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SrPt$_2$As$_2$ single crystals with CaBe$_2$Ge$_2$-type structure were synthesized by self-melting technique. X-ray diffraction, transmission electron microscopy, electrical resistivity, specific heat and optical spectroscopy measurements…

Superconductivity · Physics 2013-05-30 A. F. Fang , T. Dong , H. P. Wang , Z. G. Chen , B. Cheng , Y. G. Shi , P. Zheng , G. Xu , L. Wang , J. Q. Li , N. L. Wang

Co-doped iron arsenic single crystal of BaFe1.87Co0.13As2 with dimension up to 20 x 10 x 2 mm3 were grown by a nucleation pole: an alumina stick served as nucleation center during growth. The high quality of crystalline was illustrated by…

Superconductivity · Physics 2015-05-13 D. L. Sun , Y. Liu , J. T. Park , C. T. Lin

We report the successful growth of high quality single crystals of LiFeAs with lateral sizes up to 5 x 5 mm2 by the Sn-flux method. Electrical resistivity studies reveal that the superconducting onset temperature is 18.2 K with a transition…

Superconductivity · Physics 2010-10-20 Bumsung Lee , Seunghyun Khim , Jung Soo Kim , G. R. Stewart , Kee Hoon Kim

Measurements of the anisotropic properties of single crystals play a crucial role in probing the physics of new materials. Determining a growth protocol that yields suitable high-quality single crystals can be particularly challenging for…

Materials Science · Physics 2017-06-20 W. R. Meier , T. Kong , S. L. Bud'ko , P. C. Canfield

Millimeter sized single crystals of Mo3Sb7 are grown using the self-flux technique and a thorough characterization of their structural, magnetic, thermal and transport properties is reported. The structure parameters for the…

Superconductivity · Physics 2013-05-24 J. -Q. Yan , M. A. McGuire , A. F. May , H. Cao , A. D. Christianson , D. G. Mandrus , B. C. Sales

The growth of single crystals of MoS2 and WS2 by materials transport through a liquid salt flux made from a low melting mixture of NaCl and CsCl is described. The crystals are characterized by single crystal X-ray diffraction, which reveals…

Bismuth oxyselenide (Bi$_2$O$_2$Se) attracts great interest as a potential n-type complement to p-type thermoelectric oxides in practical applications. Previous investigations were generally focused on polycrystals. Here, we performed a…

Materials Science · Physics 2021-09-01 Jialu Wang , Wanghua Hu , Zhefeng Lou , Zhuokai Xu , Xiaohui Yang , Tao Wang , Xiao Lin

Single crystals of thallium-based cuprates with the general formula Tl$_{2}$Ba$_{2}$Ca$_{n-1}$Cu$_{n}$O$_{x}$(n=1,2,3) have been grown by the flux method. The superconducting transition temperatures determined by the ac magnetic…

Superconductivity · Physics 2009-11-11 Y. C. Ma , N. L. Wang

Superconducting whisker like and bulk single crystals of PrFeAs(O,F) were grown at 3 GPa and 1500 C from NaAs flux using the cubic anvil high pressure and high temperature technique. The ribbon shaped whisker like crystals were 400-1300…

Superconductivity · Physics 2013-11-08 N. D. Zhigadlo

Centimeter sized platelet single crystals of KFe2As2 were grown using a self-flux method. An encapsulation technique using commercial stainless steel container allowed the stable crystal growth lasting for more than 2 weeks. Ternary K-Fe-As…

In this letter, we report growth and characterization of bulk Bi2Se3 single crystals. The studied Bi2Se3 crystals are grown by self flux method through solid state reaction from high temperature (950C) melt of constituent elements and slow…

This work presents a comprehensive investigation of the structural, magnetic, and electronic properties of the double perovskite Ba$_2$CoMoO$_6$ (BCMO). Single crystals were grown via floating-zone and Czochralski techniques and…

Strongly Correlated Electrons · Physics 2026-03-17 A. R. N. Hanna , M. M. Ferreira-Carvalho , S. H. Chen , C. F. Chang , C. Y. Kuo , A. T. M. N. Islam , R. Feyerherm , L. H. Tjeng , B. Lake

We report the synthesis, and structural and physical properties of CaFe4As3 single crystals. Needle-like single crystals of CaFe4As3 were grown out of Sn flux and the compound adopts an orthorhombic structure as determined by X-ray…

Superconductivity · Physics 2015-05-27 A. B. Karki , G. T. McCandless , S. Stadler , Y. M. Xiong , J. Li , Julia Y. Chan , R. Jin

In Co$_x$NbSe$_2$, crystal symmetry, and cobalt site occupation drive the formation of two distinct magnetic phases. At $x = 1/4$, the centrosymmetric structure ($P$6$_3$/$mmc$) promotes Co-Co interactions leading to the formation of an…

Materials Science · Physics 2025-03-17 H. Cein Mandujano , Peter Y. Zavalij , Alicia Manjón-Sanz , Huibo Cao , Efrain E. Rodriguez

We report the single crystal growth of Ca(Fe1-xCox)2As2 (0 <= x <= 0.082) from Sn flux. The temperature-composition phase diagram is mapped out based on the magnetic susceptibility and electrical transport measurements. Phase diagram of…

Superconductivity · Physics 2015-06-03 Rongwei Hu , Sheng Ran , S. L. Bud'ko , W. E. Straszheim , P. C. Canfield

Single crystal of Cu0.03TaS2 with low copper intercalated content was successfully grown via chemical iodine-vapor transport. The structural characterization results show that the copper intercalated 2H-Cu0.03TaS2 single crystal has the…

Superconductivity · Physics 2009-11-13 X. D. Zhu , Y. P. Sun , X. B. Zhu , X. Luo , B. S. Wang , G. Li , Z. R. Yang , W. H. Song , J. M. Dai

The methodology of single crystal growth of metastable $\beta$-Ti alloy TIMETAL LCB in an optical floating zone furnace is presented in this paper. Chemical compositions of both precursor material and single crystals were checked. It was…

Materials Science · Physics 2018-03-21 Jana Šmilauerová , Jiří Pospíšil , Petr Harcuba , Václav Holý , Miloš Janeček

High-quality single crystals are essentially needed for the investigation of the novel bulk properties of unconventional superconductors. The availability of such crystals grown by the floating-zone method has helped to unveil the…

Superconductivity · Physics 2019-01-08 J. S. Bobowski , N. Kikugawa , T. Miyoshi , H. Suwa , S. Yonezawa , D. A. Sokolov , A. P. Mackenzie , Y. Maeno

Single crystals of mixed alkaline earth metal iron arsenide materials of Ba1-xSrxFe2As2 and Ba0.5Sr0.5(Fe1-yCoy)2As2 are synthesized via the self-flux method. Ba1-xSrxFe2As2 display spin-density wave features (TN) at temperatures…

We have grown intermetallic ErPd$_2$Si$_2$ single crystals employing laser-diodes with the floating-zone method. The temperature-dependent crystallography was determined using synchrotron and in-house X-ray powder diffraction measurements…

Materials Science · Physics 2022-08-02 Kaitong Sun , Yinghao Zhu , Si Wu , Junchao Xia , Pengfei Zhou , Qian Zhao , Chongde Cao , Hai-Feng Li