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The structural environment of substitutional Cr3+ ion in a natural pyrope Mg3Al2Si3O12 has been investigated by Cr K-edge Extended X-ray Absorption Fine Structure (EXAFS) and X-ray Absorption Near Edge Structure (XANES) coupled with…

Materials Science · Physics 2007-10-24 Amélie Juhin , Georges Calas , Delphine Cabaret , Laurence Galoisy , Jean-Louis Hazemann

X-ray absorption near edge structure (XANES) spectroscopy technique is used to better understand the charging and decharging processes of the persistent luminescence in the Cr$^{3+}$ doped AB$_2$O$_4$ spinels (A = Zn, Mg and B = Ga and Al)…

Materials Science · Physics 2015-06-30 Neelima Basavaraju , Kaustubh R. Priolkar , Didier Gourier , Aurélie Bessière , Bruno Viana

We determine the structural relaxations around paramagnetic impurities (Ti, Cr, Fe) in corundum (alpha-Al2O3), by combining x-ray absorption near edge structure (XANES) experiments and ab initio calculations. The structural relaxations are…

We have studied in this work the effect of increasing structural disorder on the persistent luminescence of Cr$^{3+}$ doped zinc gallate spinel. This disorder was introduced by progressive substitution of Zn$^{2+}$ by Mg$^{2+}$ ions, and…

The angular dependence (x-ray linear dichroism) of the Cr K pre-edge in MgAl2O4:Cr3+ spinel is measured by means of x-ray absorption near edge structure spectroscopy (XANES) and compared to calculations based on density functional theory…

Neutron and X-ray diffraction, magnetic susceptibility, and specific heat measurements have been used to investigate the magnetic and structural phase transitions of the spinel system Fe1+xCr2-xO4(0.0<=x<=1.0). The temperature versus Fe…

Dynamical properties of the lattice structure was studied by optical spectroscopy in ACr2O4 chromium spinel oxide magnetic semiconductors over a broad temperature region of T=10-335K. The systematic change of the A-site ions (A=Mn, Fe, Co,…

Strongly Correlated Electrons · Physics 2013-07-24 V. Kocsis , S. Bordács , D. Varjas , K. Penc , A. Abouelsayed , C. A. Kuntscher , K. Ohgushi , Y. Tokura , I. Kézsmárki

The crystal and magnetic structures of stoichiometric ZnCr2Se4 have been investigated using synchrotron X-ray and neutron powder diffraction, muon spin relaxation (muSR) and inelastic neutron scattering. Synchrotron X-ray diffraction shows…

Strongly Correlated Electrons · Physics 2017-04-12 P. Zajdel , W-Y. Li , W. Van Beek , A. Lappas , A. Ziolkowska , S. Jaskiewicz , C. Stock , M. A. Green

Recent experimental studies on Fe substituted spinel CoCr$_{2}$O$_{4}$ have discovered multiple functional properties in the system such as temperature and composition dependent magnetic compensation, tunable exchange bias and…

Materials Science · Physics 2018-08-29 Debashish Das , Subhradip Ghosh

The phase stability of the MgMn2O4 spinel has been studied by means of high-pressure X-ray diffraction for pressures up to 30 GPa. Two samples with different inversion degrees have been considered. Both spinels undergo a phase transition…

Materials Science · Physics 2009-11-10 Lorenzo Malavasi , Cristina Tealdi , Monica Amboage , M. Cristina Mozzati , Giorgio Flor

The difference in colour between emerald (Be3Si6Al2O18:Cr3+, green) and the Cr3+-doped spinel MgAl2O4 (red) is striking, considering that in both systems colour is due to CrO69- complexes with D3 symmetry and the measured Cr3+-O2- distance…

Materials Science · Physics 2008-05-22 J. M. Garcia-Lastra , M. T. Barriuso , J. A. Aramburu , M. Moreno

The non-equilibrium cation site occupancy in nanosized zinc ferrites (6-13 nm) with different degree of inversion (0.2 to 0.4) was investigated using Fe and Zn K-edge x-ray absorption spectroscopy XANES and EXAFS, and magnetic measurements.…

The iron arsenide Sr2CrO3FeAs with the tetragonal Sr2GaO3CuS-type structure was synthesized and its crystal structure re-determined by neutron powder diffraction. In contrast to previous X-ray crystallographic studies, a mixed occupancy of…

Superconductivity · Physics 2010-02-24 Marcus Tegel , Franziska Hummel , Yixi Su , Tapan Chatterji , Michela Brunelli , Dirk Johrendt

We report that small amounts of metal atom non-stoichiometry are possible in the ZnCr2O4 and MgCr2O4 spinels. The non-stoichiometry, though less than 2%, significantly impacts TN and the nature of the magnetic correlations above TN. The…

Materials Science · Physics 2015-05-20 S. E. Dutton , Q. Huang , O. Tchernyshyov , C. L. Broholm , R. J. Cava

The normal spinel oxide MgCr2O4 is cubic at room temperature while the normal spinel CuCr2O4 is tetragonal as a consequence of the Jahn-Teller nature of Cu2+ on the tetrahedral sites. Despite different end-member structures, complete solid…

Materials Science · Physics 2010-12-16 Daniel P. Shoemaker , Ram Seshadri

muSR experiments on the geometrically frustrated spinel oxide, Li2Mn2O4, show the development of spin correlations over a range of length scales with decreasing temperature. Increased relaxation below 150 K is consistent with the onset of…

Strongly Correlated Electrons · Physics 2009-11-11 C. R. Wiebe , P. L. Russo , A. T. Savici , Y. J. Uemura , G. J. MacDougall , G. M. Luke , S. Kuchta , J. E. Greedan

The structural and magnetic properties of spinel compounds $CoB_2O_4$ (B=Cr,Mn and Fe) are studied using the DFT+U method and generalized gradient approximation (GGA). We concentrate on understanding the trends in the properties of these…

Strongly Correlated Electrons · Physics 2016-09-21 Debashish Das , Rajkumar Biswas , Subhradip Ghosh

CuAl2O4 is a normal spinel oxide having quantum spin, S=1/2 for Cu2+. It is a rather unique feature that the Cu2+ ions of CuAl2O4 sit at a tetrahedral position, not like the usual octahedral position for many oxides. At low temperatures, it…

Using density functional calculations, we examine insertion/extraction of Mg ions in Mg3Bi2, an interesting Mg-ion battery anode. We found that a (1 1 0) facet is the most stable termination. Vacating a Mg2+ ion from the octahedral site is…

Materials Science · Physics 2022-09-26 M. Hussein N. Assadi , Christopher J. Kirkham , Ikutaro Hamada , Dorian A. H. Hanaor

We have employed first-principles electronic structure calculations to examine the hypothetical (but plausible) oxide spinel, LiCr2O4 with the d^{2.5} electronic configuration. The cell (cubic) and internal (oxygen position) structural…

Materials Science · Physics 2009-11-10 Markus Lauer , Roser Valenti , H. C. Kandpal , Ram Seshadri , .
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