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In the present study, correlative transmission Kikuchi diffraction transmission electron microscopy (TKD-TEM) measurements, atom probe tomography (APT), and density functional theory (DFT) calculations are used to reveal the elemental…

Materials Science · Physics 2026-01-21 Bowen Zou , Yixu Wang , Xiao Shen , Philipp Krooss , Thomas Niendorf , Richard Dronskowski , Wenwen Song

Atomic probe tomography (APT), based on the work of Erwin Mueller, is able to generate three-dimensional chemical maps in atomic resolution. The required instruments for APT have evolved over the last 20 years from an experimental to an…

We describe a general method to determine the location of a point source of waves relative to a two-dimensional active pixel detector. Based on the inherent structural sensitivity of crystalline sensor materials, characteristic detector…

Instrumentation and Detectors · Physics 2017-04-26 Stefano Vespucci , Carol Trager-Cowan , Dzmitry Maneuski , Val O'Shea , Aimo Winkelmann

Volumetric crystal structure indexing and orientation mapping are key data processing steps for virtually any quantitative study of spatial correlations between the local chemistry and the microstructure of a material. For electron and…

Computational Physics · Physics 2020-09-03 Markus Kühbach , Matthew Kasemer , Baptiste Gault , Andrew Breen

Transmission electron microscopy (TEM) is a potent technique for the determination of three-dimensional atomic scale structure of samples in structural biology and materials science. In structural biology, three-dimensional structures of…

Addressing the need for efficient and integrated multiscale crystallographic and defect analyses of advanced materials, this paper presents the implementation of a new multi-configuration detection system, integrating a single…

Instrumentation and Detectors · Physics 2026-05-19 Nohayla El-Khairaoui , Julien Guyon , Nathalie Gey , Luc Morhain , Nabila Maloufi

Symmetry breaking states of matter can transmit symmetry breaking to nearby atoms or molecular complexes, perturbing their spectra. We calculate one such effect, involving the `axion electrodynamics' relevant to topological insulators,…

Mesoscale and Nanoscale Physics · Physics 2019-05-29 Qing-Dong Jiang , Frank Wilczek

Transition metal dichalcogenides (TMDs) attract significant attention as potential building blocks in next-generation electronic devices. On the other hand, a comprehensive understanding of how various defects affect local electronic…

Materials Science · Physics 2026-04-28 Joshua R. Evans , Diego A. Garibay , Aiden N. Kuhls , Mehmet Z. Baykara

In the technique of Electron Backscatter Diffraction (EBSD), the accurate detection and identification of different phases existing in a sample is often limited by overlapping Kikuchi diffraction patterns originating from the extended…

Materials Science · Physics 2026-01-23 Grzegorz Cios , Aimo Winkelmann , Tomasz Tokarski , Wiktor Bednarczyk , Piotr Bała

Studying the atomic structure of intrinsic defects in two-dimensional transition metal dichalcogenides is difficult since they damage quickly under the intense electron irradiation in transmission electron microscopy (TEM). However, this…

Electron backscatter diffraction is one of the most prevalent techniques used for microstructural characterization. In recent years, there has been an increase in the use of data-driven methods to analyze raw Kikuchi patterns. However, most…

Materials Science · Physics 2026-01-21 Qi Zhang , Santiago Benito , Sebastian Weber , Markus Stricker

Crystals of the chemical elements manganese, tellurium, and selenium can show the effects of handedness. In order to sense the possible effects of a changing sense of chirality on the properties of samples from these elements, the potential…

Materials Science · Physics 2021-10-26 Aimo Winkelmann , Grzegorz Cios , Tomasz Tokarski , Piotr Bała , Yuri Grin , Ulrich Burkhardt

The properties of bulk nanostructured materials are often controlled by atomic scale features like segregation along defects or composition gradients. Here we discuss about the complimentary use of TEM and APT to obtain a full description…

Materials Science · Physics 2009-04-15 Xavier Sauvage , Williams Lefebvre , Cécile Genevois , S. Ohsaki , Kazuhiro Hono

Materials characterization using electron backscatter diffraction (EBSD) requires indexing the orientation of the measured region from Kikuchi patterns. The quality of Kikuchi patterns can degrade due to pattern overlaps arising from two or…

Materials Science · Physics 2024-06-07 Ashish Chauniyal , Pascal Thome , Markus Stricker

Defects and reconstructions in 2D moir\'e materials cause out-of-plane deformations which strongly modify their electronic properties but are difficult to experimentally access. Here, we solve the 3D atomic coordinates of twisted bilayer…

Materials Science · Physics 2025-09-10 Jeffrey Huang , Yichao Zhang , Sang hyun Bae , Ballal Ahammed , Elif Ertekin , Pinshane Y. Huang

Atomic layer deposition (ALD) provides uniform and conformal thin films that are of interest for a range of applications. To better understand the properties of amorphous ALD films, we need improved understanding of their local atomic…

Materials Science · Physics 2021-02-12 Ahmed M. Jasim , Xiaoqing He , Yangchuan Xing , Tommi A. White , Matthias J. Young

Atom probe tomography (APT) is a 3D analysis technique that offers unique chemical accuracy and sensitivity with sub-nanometer spatial resolution. Recently, there is an increasing interest in the application of APT to complex oxides…

2D materials offer an ideal platform to study the strain fields induced by individual atomic defects, yet challenges associated with radiation damage have so-far limited electron microscopy methods to probe these atomic-scale strain fields.…

Three-dimensional reconstruction of atomic structure, known as atomic electron tomography (AET), has found increasing applications in materials science. The AET has been limited to very small nanoparticles due to the challenges of obtaining…

Materials Science · Physics 2024-01-24 Liangze Mao , Jizhe Cui , Rong Yu

Using transient grating spectroscopy (TGS) we measure the thermal diffusivity of tungsten exposed to different levels of 20 MeV self-ion irradiation. Damage as low as 3.2 x 10^-4 displacements per atom (dpa) causes a measurable reduction in…

Materials Science · Physics 2020-02-05 Abdallah Reza , Hongbing Yu , Kenichiro Mizohata , Felix Hofmann