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We have grown a YCrO$_3$ single crystal by the floating-zone method and studied its temperature-dependent crystalline structure and magnetization by X-ray powder diffraction and PPMS DynaCool measurements. All diffraction patterns were well…

Strongly Correlated Electrons · Physics 2024-03-08 Qian Zhao , Yinghao Zhu , Si Wu , Junchao Xia , Pengfei Zhou , Kaitong Sun , Hai-Feng Li

We have grown intermetallic ErPd$_2$Si$_2$ single crystals employing laser-diodes with the floating-zone method. The temperature-dependent crystallography was determined using synchrotron and in-house X-ray powder diffraction measurements…

Materials Science · Physics 2022-08-02 Kaitong Sun , Yinghao Zhu , Si Wu , Junchao Xia , Pengfei Zhou , Qian Zhao , Chongde Cao , Hai-Feng Li

Our detailed temperature dependent synchrotron powder x-ray diffraction studies along with first-principles density functional perturbation theory calculations, enable us to shed light on the origin of ferroelectricity in GdCrO3. The actual…

Strongly Correlated Electrons · Physics 2017-09-20 Sudipta Mahana , Bipul Rakshit , Raktima Basu , Sandip Dhara , Boby Joseph , U. Manju , Subhendra D. Mahanti , D. Topwal

The crystal structures of the Sr1-xCaxRuO3 perovskites are investigated using both long range and local structural probes. High resolution synchrotron powder X-ray diffraction characterization at ambient temperature shows that the materials…

Materials Science · Physics 2020-03-25 Loi T. Nguyen , Milinda Abeykoon , Jing Tao , Saul Lapidus , R. J. Cava

Through powder x-ray diffraction we have investigated the structural behavior of SmVO3, in which orbital and magnetic degrees of freedom are believed to be closely coupled to the crystal lattice. We have found, contrary to previous reports,…

Magnetization measurements and time-of-flight neutron powder-diffraction studies on the high-temperature (300--980 K) magnetism and crystal structure (321--1200 K) of a pulverized YCrO$_3$ single crystal have been performed.…

Strongly Correlated Electrons · Physics 2021-11-04 Yinghao Zhu , Si Wu , Bao Tu , Shangjian Jin , Ashfia Huq , Joerg Persson , Haoshi Gao , Defang Ouyang , Zhubing He , Dao-Xin Yao , Zikang Tang , Hai-Feng Li

Density-functional calculations of lattice dynamics and high-resolution synchrotron powder diffraction uncover antiferroelectric distortion in the kagome francisite Cu$_3$Bi(SeO$_3$)$_2$O$_2$Cl below 115K. Its Br-containing analogue is…

Antiferromagnetic intermetallic compound EuRhGe3 crystalizes in a non-centrosymmetric BaNiSn3-type (I4mm) structure. We studied its pressure-dependent crystal structure by using synchrotron powder x-ray diffraction at room temperature. Our…

The structural, dielectric and ferroelectric properties of lead-free (Na0.5-xKxBi0.5-xLax)TiO3 powders synthesized by sol-gel self-combustion method were investigated. Rietveld refinement of Synchrotron x-ray diffraction data confirms pure…

The compound CaV2O4 contains V^{+3} cations with spin S = 1 and has an orthorhombic structure at room temperature containing zigzag chains of V atoms running along the c-axis. We have grown single crystals of CaV2O4 and report…

SmCrO$_3$ single crystals were successfully grown utilizing the high-pressure optical floating-zone method and their crystal structure, magnetization behavior, and magnetic phase diagrams were thoroughly investigated. Magnetic studies were…

Strongly Correlated Electrons · Physics 2025-06-05 Ning Yuan , Erik Walendy , Nour Maraytta , Waldemar Hergett , Luca Bischof , Michael Merz , Rüdiger Klingeler

The results of x-ray diffraction, and ac and dc magnetization as a function of temperature are reported for a new class of spin-chain oxides, Ca3Co1+xIr1-xO6. While the x= 0.0, 0.3, 0.5 and 1.0 are found to form in the K4CdCl6-derived…

Materials Science · Physics 2007-05-23 S. Rayaprol , Kausik Sengupta , E. V. Sampathkumaran

The structural properties of LaCoO3 were studied by means of high-resolution neutron powder diffraction in the temperature range 5<T<1000 K. Changes of the Co+3 spin states in this temperature interval are shown to affect not only the unit…

Strongly Correlated Electrons · Physics 2009-11-07 Paolo G. Radaelli , Sang-Wook Cheong

The structural properties of a $\beta$-Ga$_2$O$_3$ single crystal grown by the oxide crystal growth from cold crucible (OCCC) method were investigated using synchrotron radiation X-ray topography and X-ray reticulography. The region grown…

The crystal structure of a disordered form of Cr$_{1/3}$NbS$_2$ has been characterized using diffraction and inelastic scattering of synchrotron radiation. In contrast to the previously reported symmetry (P6$_3$22), the crystal can be…

Materials Science · Physics 2015-05-27 V. Dyadkin , F. Mushenok , A. Bosak , D. Menzel , S. Grigoriev , P. Pattison , D. Chernyshov

By means of single-crystal X-ray diffraction we have revealed the breaking of centrosymmetry when lowering the temperature under T$_s$ = 200 K concomitantly with the setting of a commensurate superstructure in the small A-site quadruple…

Materials Science · Physics 2022-11-24 M Verseils , F Mezzadri , D Delmonte , R Cabassi , B Baptiste , Y Klein , G Calestani , F Bolzoni , E Gilioli , A Gauzzi

We investigate the mechanism of the resonant X-ray scattering on the Ti $K$ edge region of YTiO$_3$ using the band structure calculation combined with the local density approximation. A large intensity is obtained for the orbital…

Strongly Correlated Electrons · Physics 2007-05-23 Manabu Takahashi , Jun-ichi Igarashi

We have investigated the temperature dependence of the crystal structure of quasi-one-dimensional monoclinic BaIrO$_3$ using X-ray diffraction. Diffraction patterns were measured across a temperature range from 13 K to 300 K, with 5-degree…

Materials Science · Physics 2025-11-07 Jeong Jinwon , Chang Bin , Noh Han-Jin , Lee Seongsu

Metallic LiOsO$_3$ undergoes a continuous ferroelectric-like structural phase transition below $T_c$ = 140 K to realize a polar metal. To understand the microscopic interactions that drive this transition, we study its critical behavior…

Strongly Correlated Electrons · Physics 2020-08-04 Jun-Yi Shan , A. de la Torre , N. J. Laurita , L. Zhao , C. D. Dashwood , D. Puggioni , C. X. Wang , K. Yamaura , Y. Shi , J. M. Rondinelli , D. Hsieh

In the quest of understanding significant variations in the physical, chemical and electronic properties of the novel functional materials, low temperature Synchrotron X-ray Diffraction (LT-SXRD) measurements on CTO (a type-II) and CMTO (a…

Materials Science · Physics 2016-08-09 Harishchandra Singh , A. K. Sinha , M. N. Singh , A. Upadhyay , Archna Sagdeo
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