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We perform an experimental investigation of the synthesis of complex materials using the Laser-diode heated floating zone method (L-FZ). We will briefly introduce the Infrared-heated floating zone method of bulk crystal growth and then…

Materials Science · Physics 2021-03-10 Alemayehu S. Admasu , Durga Sankar Vavilapalli

High quality electron-doped HTSC single crystals of $\rm Pr_{2-x}Ce_{x}CuO_{4+\delta}$ and $\rm Nd_{2-x}Ce_{x}CuO_{4+\delta}$ have been successfully grown by the container-free traveling solvent floating zone technique. The optimally doped…

Materials Science · Physics 2010-10-18 Michael Lambacher , Toni Helm , Mark Kartsovnik , Andreas Erb

Single crystal growth of several rare earth hexaborides has been carried out by the floating zone technique. A high power Xenon arc lamp image furnace was used for the crystal growth. Large high quality crystals of LaB$_{6}$, CeB$_{6}$,…

Strongly Correlated Electrons · Physics 2009-11-10 G. Balakrishnan , M. R. Lees , D. McK. Paul

The interplay between unconventional superconductivity and quantum critical ferromagnetism in the U-Ge compounds represents an open problem in strongly correlated electron systems. Sample quality can have a strong influence on both of these…

We report a simple, reliable method to grow high quality BaFe$_{2-x}$Co$_x$As$_2$ single crystal samples without using any fluxing agent. The starting materials for the single crystal growth come from well-crystallized polycrystalline…

Superconductivity · Physics 2011-03-23 Changjin Zhang , Lei Zhang , Chuanying Xi , Langsheng Ling , Shun Tan , Yuheng Zhang

Polycrystalline Ba4NbIr3O12 has recently been shown to be a promising spin liquid candidate. We report an easy and reliable method to grow millimeter-sized single crystals of this trimer based spin liquid candidate material with the actual…

Materials Science · Physics 2020-04-24 Gohil S. Thakur , Sumanta Chattopadhyay , Thomas Doert , T. Herrmannsdörfer , Claudia Felser

Single crystals of superconducting KxFe2-ySe2 have been grown with the optical floating-zone technique under application of 8 bar of argon pressure. We found that large and high quality single crystals with dimensions of ~\varnothing6…

Superconductivity · Physics 2012-07-09 Y. Liu , Z. C. Li , W. P. Liu , G. Friemel , D. S. Inosov , R. E. Dinnebier , Z. J. Li , C. T. Lin

Incorporation of $\mathrm{Al_{y}Ga_{1-y}N}$ (AGN) semiconductors into high power electronics offers efficiency improvements in power transmission, generation, and use, if approaches to eliminate the defects arising from film-lattice…

The oscillating temperature technique was successfully employed to grow large and composition homogeneous CaFeAsF single crystals due to the reduction of nuclei number by temperature oscillation. The largest as-grown CaFeAsF single crystal…

Superconductivity · Physics 2022-03-02 Ming-Wei Ma , Binbin Ruan , Menghu Zhou , Yadong Gu , Qingsong Yang , Junnan Sun , Zhi-An Ren

A new approach to grow FeSe1-xTex single crystals with optical zone-melting technique was successfully employed. Crystals with actual composition 0.4 < x < 1.0 all show high crystallinity with no phase separation. The ability to visually…

Superconductivity · Physics 2009-11-16 K. W. Yeh , C. T. Ke , T. W. Huang , T. K. Chen , Y. L. Huang , P. M. Wu , M. K. Wu

Single crystals are essential for characterizing a wide range of magnetic states, including exotic ones such as quantum spin liquids. This study reports a flux method for growing single crystals of NdTa$_7$O$_{19}$, the first quantum spin…

Strongly Correlated Electrons · Physics 2025-05-13 Lia Šibav , Matic Lozinšek , Zvonko Jagličić , Tina Arh , Panchanana Khuntia , Andrej Zorko , Mirela Dragomir

We describe the crystal growth of high quality single crystals of the non-centrosymmetric superconductor, Ru7B3 by the floating zone technique, using an optical furnace equipped with xenon arc lamps. The crystals obtained are large and…

Superconductivity · Physics 2014-07-29 Ravi P. Singh , Natalia A. Parzyk , Martin R. Lees , Don McK Paul , Geetha Balakrishnan

Pyrochlore erbium titanate samples in the form of powders (with nominal compositions of Er2Ti2+xO7) and bulk single crystals were prepared to elucidate the effect of synthesis and growth conditions on their composition, structure, and…

Materials Science · Physics 2018-12-14 Q. Wang , A. Ghasemi , A. Scheie , S. M. Koohpayeh

High quality single crystals of BaFe$_{12}$O$_{19}$ were grown using the floating zone technique in flowing oxygen pressurized to 100 atm. Single crystal neutron diffraction was used to determine the nuclear and magnetic structure of…

Materials Science · Physics 2015-06-25 H. B. Cao , Z. Y. Zhao , M. Lee , E. S. Choi , M. A. McGuire , B. C. Sales , H. D. Zhou , J. -Q. Yan , D. G. Mandrus

Single crystals of the novel strontium osmate Sr3Os4O14 have been grown by the hydrothermal method using opposed anvil high-pressure and high-temperature technique. The reaction took place in sealed gold capsules at 3 GPa and a temperature…

Materials Science · Physics 2023-09-13 N. D. Zhigadlo

High-quality Bi$_{2+x}$Sr$_{2-x}$CuO$_{6+\delta}$(0$<$x$\leq$0.5) single crystals have been grown successfully using the travelling-solvent floating-zone(TSFZ) technique. The samples with $x >$ 0.05 are in the underdoped level. The…

Superconductivity · Physics 2009-11-11 Huiqian Luo , Lei Fang , Gang Mu , Hai-Hu Wen

We report on the synthesis and physical properties of cm-sized CoGeO$_3$ single crystals grown in a high pressure mirror furnace at pressures of 80~bar. Direction dependent magnetic susceptibility measurements on our single crystals reveal…

Materials Science · Physics 2021-04-07 L. Zhao , Z. Hu , H. Guo , C. Geibel , H. J. Lin , C. T. Chen , D. I. Khomskii , L. H. Tjeng , A. C. Komarek

A crack free and high structural quality Sr2Nb2O7 single crystals were grown by the optical float zone method using optimized growth parameters. Laue pattern confirms single crystalline nature of the grown crystal. Temperature dependent…

$\alpha$-TeO2 is widely used in acousto-optic devices due to its excellent physical properties. Conventionally, $\alpha$-TeO2 single crystals were grown using melt methods. Here, we report for the first time the growth of $\alpha$-TeO2…

Materials Science · Physics 2024-04-04 Lu Han , Chao Liu , Xiaoli Wang , Feiyu Li , Chuanyan Fan , Junjie Zhang

Terbium titanate (Tb$_2$Ti$_2$O$_7$) is a spin-ice material with remarkable magneto-optical properties. It has a high Verdet constant and is a promising substrate crystal for the epitaxy of quantum materials with the pyrochlore structure.…