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The effect of sintering regimes on the density, microstructure parameters, and mechanical properties of Al2O3 and Al2O3 + 0.25%MgO ceramics has been investigated. The ceramics were sintered in three regimes: Regime I - heating at a constant…

Multiferroic bismuth ferrite Bi_2Fe_4O_9 (BFO) ceramic was synthesized by conventional solid state reaction route. X-ray diffraction and Rietveld refinement show formation of single phase ceramic with orthorhombic crystal structure (space…

材料科学 · 物理学 2016-05-06 S. R. Mohapatra , B. Sahu , T. Badapanda , M. S. Pattanaik , S. D. Kaushik , A. K. Singh

NdFeO3 modified polycrystalline ceramics with composition (NdFeO3)0.1-(Ba0.7Sr0.3TiO3)0.9 (NFBST) ceramics have been synthesized via solid-state reaction route. The Rietveld refinement of the XRD data confirmed the existence of a tetragonal…

材料科学 · 物理学 2019-06-26 Anumeet Kaur , Lakhwant Singh

The Ba0.85Ca0.15Zr0.1Ti0.9O3 (BCZT) ceramics were successfully prepared by sol-gel process, and sintered at 1420 degree. The effect of sintering times (2, 4 and 6 h) on structural, microstructural, electric properties, energy storage, and…

材料科学 · 物理学 2021-02-03 H. Mezzourh , S. Belkhadir , D. Mezzane , M. Amjoud , E. Choukri , A. Lahmar , Y. Gagou , Z. Kutnjak , M. El Marssi

Silicate ceramics are of considerable promise as high frequency dielectrics in emerging millimetre wave applications including high bandwidth wireless communication and sensing. In this review, we show how high quality factors and low,…

材料科学 · 物理学 2021-04-15 Franz Kamutzki , Sven Schneider , Jan Barowski , Aleksander Gurlo , Dorian A. H. Hanaor

Lead-free Ba0.9Sr0.1Ti0.9Sn0.1O3 (BSTSn) ceramic was prepared by the sol gel method. X-ray diffraction measurement at room temperature reveals the single-phase formation with tetragonal structure refined in the P4mm space group. Raman…

材料科学 · 物理学 2023-06-13 S. Khardazi , H. Zaitouni , B. Asbani , D. Mezzane , M. Amjoud , E. Choukri , S. Terenchuk , A. Erramli , Y. Gagou

Conductive ceramics played an important role in industries and manufactures due to their wide applications on electronics devices. Many synthesis approaches to prepare ceramics have been developing rapidly in the few decades. One of the…

材料科学 · 物理学 2017-07-18 Deski Beri , Rahmi Muthia , Ali Amran

The perovskite (1-x)YMnO$_3$-xBiFeO$_3$ binary system is very promising because of its multiferroic end members. Nanocrystalline phases have been recently obtained by mechanosynthesis across the system, and the perovskite structural…

The effect of sintering temperatures (Ts) on the structural and magnetic properties of Ni0.6Zn0.4Fe2O4 (NZFO) ferrites synthesized by conventional double sintering method has been reported. The samples are sintered at 1200, 1250 and 1300…

Focused ion beam (FIB)-scanning electron microscopy (SEM) allowed the characterization of the microstructure of two solid oxide fuel cells prepared at different sintering temperatures. 3D volume reconstruction showed that a relatively low…

应用物理 · 物理学 2023-04-27 C. M. Ruse , L. A. Hume , Y. Wang , T. Pesacreta , X-D. Zhou

We have carried out the powder x-ray diffraction and dielectric studies on multiferroic particulate composite xNi0.9Zn0.1Fe2O4/(1-x)PbZr0.52Ti0.48O3 with x=0.15, 0.30, 0.45, 0.60, 0.75 and 0.90 to explore the structural and ferroelectric…

材料科学 · 物理学 2014-02-20 Rishikesh Pandey , Braj Raj Meena , Akhilesh Kumar Singh

Structural properties, impedance, dielectric and electric modulus spectra have been used to investigate the sintering temperature (Ts) effect on the single phase cubic spinel Ni0.6Zn0.4Fe2O4 (NZFO) ceramics synthesized by standard ceramic…

材料科学 · 物理学 2016-10-19 M. A. Ali , M. N. I. Khan , F. -U. -Z. Chowdhury , S. Akhter , M. M. Uddin

In this work, we report the combined effect of donor (Nd) and acceptor (Li) co-doping at the Zn-site of ZnO ceramics on structural, microstructural and dielectric properties. Combining experimental observations with DFT based theoretical…

材料科学 · 物理学 2020-09-10 Md. Zahidur Rahaman , Hidekazu Tanaka , A. K. M. Akther Hossain

Laser nitriding represents a versatile approach for tailoring the surface properties of metals. Up to now, its effect on the superconducting response of niobium nitrides remains largely unexplored. In this work, the nitriding process of…

材料科学 · 物理学 2026-04-20 J. Frechilla , A. Frechilla , G. F. de la Fuente , A. Larrea , L. A. Angurel , E. Martínez

We report on the structure and dielectric properties of ternary A6B2O17 (A = Zr; B = Nb, Ta) thin films and ceramics. Thin films are produced via sputter deposition from dense, phase-homogenous bulk ceramic targets, which are synthesized…

Barium sodium niobate Ba$_2$NaNb$_5$O$_{15}$ (BNN) ceramics with different amounts of BaO-Na$_2$O-Nb$_2$O$_5$-P$_2$O$_5$ (BNNP) glass were prepared via the conventional solid-state method. The effect of glass content on the structural,…

Nanocrystalline metals and ceramics with <100 nm grain sizes and superior properties (e.g., mechanical strength, hardness, fracture toughness and stored dielectric energy) are of great interest. Much has been discussed about achieving nano…

材料科学 · 物理学 2020-11-10 Yanhao Dong , Hongbing Yang , Lin Zhang , Xingyu Li , Dong Ding , Xiaohui Wang , Ju Li , Jiangong Li , I-Wei Chen

Samples of $\alpha$-SiC have been sintered with liquid phase (LPS) to 1950 $^\circ$C, in atmosphere of argon and processing times between 1 and 7 hours. Using scanning electron microscopy (SEM) the microstructure of the samples has been…

Using the high-resolution x-ray diffraction (XRD) analysis, scanning electron microscopy (SEM), and the temperature-dependent microwave resonator characterization, structural properties, phase assemblage and dielectric properties of…

材料科学 · 物理学 2015-02-27 Kouros Khamoushi , Eero Arola

High-temperature and high-pressure experiments were conducted on columbite-type ZnNb2O6, reaching temperatures up to 873 K at ambient pressure and pressures up to 30 GPa at ambient temperature, respectively. Through systematic analysis…

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