Grazing Incidence Small Angle X-ray Scattering (GISAXS) experiments. The algorithm interprets the…

仪器与探测器 · 物理学 2023-07-26 Yi Yang , Sunil K. Sinha

A new method for estimation of intragranular strain fields in polycrystalline materials based on scanning three-dimensional X-ray diffraction data (scanning-3DXRD) is presented and evaluated. Given an apriori known anisotropic compliance,…

材料科学 · 物理学 2021-06-16 Axel Henningsson , Johannes Hendriks

This paper addresses three-dimensional signal distortion and image reconstruction issues in x-ray Bragg coherent diffraction imaging (BCDI) in the event of a general non-orthogonal orientation of the area detector with respect to the…

仪器与探测器 · 物理学 2020-12-07 Siddharth Maddali , Marc Allain , Peng Li , Virginie Chamard , Stephan O. Hruszkewycz

Measurement modalities in Bragg coherent diffraction imaging (BCDI) rely on finding signal from a single nanoscale crystal object, which satisfies the Bragg condition among a large number of arbitrarily oriented nanocrystals. However, even…

Van der Waals heterostructures have been lately intensively studied because they offer a large variety of properties that can be controlled by selecting 2D materials and their sequence in the stack. The exact arrangement of the layers as…

Solution-phase bottom up self-assembly of nanocrystals into superstructures such as ordered superlattices is an attractive strategy to generate functional materials of increasing complexity, including very recent advances that incorporate…