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Single crystal growth of {\alpha}-Na$_x$MnO$_2$ (x = 0.90) is reported via the floating zone technique. The conditions required for stable growth and intergrowth-free crystals are described along with the results of trials under alternate…

CuFeO$_2$ single crystals up to 50 mm in length and up to 10 mm in diameter were grown by the optical floating-zone method. Stoichiometric polycrystalline rods with a diameter of 6-12 mm were used as feed materials to produce crystals of…

Materials Science · Physics 2020-01-07 Nora Wolff , Tobias Schwaigert , Dietmar Siche , Darrell G. Schlom , Detlef Klimm

Mm-sized LiMn$_{1-x}$Fe$_x$PO$_4$ single crystals with $0\leq x \leq 1$ were grown by means of the traveling floating-zone technique at elevated Argon pressure of 30~bar. For the various doping levels, the growth process was optimized with…

Strongly Correlated Electrons · Physics 2017-02-07 Christoph Neef , Hubert Wadepohl , Hans-Peter Meyer , Rüdiger Klingeler

We report the optimized conditions for growing the high quality single crystals of candidate quantum spin-ice Pr2Hf2O7 using the optical floating-zone method. Large single crystals of Pr2Hf2O7 have been grown under different growth…

Strongly Correlated Electrons · Physics 2019-01-02 V. K. Anand , A. T. M. N. Islam , A. Samartzis , J. Xu , N. Casati , B. Lake

We report the growth of mm-sized Pmnb-Li2FeSiO4 single crystals by means of the optical floating-zone method at high argon pressure and describe the conditions required for a stable growth process. The crystal structure is determined and…

We have grown underdoped (x = 0.11, 0.12) and optimally doped (x = 0.16) La2-xSrxCuO4 (LSCO) crystals by traveling-solvent floating-zone (TSFZ) technique. In order to obtain LSCO single crystals of high quality, we have made much effort to…

Superconductivity · Physics 2009-01-23 Xiaoli Shen , Zhengcai Li , Caixia Shen , Wei Lu , Xiaoli Dong , Fang Zhou* , Zhongxian Zhao

The floating zone technique is a well-established single crystal growth method in materials research, able to produce volumetrically large specimens with extremely high purities. However, traditional furnace designs have relied on heating…

Materials Science · Physics 2019-04-25 Julian L. Schmehr , Michael Aling , Eli Zoghlin , Stephen D. Wilson

We perform an experimental investigation of the synthesis of complex materials using the Laser-diode heated floating zone method (L-FZ). We will briefly introduce the Infrared-heated floating zone method of bulk crystal growth and then…

Materials Science · Physics 2021-03-10 Alemayehu S. Admasu , Durga Sankar Vavilapalli

The availability of large high-quality single crystals is an important prerequisite for many studies in solid-state research. The optical floating-zone technique is an elegant method to grow such crystals, offering potential to prepare…

A floating zone furnace is a powerful tool for single crystal growth. Here, we report the floating zone furnace using a high power diode laser of 1kW composed of five 200 Watt heating beams. The five beams with the designed irradiation…

Strongly Correlated Electrons · Physics 2019-12-20 Yoshio Kaneko , Yoshinori Tokura

We present a route to grow single crystals of Ba$_{0.9}$Sr$_{0.1}$CuSi$_{2}$O$_{6}$ suitable for inelastic neutron studies via the floating zone technique. Neutron single crystal diffraction was utilized to check their bulk quality and…

Materials Science · Physics 2019-07-02 Pascal Puphal , Stephan Allenspach , Christian Rüegg , Ekaterina Pomjakushina

We report a study on the crystal growth of the hexagonal manganites $R$MnO$_3$ ($R$ = Y, Lu, Ho, Er, and Tm) by using an optical floating-zone method. It was found that high-quality single crystals of $R$ = Y, Lu, and Ho could be easily…

Strongly Correlated Electrons · Physics 2015-06-17 C. Fan , Z. Y. Zhao , J. D. Song , J. C. Wu , F. B. Zhang , X. F. Sun

We report on single crystal growth of laser material Nd:YAG widely used in the applications by innovative crucible-free floating zone method implemented in an advanced laser optical furnace. We have optimized the parameters for the…

High-quality Bi$_{2+x}$Sr$_{2-x}$CuO$_{6+\delta}$(0$<$x$\leq$0.5) single crystals have been grown successfully using the travelling-solvent floating-zone(TSFZ) technique. The samples with $x >$ 0.05 are in the underdoped level. The…

Superconductivity · Physics 2009-11-11 Huiqian Luo , Lei Fang , Gang Mu , Hai-Hu Wen

High-quality single crystals are essentially needed for the investigation of the novel bulk properties of unconventional superconductors. The availability of such crystals grown by the floating-zone method has helped to unveil the…

Superconductivity · Physics 2019-01-08 J. S. Bobowski , N. Kikugawa , T. Miyoshi , H. Suwa , S. Yonezawa , D. A. Sokolov , A. P. Mackenzie , Y. Maeno

We report the growth of YFe2O4-\delta\ single crystals by the optical floating zone method, showing for the first time the same magnetization as highly stoichiometric (\delta = 0.00) powder samples and sharp superstructure reflections in…

Materials Science · Physics 2015-08-13 Thomas Mueller , Joost de Groot , Joerg Strempfer , Manuel Angst

Single crystals of PrNiO3 were grown under an oxygen pressure of 295 bar using a unique high-pressure optical-image floating zone furnace. The crystals, with volume in excess of 1 mm3, were characterized structurally using single crystal…

Incorporation of $\mathrm{Al_{y}Ga_{1-y}N}$ (AGN) semiconductors into high power electronics offers efficiency improvements in power transmission, generation, and use, if approaches to eliminate the defects arising from film-lattice…

The optical floating zone crystal growth technique is a well-established method for obtaining large, high-purity single crystals. While the floating zone method has been constantly evolving for over six decades, the development of…

We have developed the laser-diode-heated floating zone (LDFZ) method, in order to improve the broad and inhomogeneous light focusing in the conventional lamp-heated floating zone method, which often causes difficulties in the crystal growth…

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