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Related papers: KxFe2-ySe2 single crystals: Floating-zone growth, …

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Single crystals of K0.80Fe1.76Se2.02 were suscessfully grown from a ternary solution. We show that although crystals form when cooling a near stoichiometric melt, crystals are actually growing out of a ternary solution that remains liquid…

Superconductivity · Physics 2015-05-27 R. Hu , K. Cho , H. Kim , H. Hodovanets , W. E. Straszheim , M. A. Tanatar , R. Prozorov , S. L. Bud'ko , P. C. Canfield

Millimeter sized single crystals of CaFe$_{1-x}$Co$_x$AsF were grown using a self-flux method. It is found that high-quality single crystals can be grown from three approaches with different initial raw materials. The chemical compositions…

Superconductivity · Physics 2016-08-09 Yonghui Ma , Kangkang Hu , Qiucheng Ji , Bo Gao , Hui Zhang , Gang Mu , Fuqiang Huang , Xiaoming Xie

Single crystals of MgB2 with a size up to 1.5x0.9x0.2 mm3 have been grown with a high pressure cubic anvil technique. The crystal growth process is very peculiar and involves an intermediate nitride, namely MgNB9. Single crystals of BN and…

Single crystals of SrFe2-xPtxAs2 (0 < x < 0.36) were grown using the self flux solution method and characterized using x-ray crystallography, electrical transport, magnetic susceptibility, and specific heat measurements. The…

Superconductivity · Physics 2010-10-21 Kevin Kirshenbaum , Shanta R. Saha , Tyler Drye , Johnpierre Paglione

We report the successful growth of high quality single crystals of LiFeAs with lateral sizes up to 5 x 5 mm2 by the Sn-flux method. Electrical resistivity studies reveal that the superconducting onset temperature is 18.2 K with a transition…

Superconductivity · Physics 2010-10-20 Bumsung Lee , Seunghyun Khim , Jung Soo Kim , G. R. Stewart , Kee Hoon Kim

The optical properties of the iron-chalcogenide superconductor K{0.8}Fe{2-y}Se2, with a critical temperature Tc = 31 K, have been measured over a wide frequency range in the a-b planes above and below Tc. The conductivity is incoherent at…

Superconductivity · Physics 2012-05-28 C. C. Homes , Z. J. Xu , J. S. Wen , G. D. Gu

We have grown underdoped (x = 0.11, 0.12) and optimally doped (x = 0.16) La2-xSrxCuO4 (LSCO) crystals by traveling-solvent floating-zone (TSFZ) technique. In order to obtain LSCO single crystals of high quality, we have made much effort to…

Superconductivity · Physics 2009-01-23 Xiaoli Shen , Zhengcai Li , Caixia Shen , Wei Lu , Xiaoli Dong , Fang Zhou* , Zhongxian Zhao

Single crystals of Tl0.58Rb0.42Fe1.72Se2 are successfully grown with the superconducting transition temperatures Tconset=32K and Tczero=31.4K. The Hall coefficient exhibits a multi-band behavior, which is very similar to that of all other…

Superconductivity · Physics 2011-02-21 Hangdong Wang , Chihen Dong , Zujuan Li , Shasha Zhu , Qianhui Mao , Chunmu Feng , H. Q. Yuan , Minghu Fang

We report single crystal growth and a study of superconducting properties in Fe_{1+y}Te_{1-x}S_{x}. We demonstrate the smallest upper critical field anisotropy, gamma=H_{c2}^{//c}/H_{c2}^{//a}, among all iron based superconductors, the…

Superconductivity · Physics 2009-07-22 Rongwei Hu , J. B. Warren , C. Petrovic

We report significantly enhanced magnetic moment in K0.69(2)Fe1.45(1)Se2.00(1) single crystals with sharp Tc and bulk superconductivity obtained by postannealing and quenching process. There are two Fe sites in the…

Superconductivity · Physics 2012-07-02 Hyejin Ryu , Hechang Lei , A. I. Frenkel , C. Petrovic

High-quality Bi$_{2+x}$Sr$_{2-x}$CuO$_{6+\delta}$(0$<$x$\leq$0.5) single crystals have been grown successfully using the travelling-solvent floating-zone(TSFZ) technique. The samples with $x >$ 0.05 are in the underdoped level. The…

Superconductivity · Physics 2009-11-11 Huiqian Luo , Lei Fang , Gang Mu , Hai-Hu Wen

Single crystals of Ba0.6K0.4Fe2As2 with excellent quality have been successfully grown without fluxing agent through a simple one-step method for the first time. X-ray diffraction patterns demonstrate that the samples have high crystalline…

Superconductivity · Physics 2015-05-20 Chunlei Wang , Chao Yao , Lei Wang , Yanpeng Qi , Zhaoshun Gao , Dongliang Wang , Xianping Zhang , Yanwei Ma

We report single-crystal growth of La$_{0.34}$Na$_{0.66}$Fe$_2$As$_2$ iron-based superconductor with the size of several millimeters. The samples were accidentally obtained in trying to grow LaFeAsO$_{1-y}$F$_y$ ( $y \geq$ 0.8 ) single…

Superconductivity · Physics 2018-11-14 Yanhong Gu , Jia-Ou Wang , Xiaoyan Ma , Huiqian Luo , Youguo Shi , Shiliang Li

The single crystal growth and superconducting properties of PbTaSe2 with non-centrosymmetric crystal structure is reported. Using the chemical vapor transport (CVT) technique, PbTaSe2 crystallizes in a layered structure and the crystal…

Single crystal of La(O,F)BiSe2 was successfully grown for the first time by the CsCl flux method. Single crystal X-ray structural analysis clearly showed that La(O,F)BiSe2 crystalizes with space group P4/nmm (lattice parameters a =…

We study the relationship between precipitate morphology and superconductivity in KxFe1.6+ySe2 single crystals grown by self-flux method. Scanning electron microscopy (SEM) measurements revealed that superconducting phase forms a network in…

Superconductivity · Physics 2012-10-09 Y. Liu , Q. Xing , K. W. Dennis , R. W. McCallum , T. A. Lograsso

We report the single crystal growth and characterization of the highest Tc iron-based superconductor SmFeAsO1-xHx. Some sub-millimeter-sized crystals were grown using the mixture flux of Na3As + 3NaH + As at 3.0 GPa and 1473 K. The chemical…

Superconductivity · Physics 2017-09-12 Soshi Iimura , Takashi Muramoto , Satoru Fujitsu , Satoru Matsuishi , Hideo Hosono

Magnetic field penetration and magnetization hysteresis loops (MHLs) have been measured in KxFe2-ySe2 single crystals. The magnetic field penetration shows a two-step feature with a very small full-magnetic-penetration field (Hp1= 300 Oe at…

Superconductivity · Physics 2011-11-03 B. Shen , B. Zeng , G. F. Chen , J. B. He , D. M. Wang , H. Yang , H. H. Wen

Sizable single crystals of $BaFe_2As_2$ have been grown with self-flux method. The crystals are plate-like with c-axis perpendicular to the plane. The size can be as large as 3 x 5 x 0.2 $mm^3$. The resistivity anisotropy…

Superconductivity · Physics 2009-11-13 X. F. Wang , T. Wu , G. Wu , H. Chen , Y. L. Xie , J. J. Ying , Y. J. Yan , R. H. Liu , X. H. Chen

An extended study of the superconducting and normal-state properties of various as-grown and post-annealed RbxFe2-ySe2 single crystals is presented. Magnetization experiments evidence that annealing of RbxFe2-ySe2 at 413 K, well below the…