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Transition metal oxides have been attracted much attention in thermoelectric community from the last few decades. In the present work, we have synthesized LaNiO$_{3}$ by a simple solution combustion process. To analyze the crystal structure…

Materials Science · Physics 2022-02-02 Arzena Khatun , Shamim Sk , Sudhir K. Pandey

Phase-separated manganites provide a unique platform to study the dynamics of competing electronic and structural orders in correlated systems. In La0.275Pr0.35Ca0.375MnO3 (LPCMO), we use temperature-cycling Raman spectroscopy to uncover a…

SrTiO$_3$ thin films were used as a model system to study the effects of strain and epitaxial constraint on structural phase transitions of perovskite films. The basic phenomena revealed will apply to a variety of important structural…

Other Condensed Matter · Physics 2007-05-23 Feizhou He , B. O. Wells , S. M. Shapiro

We used low-temperature synchrotron x-ray diffraction to investigate the structural phase transitions of Fe1+yTe in the vicinity of a tricitical point in the phase diagram. Detailed analysis of the powder diffraction patterns and…

Superconductivity · Physics 2013-10-03 Cevriye Koz , Sahana Rößler , Alexander A. Tsirlin , Steffen Wirth , Ulrich Schwarz

We have investigated heteroepitaxial films of Sm-doped BiFeO3 with a Sm-concentration near a morphotropic phase boundary. Our high-resolution synchrotron X-ray diffraction, carried out in a temperature range of 25C to 700C, reveals…

Materials Science · Physics 2015-05-18 S. B. Emery , C. -J. Cheng , D. Kan , F. J. Rueckert , S. P. Alpay , V. Nagarajan , I. Takeuchi , B. O. Wells

High-entropy spinel oxides provide an excellent platform for investigating entropy-stabilized correlated systems with strong configurational disorder. In this work, we systematically study the temperature evolution of the structural and…

In this Letter we report high-resolution synchrotron X-ray powder diffraction and transmission electron microscope analysis of Mn-substituted LaFeAsO samples, demonstrating that a static incommensurate modulated structure develops across…

Superconductivity · Physics 2017-02-08 A. Martinelli , P. Manfrinetti , A. Provino , A. Genovese , F. Caglieris , G. Lamura , C. Ritter , M. Putti

Predicting solid-solid phase transitions remains a long-standing challenge in materials science. Solid-solid transformations underpin a wide range of functional properties critical to energy conversion, information storage, and thermal…

Materials Science · Physics 2025-06-03 Cibrán López , Joshua Ojih , Ming Hu , Josep Lluis Tamarit , Edgardo Saucedo , Claudio Cazorla

The elastic and magnetic properties, thermodynamical stability, deviation from stoichiometry and order/disorder transformations of phases that are relevant to Be alloys were investigated using density functional theory simulations coupled…

Materials Science · Physics 2015-04-01 Patrick A. Burr , Simon C. Middleburgh , Robin W. Grimes

Highly-strained BiFeO3 exhibits a "tetragonal-like, monoclinic" crystal structure found only in epitaxial films (with an out-of-plane lattice parameter exceeding the in-plane value by >20%). Previous work has shown that this phase is…

Materials Science · Physics 2011-08-17 Wolter Siemons , Michael D. Biegalski , Joong Hee Nam , Hans M. Christen

Layered three-dimensional centrosymmetric crystals can exhibit characteristics of noncentrosymmetric materials. This happens when each individual layer alone lacks inversion, but, when combined, inversion symmetry is restored; hence the…

Superconductivity · Physics 2021-11-01 David Möckli , Aline Ramires

A series of new Cr$_{5+x}$Mo$_{35-x}$W$_{12}$Re$_{35}$Ru$_{13}$C$_{20}$ high-entropy alloys (HEAs) have been synthesized and characterized by x-ray diffraction, scanning electron microscopy, electrical resistivity, magnetic susceptibility…

Superconductivity · Physics 2023-02-14 Guorui Xiao , Wuzhang Yang , Qinqing Zhu , Shijie Song , Guang-han Cao , Zhi Ren

We report a density functional theory plus dynamical mean field theory (DFT+DMFT) study of an oxide heterostructure of LaNiO$_3$ (LNO) bilayers in [111] direction interleaved with four atomic monolayers of LaAlO$_3$. DFT+$U$ optimizations…

Strongly Correlated Electrons · Physics 2019-09-20 Oleg Janson , Karsten Held

Up to now the crystallographic structure of the magnetoelectric perovskite EuTiO3 was considered to remain cubic down to low temperature. Here we present high resolution synchrotron X-ray powder diffraction data showing the existence of a…

Oxide heterostructures are of great interest both for fundamental and applicative reasons. In particular the two-dimensional electron gas at the LaAlO$_3$/SrTiO$_3$ or LaTiO$_3$/SrTiO$_3$ interfaces displays many different physical…

Mesoscale and Nanoscale Physics · Physics 2016-01-20 N. Scopigno , D. Bucheli , S. Caprara , J. Biscaras , N. Bergeal , J. Lesueur , M. Grilli

In this work, density functional theory (DFT) based calculations were performed to compute the physical properties (structural stability, mechanical behavior, electronic, thermodynamic, and optical properties) of synthesized MAX phases…

Materials Science · Physics 2023-06-22 J. Islam , M. D. Islam , M. A. Ali , H. Akter , A. Hossain , M. Biswas , M. M. Hossain , M. M. Uddin , S. H. Naqib

The recent discovery of superconductivity with relatively high transition temperature Tc in the layered iron-based quaternary oxypnictides La[ O1-xFx] FeAs was a real surprise. The excitement generated can be seen by the number of…

The orthorhombic phase of Si-doped Fe carbide is synthesized at high pressures and temperatures using laser-heated diamond anvil cell (LHDAC), followed by its characterization using X-ray diffraction (XRD) measurements, Transmission…

Materials Science · Physics 2020-11-17 Pinku Saha , Konstantin Glazyrin , Goutam Dev Mukherjee

Multiferroic bismuth ferrite Bi_2Fe_4O_9 (BFO) ceramic was synthesized by conventional solid state reaction route. X-ray diffraction and Rietveld refinement show formation of single phase ceramic with orthorhombic crystal structure (space…

Materials Science · Physics 2016-05-06 S. R. Mohapatra , B. Sahu , T. Badapanda , M. S. Pattanaik , S. D. Kaushik , A. K. Singh

Phase diagrams of [001] and [110] field-cooled (FC) (1-x)Pb(Mg1/3Nb2/3O3)-xPbTiO3 or PMN-xPT crystals have been constructed, based on high-resolution x-ray diffraction data. Comparisons reveal several interesting findings. First, a region…

Materials Science · Physics 2009-11-11 Hu Cao , Jiefang Li