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A neutron powder diffraction study has been carried out on Pb(Zr0.52Ti0.48)O3 in order to resolve an ongoing controversy about the nature of the low-temperature structure of this strongly-piezoelectric and technologically-important…

Materials Science · Physics 2009-11-10 D. E. Cox , B. Noheda , G. Shirane

We report a comprehensive study of dc susceptibility, specific heat, neutron diffraction, and inelastic neutron scattering measurements on polycrystalline Ba3(Cr1-xVx)2O8 samples, where x=0, 0.06, 0.15, and 0.53. A Jahn-Teller structure…

Materials Science · Physics 2013-05-02 Tao Hong , L. Y. Zhu , X. Ke , V. O. Garlea , Y. Qiu , Y. Nambu , H. Yoshizawa , M. Zhu , G. E. Granroth , A. T. Savici , Zheng Gai , H. D. Zhou

We performed neutron powder diffraction measurements on the as-sintered (AS) and oxygen-reduced (OR) La$_{1.8}$Eu$_{0.2}$CuO$_{4+\alpha-\delta}$ (LECO). The structural parameters for oxygens in AS and OR samples refined by the Rietveld…

We have determined the crystal structures and superconducting transition temperatures of La1.48Nd0.4Sr0.12CuO4 under nearly hydrostatic pressures in diamond anvil cells to 5.0 GPa and 19.0 GPa, respectively. Synchrotron x-ray powder…

Bulk superconductor samples of YBa2Cu3-xCoxO7-{\delta} with x = 0, 0.01, 0.03, 0.05 are synthesized by solid-state reaction route. Both x-ray diffraction and electron microscopy have been employed to study the phase identification,…

Superconductivity · Physics 2011-07-07 Sushant Gupta , R. S. Yadav , N. P. Lalla , G. D. Verma , B. Das

A structural transition at $T\approx 322$ K from the $Pmmm$ to $Pmma$ phase is found to coincide with an anomaly of resistivity. Another structural phase transition doubling the lattice parameter $c$, which has been postulated earlier to…

Small angle neutron diffraction experiments are analyzed using recently developed and properly generalized one-field effective free energy method. In the case of experiment of Keimer et al on YBCO, we show that the fourfold symmetry of the…

Superconductivity · Physics 2009-10-30 D. Chang , C. -Y. Mou , B. Rosenstein , C. L. Wu

The temperature (T) dependent x-ray diffraction (XRD) and resistivity measurements of La0.175Pr0.45Ca0.375MnO3 (LPCMO) have been performed down to 2K to understand the structural and transport properties. From room temperature down to 220K,…

Materials Science · Physics 2016-06-22 Shivani Sharma , Aga Shahee , Kiran Singh , N. P. Lalla

We report the structural, magnetic, and magnetocaloric properties of Co$_2$Cr$_{1-x}$Ti$_x$Al ($x=$ 0--0.5) Heusler alloys for spintronic and magnetic refrigerator applications. Room temperature X-ray diffraction and neutron diffraction…

Materials Science · Physics 2019-11-06 Priyanka Nehla , Yousef Kareri , Guru Dutt Gupt , James Hester , P. D. Babu , Clemens Ulrich , R. S. Dhaka

The structure and physical properties of the Zr-stabilized, nonstoichiometric molybdenum diboride superconductor are reported. Good quality material of the diboride structure type can only be obtained by partial substitution of Zr for Mo,…

Superconductivity · Physics 2009-11-07 L. E. Muzzy , M. Avdeev , G. Lawes , M. K. Haas , H. W. Zandbergen , A. P. Ramirez , J. D. Jorgensen , R. J. Cava

The crystal structure of the candidate topological superconductor Cu$_x$Bi$_2$Se$_3$ was studied by single-crystal neutron diffraction using samples obtained by inserting the Cu dopant electrochemically. Neither structural refinements nor…

Superconductivity · Physics 2022-03-24 Tobias Fröhlich , Zhiwei Wang , Mahasweta Bagchi , Anne Stunault , Yoichi Ando , Markus Braden

We present x-ray powder diffraction (XRPD) and neutron diffraction measurements on the slightly underdoped iron pnictide superconductor Ba(1-x)K(x)Fe2As2, Tc = 32K. Below the magnetic transition temperature Tm = 70K, both techniques show an…

We have grown intermetallic ErPd$_2$Si$_2$ single crystals employing laser-diodes with the floating-zone method. The temperature-dependent crystallography was determined using synchrotron and in-house X-ray powder diffraction measurements…

Materials Science · Physics 2022-08-02 Kaitong Sun , Yinghao Zhu , Si Wu , Junchao Xia , Pengfei Zhou , Qian Zhao , Chongde Cao , Hai-Feng Li

DC and ac magnetization, resistivity, specific heat, and neutron diffraction data reveal that stoichiometric LaOFeP is metallic and non-superconducting above T = 0.35 K, with gamma = 12.5 mJ/mol*K. Neutron diffraction data at room…

Superconductivity · Physics 2008-08-11 T. M. McQueen , M. Regulacio , A. J. Williams , Q. Huang , J. W. Lynn , Y. S. Hor , D. V. West , M. A. Green , R. J. Cava

Single crystal neutron diffraction is used to investigate the magnetic and structural phase diagram of the electron doped superconductor Ba(Fe$_{1-x}$Co$_x$)$_2$As$_2$. Heat capacity and resistivity measurements have demonstrated that Co…

We present local structural evidence supporting the presence of charge inhomogeneities in the CuO2 planes of underdoped La2-xSrxCuO4. High-resolution atomic pair distribution functions have been obtained from neutron powder diffraction data…

Superconductivity · Physics 2016-08-31 E. S. Bozin , G. H. Kwei , H. Takagi , S. J. L. Billinge

Using high-energy diffraction we show that a 4-unit-cell superstructure, q0=(1/4,0,0), along the shorter Cu-Cu bonds coexists with superconductivity in optimally doped YBCO. A complex set of anisotropic atomic displacements on neighboring…

Superconductivity · Physics 2009-11-10 Zahirul Islam , X. Liu , S. K. Sinha , J. C. Lang , S. C. Moss , D. Haskel , G. Srajer , P. Wochner , D. R. Lee , D. R. Haeffner , U. Welp

We report the results of our investigations on a polycrystalline sample of Lu$_2$Ir$_3$Si$_5$ which crystallizes in the U$_2$Co$_3$Si$_5$ type structure (Ibam). These investigations comprise powder X-ray diffraction, magnetic…

Strongly Correlated Electrons · Physics 2017-07-26 Yogesh Singh , Dilip Pal , S. Ramakrishnan , A. M. Awasthi , S. K. Malik

We report a neutron and Raman scattering study of a single-crystal of La(2)CuO(4.05) prepared by high temperature electrochemical oxidation. Elastic neutron scattering measurements show the presence of two phases, corresponding to the two…

The cuprate superconductors are among the most widely studied quantum materials, yet there remain fundamental open questions regarding their electronic properties and the role of the structural degrees of freedom. Recent neutron and x-ray…