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We have produced synthetic analogues of cosmic silicates using the Sol Gel method, producing amorphous silicates of composition Mg(x)Ca(1-x)SiO3. Using synchrotron X-ray powder diffraction on Beamline I11 at the Diamond Light Source,…

Earth and Planetary Astrophysics · Physics 2015-06-12 S. J. Day , S. P. Thompson , A. Evans , J. E. Parker

X-ray diffraction with high spatial resolution is commonly used to characterize (poly-)crystalline samples with, for example, respect to local strain, residual stress, grain boundaries and texture. However, the investigation of highly…

Over the past two decades synchrotron facilities dedicated to the generation of x-rays for study of atoms, molecules and condensed matter have proliferated all over the world. As a result of the special properties of x-rays produced by…

Statistical Mechanics · Physics 2009-09-29 Oleg G. Shpyrko

We present the development, manufacturing and performance of spherically bent crystal analyzers (SBCAs) of 100 mm diameter and 0.5 m bending radius. The elastic strain in the crystal wafer is partially released by a "strip-bent" method…

Instrumentation and Detectors · Physics 2017-01-25 Mauro Rovezzi , Christophe Lapras , Alain Manceau , Pieter Glatzel , Roberto Verbeni

Synchrotron X-ray diffraction measurements have been conducted on aqueous mixtures of propan-2-ol (a.k.a. isopropanol, or 2-propanol), for alcohol contents between 10 and 90 molar %, from room temperature down to 230 K. Molecular dynamics…

The characterization of the wetting on superhydrophobic surfaces is rather complex. Usual contact angle experiments are difficult to perform and the lateral movement of droplets as well as the pinning at point defects on the surface can…

In this study, we investigate the use of hyperspectral imaging (HSI) to inspect the formation of corrosion products on galvanised carbon steel samples. Ten samples were subjected to an accelerated corrosion test with different exposure…

Optics · Physics 2022-06-24 Thomas De Kerf , Zohreh Zahiri , Paul Scheunders , Steve Vanlanduit

We present results of analysis of physical conditions (number density, intensity of UV field, kinetic temperature) in the cold H$_2$-bearing interstellar medium of local and high redshift galaxies. Our measurements based on the fit to the…

Astrophysics of Galaxies · Physics 2020-10-07 V. V. Klimenko , S. A. Balashev

Vanadium oxide films and fibers have been fabricated by the acetylacetonate sol-gel method followed by annealing in wet nitrogen. The samples are characterized by X-ray diffraction and electrical conductivity measurements. The effects of a…

We present x-ray reflectivity and diffuse scattering measurements from the liquid surface of pure potassium. They strongly suggest the existence of atomic layering at the free surface of a pure liquid metal with low surface tension. Prior…

Statistical Mechanics · Physics 2007-05-23 Oleg Shpyrko , Patrick Huber , Peter S. Pershan , Holger Tostmann , Alexei Grigoriev , Ben Ocko , Moshe Deutsch

Recent cutting-edge experiments have provided {\it in situ} structure characterization and measurements of the pressure ($P$), density ($\bar{\rho}$) and temperature ($T$) of shock compressed silicon in the 100 GPa range of pressures and…

Materials Science · Physics 2024-12-12 M. W. C. Dharma-wardana , Dennis D. Klug , Hannah Poole , G. Gregori

Hydrocarbons are observed in the gas or solid phases of solar system objects, including comets, Trans-Neptunian Objects, planets and their moons. In the presence of water ice in these environments, hydrocarbons-bearing clathrate hydrates…

Earth and Planetary Astrophysics · Physics 2021-04-28 Emmanuel Dartois

The crystal structure and chemical bonding of magnetron-sputtering deposited nickel carbide Ni$_{1-x}$C$_{x}$ (0.05$\leq$x$\leq$0.62) thin films have been investigated by high-resolution X-ray diffraction, transmission electron microscopy,…

Materials Science · Physics 2014-09-23 Andrej Furlan , Jun Lu , Lars Hultman , Ulf Jansson , Martin Magnuson

Synchrotron X-ray diffraction experiments and molecular dynamics simulations have been performed on simple aliphatic aldehydes, from propanal to nonanal. The performance of the OPLS all-atom interaction potential model for aldehydes has…

Chemical Physics · Physics 2018-11-27 Ildikó Pethes , László Temleitner , Matija Tomšič , Andrej Jamnik , László Pusztai

The structure of the recently identified metastable ice XVII, obtained by release of hydrogen from the C$_0$ D$_2$O-H$_2$ compound (filled ice), has been accurately measured by neutron powder diffraction. The diffraction pattern is indexed…

The crystal structure and oxygen stoichiometry in two-layer Na0.74CoO2 and Na0.38CoO2 at room temperature are analyzed by powder neutron diffraction. Two sets of diffraction data for each sample, taken at different incident neutron…

Strongly Correlated Electrons · Physics 2009-11-11 L. Viciu , Q. Huang , R. J. Cava

Oxide Y2.5Nd0.5Al5O12 (YAG:Nd) with garnet structure was synthesized in the powder and ceramics forms. Fine-grained YAG:Nd ceramics with a relative density of ~99% were obtained by the Spark Plasma Sintering method (SPS). The radiation…

First-principles calculations using the plane-wave pseudopotential method within the generalized gradient approximation method were performed to study the pressure dependence of the structural, elastic, electronic and optical properties for…

Materials Science · Physics 2021-12-21 M. Radjai , A. Bouhemadou , D. Maouche

Thermal behaviors of hydroxypropyl cellulose dilute aqueous solutions with impurities of Group~I alkali metal ions (Li, Na, K, Rb and Cs chlorides) has been studied by means of static and dynamic light scattering measurements. From the…

Soft Condensed Matter · Physics 2025-04-08 Valery I. Kovalchuk

Detection of molecules using infrared spectroscopy probes the conditions and compositions of exoplanet atmospheres. Water (H2O), methane (CH4), carbon dioxide (CO2), and carbon monoxide (CO) have been detected in two hot Jupiters. These…