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Gratings enable dispersive spectroscopy from the X-ray to the optical, and feature prominently in proposed flagships and SmallSats alike. The exacting performance requirements of these future missions necessitate assessing whether the…

Instrumentation and Methods for Astrophysics · Physics 2020-12-09 Casey T. DeRoo , Jared Termini , Fabien Grise , Randall L. McEntaffer , Benjamin D. Donovan , Chad Eichfeld

In a companion paper we have reported a $>5\sigma$ detection of degree scale $B $-mode polarization at 150 GHz by the BICEP2 experiment. Here we provide a detailed study of potential instrumental systematic contamination to that…

Optimizing grain boundary characteristics in polycrystalline materials can improve their properties. Many processing methods have been developed for grain boundary manipulation, including the use of intense radiation in certain…

Grazing incidence fast atom diffraction (GIFAD, or FAD) has developed as a surface sensitive technique. GIFAD is less sensitive to thermal decoherence but more demanding in terms of surface coherence, the mean distance between defects. Such…

Atomic Physics · Physics 2016-09-21 Maxime Debiossac , Philippe Roncin

We report the design and construction of a novel soft x-ray diffractometer installed at Diamond Light Source. The beamline endstation RASOR is constructed for general users and designed primarily for the study of single crystal diffraction…

Strongly Correlated Electrons · Physics 2014-11-21 T. A. W. Beale , T. P. A. Hase , T. Iida , K. Endo , P. Steadman , A. R. Marshall , S. S. Dhesi , G. van der Laan , P. D. Hatton

We demonstrate a smart laser-diffraction analysis technique for particle mixture identification. We retrieve information about the size, geometry, and ratio concentration of two-component heterogeneous particle mixtures with an efficiency…

Image and Video Processing · Electrical Eng. & Systems 2022-02-03 Arturo Villegas , Mario A. Quiroz-Juarez , Alfred U'Ren , Juan P. Torres , Roberto de J. Leon-Montiel

Three-dimensional electron diffraction (3D ED) has emerged as a powerful method for solving the structures of sub-micron-sized particles down to nanoparticles. However, it faces technical challenges when applied to beam-sensitive samples or…

Precession Electron Diffraction (PED) offers a number of advantages for crystal structure analysis and solving unknown structures using electron diffraction. The current article uses many-beam simulations of PED intensities, in combination…

Materials Science · Physics 2025-09-22 W. Sinkler , L. D. Marks

Zircaloy-4 is used extensively as nuclear fuel cladding materials and hydride embrittlement is a major failure mechanism. To explore the effect of {\delta}-hydride on plastic deformation and performance of Zircaloy-4, in situ high angular…

Materials Science · Physics 2019-03-28 Siyang Wang , Szilvia Kalácska , Xavier Maeder , Johann Michler , Finn Giuliani , T. Ben Britton

We present here a nanosecond laser ablation of Si(111) wafer with diffraction-free (Bessel-$J_0$) beams. First, the Axicon a conical shaped optical element for beam shaping is characterized with a visible and infrared light sources. Then,…

Applied Physics · Physics 2020-05-20 Erkan Demirci , Elif Turkan Aksit Kaya , Ramazan Sahin

We present an assessment of a multi-method approach based on ion beam analysis to obtain high-resolution depth profiles of the total chemical composition of complex alloy systems. As a model system we employ an alloy based on several…

Applied Physics · Physics 2019-07-15 M. V. Moro , R. Holeňák , L. Zendejas Medina , U. Jansson , D. Primetzhofer

Ultrafast electron diffraction (UED) is a technique in which short-pulse electron beams can probe the femtosecond-scale evolution of atomic structure in matter driven far from equilibrium. As an accelerator physics challenge, UED imposes…

Pulsed-laser dry printing of noble-metal microrings with a tunable internal porous structure, which can be revealed via an ion-beam etching post-procedure, was demonstrated. Abundance and average size of the pores inside the microrings were…

Applied Physics · Physics 2017-09-27 S. Syubaev , A. Nepomnyashchiy , E. Mitsai , E. Pustovalov , O. Vitrik , S. Kudryashov , A. Kuchmizhak

The advent of X-ray Free Electron Lasers promises the possibility to determine the structure of individual particles such as microcrystallites, viruses and biomolecules from single-shot diffraction snapshots obtained before the particle is…

Soft Condensed Matter · Physics 2010-05-06 Brian Moths , Abbas Ourmazd

The use of strongly bent crystals in spectrometers for pulses of a hard x-ray free-electron laser is explored theoretically. Diffraction is calculated in both dynamical and kinematical theories. It is shown that diffraction can be treated…

Instrumentation and Detectors · Physics 2019-05-28 Vladimir Kaganer , Ilia Petrov , Liubov Samoylova

Nanoscale strain mapping by four-dimensional scanning transmission electron microscopy (4D-STEM) relies on determining the precise locations of Bragg-scattered electrons in a sequence of diffraction patterns, a task which is complicated by…

The resolution of X-ray diffraction microscopy is limited by the maximum dose that can be delivered prior to sample damage. In the proposed Serial Crystallography method, the damage problem is addressed by distributing the total dose over…

Transmission electron microscopy and spectroscopy currently enable the acquisition of spatially resolved spectral information from a specimen by focusing electron beams down to a sub-Angstrom spot and then analyzing the energy of the…

Materials Science · Physics 2022-09-12 Andrea Konečná , Fadil Iyikanat , F. Javier García de Abajo

Layered materials (LMs) are at the centre of an ever increasing research effort due to their potential use in a variety of applications. The presence of imperfections, such as bi- or multilayer areas, holes, grain boundaries, isotropic and…

Four-dimensional scanning transmission electron microscopy (4D-STEM) provides rich, atomic-scale insights into materials structures. However, extracting specific physical properties - such as polarization directions essential for…

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