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Related papers: Growth and Spectroscopic Properties of Pr$^{3+}$ D…

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Bulk single crystals of SrPt3P have been grown for the first time by a self-flux method at 2 GPa and 1500 {\deg}C using the cubic-anvil, high-pressure and high-temperature technique. The grown black crystals were found to have either a…

Superconductivity · Physics 2016-10-11 Nikolai D. Zhigadlo

$Lu_2S_3$ material from the family of sesquisulfide hosts appears to be a promising low-phonon material for use as a laser gain medium allowing for a laser emission over a broad spectral range from ultraviolet to far mid-infrared…

0.5%, 1%, 3% and 5% Ce-concentration single crystals of Tl2LiLuCl6 were grown from the melt using two zone vertical Bridgman technique. X-ray induced emission spectra showed Ce3+ emission between 370 nm and 540 nm wavelength range. Energy…

Materials Science · Physics 2017-04-26 Gul Rooh , H. J. Kim , Jonghoon Jang , Sunghwan Kim

A new method to grow single crystals of skutterudite compounds is examined. Using a wedge-type, cubic-anvil, high-pressure apparatus, single crystals of CoP3 were grown from stoichiometric melts under a pressure of 3.5 GPa. Powder x-ray…

Strongly Correlated Electrons · Physics 2009-11-10 C. H. Lee , H. Kito , H. Ihara , K. Akita , N. Yanase , C. Sekine , I. Shirotani

High-quality single crystals are essentially needed for the investigation of the novel bulk properties of unconventional superconductors. The availability of such crystals grown by the floating-zone method has helped to unveil the…

Superconductivity · Physics 2019-01-08 J. S. Bobowski , N. Kikugawa , T. Miyoshi , H. Suwa , S. Yonezawa , D. A. Sokolov , A. P. Mackenzie , Y. Maeno

Based on differential thermal analysis (DTA) and X-ray powder diffraction (XRD), a description of the system Nd$_2$O$_3$--Lu$_2$O$_3$--Sc$_2$O$_3$ was obtained by thermodynamic assessment. Four fields of primary crystallization could be…

Materials Science · Physics 2018-11-14 Tamino Hirsch , Christo Guguschev , Albert Kwasniewski , Steffen Ganschow , Detlef Klimm

We report on the single crystal growth of Eu(Pd$_{1-x}$Au$_x$)$_2$Si$_2$, $0< x\leq 0.2$, from a levitating Eu-rich melt using the Czochralski method. Our structural analysis of the samples confirms the ThCr$_2$Si$_2$-type structure as well…

Large single crystals of the pyrochlore Pr2Hf2O7 have been successfully grown by the floating zone technique using an optical furnace equipped with high power Xenon arc lamps. Structural investigations have been carried out by both…

In this letter, we report growth and characterization of bulk Bi2Se3 single crystals. The studied Bi2Se3 crystals are grown by self flux method through solid state reaction from high temperature (950C) melt of constituent elements and slow…

Lanthanide-doped Y$_{2}$SiO$_{5}$ microcrystals were prepared using the solution combustion, solid state and sol-gel synthesis techniques. Of these, the sol-gel method yields the most reliable and high-quality X2 phase Y$_{2}$SiO$_{5}$…

Materials Science · Physics 2024-09-26 Jamin L. B. Martin , Lily F. Williams , Michael F. Reid , Jon-Paul R. Wells

We describe the crystal growth of high quality single crystals of the non-centrosymmetric superconductor, Ru7B3 by the floating zone technique, using an optical furnace equipped with xenon arc lamps. The crystals obtained are large and…

Superconductivity · Physics 2014-07-29 Ravi P. Singh , Natalia A. Parzyk , Martin R. Lees , Don McK Paul , Geetha Balakrishnan

The technology to grow single crystals of the required shape directly from a melt has been researched extensively and developed in various industries and research fields. In this study, a micro-pulling-down method and a Mo crucible were…

Materials Science · Physics 2021-10-27 Masao Yoshino , Atsushi Kotaki , Yuui Yokota , Takahiko Horiai , Akira Yoshikawa

Transition metal halides can host a large variety of novel phenomena, such as magnetism in the monolayer limit, quantum spin liquid and spiral spin liquid states, and topological magnons and phonons. Sizeable high quality single crystals…

Materials Science · Physics 2023-01-31 J. -Q. Yan , M. A. McGuire

We grew (Hg,Re)Ba$_2$Ca$_2$Cu$_3$O$_{8+\delta}$ ((Hg,Re)1223) single crystals with good reproducibility via the single-step flux method using monoxides as raw materials. A double-sealing method using a thick-walled quartz tube and a…

An optically high-quality single crystal of sodium mesitylene sulfonate crystal was successfully grown by a slow evaporation method using methanol as solvent at room temperature. Single-crystal XRD has characterized the material and belongs…

We report on the first successful growth of single crystals of the noncentrosymmetric superconductor Mo$_3$Al$_2$C obtained by means of a cubic-anvil, high-pressure and high-temperature technique. Composition, structure, and normal-state…

Superconductivity · Physics 2018-06-27 N. D. Zhigadlo , D. Logvinovich , R. S. Gonnelli , V. A. Stepanov , D. Daghero

By varying the parameters controlling the growth of crystals, including the thermodynamic variables, such as temperature, pressure, and reagent composition and the kinetic factors, namely reaction time and cooling rate, we found the most…

Superconductivity · Physics 2019-06-26 Nikolai D. Zhigadlo

Pyrochlore $\rm Pr^{3+}_{2+x}Zr^{4+}_{2-x}O_{7-x/2}$ samples in the form of both powders $(-0.02 \le x \le 0.02)$ and bulk single crystals have been studied to elucidate the dependence of their magnetic, compositional and structural…

Materials Science · Physics 2014-07-08 S. M. Koohpayeh , J. -J. Wen , B. A. Trump , C. L. Broholm , T. M. McQueen

This report presents a new synthesis protocol for the single crystal growth of rare earth monopnictide DySb by self-flux technique. A detailed structural, transport and magnetic characterization have been done using X-Ray diffraction (XRD),…

Materials Science · Physics 2023-01-11 Mukesh Kumar Dasoundhi , Archana Lakhani

We report the detailed optical properties of Cd$_3$As$_2$ crystals in a wide parameter space: temperature, magnetic field, carrier concentration and crystal orientation. We investigate high-quality crystals synthesized by three different…

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