High-quality Bi2+xSr2−xCuO6+δ(0<x≤0.5) single crystals have been grown successfully using the travelling-solvent floating-zone(TSFZ) technique. The samples with x> 0.05 are in the underdoped level. The structure of these crystals was investigated by X-ray diffraction. The evolution of c-axis lattice parameters with varied \emph{x} is displayed, which is strongly associated with the behavior of Tc. The crystals exhibit superconducting transitions with Tc=9 to 0.8 K for the samples with x=0.05 to 0.20, while for samples with x=0.25 and above no superconductivity was discovered down to 1.6 K. The resistivity of samples with x=0.31, 0.40 and 0.50 exhibits a drastic divergence as temperature approaches 0 K.
@article{arxiv.cond-mat/0611349,
title = {Growth and Characterization of Bi$_{2+x}$Sr$_{2-x}$CuO$_{6+\delta}$ Single Crystals},
author = {Huiqian Luo and Lei Fang and Gang Mu and Hai-Hu Wen},
journal= {arXiv preprint arXiv:cond-mat/0611349},
year = {2009}
}
Comments
6 pages,7 figures. submitted to Journal of Crystal Growth