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Magnetic nanoparticles (NP) of magnetite (Fe3O4) coated with oleic acid (OA) and dodecanoic acid (DA) were synthesized and investigated through Transmission Electron Microscopy (TEM),magnetization M, and ac magnetic susceptibility…

介观与纳米尺度物理 · 物理学 2010-04-14 V. B. Barbeta , R. F. Jardim , P. K. Kiyohara , F. B. Effenberger , L. M. Rossi

We report high-temperature (300-1120 K) magnetization data of Fe and Fe3O4 nanoparticles embedded in multi-walled carbon nanotubes. The magnetic impurity concerntations are precisely determined by both high-energy synchrotron x-ray…

强关联电子 · 物理学 2011-07-20 Guo-meng Zhao , Jun Wang , Yang Ren , Pieder Beeli

Magnetic measurements up to 1000 K have been performed on hydrothermally synthesized $\alpha$-Fe$_{2}$O$_{3}$ nanoparticles (60 nm) using a Quantum Design vibrating sample magnetometer. A high vacuum environment (1$\times$10$^{-5}$ torr)…

介观与纳米尺度物理 · 物理学 2015-05-20 Jun Wang , Wei Wu , Fan Zhao , Guo-meng Zhao

Iron oxide nano particles with nominal Fe2O3 stoichiometry were synthesized by a wet, soft chemical method with the heat treatment temperatures from 250{\deg}C to 900{\deg}C in air. The variation in the structural properties of the nano…

材料科学 · 物理学 2011-11-29 Debajeet K. Bora , Artur Braun , Selma Erat , Olga Safonova , Thomas Graule , Edwin C. Constable

The magnetic behavior of $Fe_{3-x}O_4$ nanoparticles synthesized either by high-temperature decomposition of an organic iron precursor or low-temperature co-precipitation in aqueous conditions, is compared. Transmission electron microscopy,…

Magnetic particle hyperthermia, in which colloidal nanostructures are exposed to an alternating magnetic field, is a promising approach to cancer therapy. Unfortunately, the clinical efficacy of hyperthermia has not yet been optimized.…

We present a study on the magnetic properties of naked and silica-coated Fe3O4 nanoparticles with sizes between 5 and 110 nm. Their efficiency as heating agents was assessed through specific power absorption (SPA) measurements as a function…

We report detailed studies on magnetic properties of Co3O4 nanoparticles of average size 12.5 nm. Temperature and field dependence of magnetization, wait time dependence of magnetic relaxation (aging), memory effects and temperature…

介观与纳米尺度物理 · 物理学 2010-09-03 Vijay Bisht , K. P. Rajeev

Heating magnetic nanoparticles with high frequency magnetic fields is a topic of interest for biological applications (magnetic hyperthermia) as well as for heterogeneous catalysis. This study shows why FeC NPs of similar structures and…

Fe2O3 nanoparticles of different sizes ranging from 22 to 56nm were synthesized chemically by a modified sol-gel method. Pure alpha phase particles as well as particles with admixture of alpha and gamma phase were obtained and identified by…

材料科学 · 物理学 2007-05-23 Shakeel Akbar , S. K. Hasanain , Nasia Azmat , M. Nadeem

Using microemulsion methods, CoO-Pt core-shell nanoparticles (NPs), with diameters of nominally 4 nm, were synthesized and characterized by high-resolution transmission electron microscopy (HRTEM) and a suite of x-ray spectroscopies,…

介观与纳米尺度物理 · 物理学 2014-03-25 Adriana Zelenakova , Vladimir Zelenak , Stefan Michalik , Jozef Kovac , Mark W. Meisel

In this work, the structural and magnetic properties of the gold-coated FePt nanoparticles synthesized from high-temperature solution phase are presented. The amount of gold was optimized to obtain most of the FePt particles coated. The…

材料科学 · 物理学 2009-11-26 P. de la Presa , M. Multigner , M. P. Morales , T. Rueda , E. Fernandez-Pinel , A. Hernando

We have studied the magnetic and power absorption properties of three samples of CoFe2O4 nanoparticles with sizes from 5 to 12 nm prepared by thermal decomposition of Fe (acac)3 and Co(acac)2 at high temperatures. The blocking temperatures…

材料科学 · 物理学 2011-03-22 T. E. Torres , A. G. Roca , M. P. Morales , A. Ibarra , C. Marquina , M. R. Ibarra , G. F. Goya

We prepared very high-coercivity cobalt ferrite nanoparticles using short-time high-energy mechanical milling. After the milling process, the coercivity of the nanoparticles reached 3.75 kOe - a value almost five times higher than that…

介观与纳米尺度物理 · 物理学 2015-06-19 E. F. Chagas , A. S. Ponce , R. J. Prado , G. M. Silva , J. Bettini , E. Baggio-Saitovitch

We describe a low-cost and simple setup for hyperthermia measurements on colloidal solutions of magnetic nanoparticles (ferrofluids) with a frequency-adjustable magnetic field in the range 5-500 kHz produced by an electromagnet. By…

材料科学 · 物理学 2008-10-09 L. -M. Lacroix , J. Carrey , M. Respaud

Co2FeAl (CFA) nanoparticles (NPs) of different sizes were synthesized by chemical route. The effect of the size of NPs upon the structure and magnetization compared to its bulk counterpart was investigated. The structure and composition…

强关联电子 · 物理学 2019-10-01 Aquil Ahmad , Srimanta Mitra , S. K. Srivastava , A. K. Das

Specific heat of the layered NaxCoO2 (x=0.65, 0.70 and 0.75) oxides has been measured in the temperature range of 3-360 K and magnetic field of 0 and 9 T. The analysis of data, assuming the combined effect of inter-layer superexchange and…

强关联电子 · 物理学 2009-11-11 A. Zorkovska , M. Orendac , J. Sebek , E. Santava , P. Svoboda , I. Bradaric , I. Savic , A. Feher

This work focuses on the microstructure, magnetic properties and magnetocaloric effect of CoFe$_2$O$_4$ (CFO) nanoparticles elaborated by sol-gel auto combustion method. The XRD investigation indicates that CFO is crystallized in a cubic…

We report about the magnetic properties of antiferromagnetic (AF) MnO nanoparticles (NPs) with different sizes (6-19nm). Using a combination of polarized neutron scattering and magnetometry we were able to resolve previously observed…

介观与纳米尺度物理 · 物理学 2017-04-26 X. Sun , A. Klapper , Y. Su , K. Nemkovski , A. Wildes , H. Bauer , O. Köhler , A. Schilmann , W. Tremel , O. Petracic , Th. Brückel

Magnetic nanoparticles are important building blocks for future technologies ranging from nano-medicine to spintronics. Many related applications require nanoparticles with tailored magnetic properties. However, despite significant efforts…

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