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In this paper we report the growth and superconductivity of $Na_xTaS_2$ crystals. The structural data deduced from X-ray diffraction pattern shows that the sample has the same structure as $2H-TaS_2$. A series of crystals with different…

Superconductivity · Physics 2009-11-11 L. Fang , Y. Wang , P. Y. Zou , L. Tang , Z. Xu , H. Chen , C. Dong , L. Shan , H. H. Wen

Superconducting Sm(O,F)BiS2 single crystals were successfully grown using KI-KCl flux. The obtained single crystals were flat-shaped and their size was 500um. The structure and composition of the obtained single crystals were obtained using…

We report the successful growth of high quality single crystals of LiFeAs with lateral sizes up to 5 x 5 mm2 by the Sn-flux method. Electrical resistivity studies reveal that the superconducting onset temperature is 18.2 K with a transition…

Superconductivity · Physics 2010-10-20 Bumsung Lee , Seunghyun Khim , Jung Soo Kim , G. R. Stewart , Kee Hoon Kim

Single crystals of SrFe2-xPtxAs2 (0 < x < 0.36) were grown using the self flux solution method and characterized using x-ray crystallography, electrical transport, magnetic susceptibility, and specific heat measurements. The…

Superconductivity · Physics 2010-10-21 Kevin Kirshenbaum , Shanta R. Saha , Tyler Drye , Johnpierre Paglione

Single crystal of Cu0.03TaS2 with low copper intercalated content was successfully grown via chemical iodine-vapor transport. The structural characterization results show that the copper intercalated 2H-Cu0.03TaS2 single crystal has the…

Superconductivity · Physics 2009-11-13 X. D. Zhu , Y. P. Sun , X. B. Zhu , X. Luo , B. S. Wang , G. Li , Z. R. Yang , W. H. Song , J. M. Dai

Centimeter sized platelet single crystals of KFe2As2 were grown using a self-flux method. An encapsulation technique using commercial stainless steel container allowed the stable crystal growth lasting for more than 2 weeks. Ternary K-Fe-As…

F-substituted NdOBiS2 superconducting single crystals were grown using CsCl/KCl flux. This is the first example of the single-crystal growth of a BiS2-based superconductor. The obtained single crystals had a plate-like shape with a size of…

We report single-crystal growth of La$_{0.34}$Na$_{0.66}$Fe$_2$As$_2$ iron-based superconductor with the size of several millimeters. The samples were accidentally obtained in trying to grow LaFeAsO$_{1-y}$F$_y$ ( $y \geq$ 0.8 ) single…

Superconductivity · Physics 2018-11-14 Yanhong Gu , Jia-Ou Wang , Xiaoyan Ma , Huiqian Luo , Youguo Shi , Shiliang Li

Millimeter sized single crystals of CaFe$_{1-x}$Co$_x$AsF were grown using a self-flux method. It is found that high-quality single crystals can be grown from three approaches with different initial raw materials. The chemical compositions…

Superconductivity · Physics 2016-08-09 Yonghui Ma , Kangkang Hu , Qiucheng Ji , Bo Gao , Hui Zhang , Gang Mu , Fuqiang Huang , Xiaoming Xie

Single crystals of undoped CaFe2As2 were grown by a FeAs self-flux method, and the crystals were quenched in ice-water rapidly after high temperature growth. The quenched crystal undergoes a collapsed tetragonal structural phase transition…

Superconductivity · Physics 2017-08-22 Dong-Yun Chen , Jia Yu , Bin-Bin Ruan , Qi Guo , Lei Zhang , Qing-Ge Mu , Xiao-Chuan Wang , Bo-Jin Pan , Gen-Fu Chen , Zhi-An Ren

Single crystals of SmFeAsO1-xFy of a size up to 120 micrometers have been grown from NaCl/KCl flux at a pressure of 30 kbar and temperature of 1350-1450 C using the cubic anvil high-pressure technique. The superconducting transition…

Superconductivity · Physics 2009-11-13 N. D. Zhigadlo , S. Katrych , Z. Bukowski , S. Weyeneth , R. Puzniak , J. Karpinski

Millimeter sized single crystals of KCa_2Fe_4As_4F_2 were grown using a self-flux method. The chemical compositions and crystal structure were characterized carefully. Superconductivity with the critical transition T_c = 33.5 K was…

Cd-doped La(O,F)BiS2 single crystals were grown using a CsCl/KCl flux. The grown crystals have a plate-like shape with ~1-2 mm square size in a well-developed ab-plane. The Cd doping in the crystals was successfully characterized by single…

Superconductivity · Physics 2017-06-16 Masanori Nagao , Masashi Tanaka , Satoshi Watauchi , Yoshihiko Takano , Isao Tanaka

High-quality Bi$_{2+x}$Sr$_{2-x}$CuO$_{6+\delta}$(0$<$x$\leq$0.5) single crystals have been grown successfully using the travelling-solvent floating-zone(TSFZ) technique. The samples with $x >$ 0.05 are in the underdoped level. The…

Superconductivity · Physics 2009-11-11 Huiqian Luo , Lei Fang , Gang Mu , Hai-Hu Wen

Single crystals of Ba0.6K0.4Fe2As2 with excellent quality have been successfully grown without fluxing agent through a simple one-step method for the first time. X-ray diffraction patterns demonstrate that the samples have high crystalline…

Superconductivity · Physics 2015-05-20 Chunlei Wang , Chao Yao , Lei Wang , Yanpeng Qi , Zhaoshun Gao , Dongliang Wang , Xianping Zhang , Yanwei Ma

An eutectic LiCl/KCl flux method in a horizontal configuration has been used to grow a series of homogeneous Fe$_{1+\delta}$Se$_{1-x}$Te$_x$ single crystals of high quality with 0.5 $\leq$ $x$ $\leq$ 1. Compared with previously used…

In this paper we present the single crystal growth of Fe0.95Se0.6Te0.4 high TC superconducting sample by the modified Bridgman technique. The x-ray diffraction pattern shows the single crystal nature of the sample, as only (00l) peaks are…

Superconductivity · Physics 2019-07-23 Anmol Shukla , Vishal K. Maurya , Rajendra S. Dhaka

F-substituted LaOBiSe2 single crystals were grown using CsCl flux. The obtained single crystals showed a plate-like shape with a size of about 1.0 mm square. The c-axis lattice constant of the grown crystals was determined to be 14.114(3)…

Superconductivity · Physics 2014-10-29 Masanori Nagao , Masashi Tanaka , Satoshi Watauchi , Isao Tanaka , Yoshihiko Takano

Millimeter-sized single crystals of LaFeAsO, LaFeAsO1-xFx, and LaFe1-xCoxAsO were grown in NaAs flux at ambient pressure. The detailed growth procedure and crystal characterizations are reported. The as-grown crystals have typical…

The single crystal of ThCr2Si2-type BaPd2As2 was successfully prepared by a self-flux method, and the crystal structure was characterized by X-ray diffraction method with the lattice parameters a = 4.489(2) {\AA} and c = 10.322(3) {\AA}.…

Superconductivity · Physics 2016-02-17 Qi Guo , Jia Yu , Bin-Bin Ruan , Dong-Yun Chen , Xiao-Chuan Wang , Qing-Ge Mu , Bo-Jin Pan , Gen-Fu Chen , Zhi-An Ren
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