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Millimeter sized single crystals of CaFe$_{1-x}$Co$_x$AsF were grown using a self-flux method. It is found that high-quality single crystals can be grown from three approaches with different initial raw materials. The chemical compositions…

Superconductivity · Physics 2016-08-09 Yonghui Ma , Kangkang Hu , Qiucheng Ji , Bo Gao , Hui Zhang , Gang Mu , Fuqiang Huang , Xiaoming Xie

To prevent the loss of K in growing single crystals of Ba1-x Kx Fe2 As2 we developed a rapid heating Sn-flux method. Large single crystals with the optimal superconducting transition temperature TC about 38K were obtained and their…

Superconductivity · Physics 2009-02-21 P. Reuvekamp , F. S. Razavi , C. Hoch , J. S. Kim , R. K. Kremer , A. Simon

This article presents a direct measurement of the growth angle during the growth of a cylindrical 2" silicon crystal using a radio-frequency heated floating zone process. From the high-resolution pictures taken during the process, this…

Materials Science · Physics 2011-02-21 Michael Wünscher , Anke Lüdge , Helge Riemann

Ni-doped LiMn0.95Ni0.05PO4 single crystals have been grown for the first time by the travelling-solvent floating-zone method at low Argon pressure. The grown sample exhibits large single crystalline grains as revealed by means of…

Crystallization is a fundamental process in materials science, providing the primary route for the realization of a wide range of new materials. Crystallization rates are also considered to be useful probes of glass-forming ability. At the…

Neutron time-of-flight spectroscopy has been employed to study the crystal-field splitting of Pr$^{3+}$ in the pyrochlore stannate Pr$_{2}$Sn$_{2}$O$_{7}$. The crystal field has been parameterized from a profile fit to the observed neutron…

Strongly Correlated Electrons · Physics 2013-10-28 A. J. Princep , D. Prabhakaran , A. T. Boothroyd , D. T. Adroja

We report on the single crystal growth of Eu(Pd$_{1-x}$Au$_x$)$_2$Si$_2$, $0< x\leq 0.2$, from a levitating Eu-rich melt using the Czochralski method. Our structural analysis of the samples confirms the ThCr$_2$Si$_2$-type structure as well…

This work aimed first at growing high quality bulk $\alpha$-GeO$_2$ crystals in their Quartz iso-structural form ($\alpha$-SiO$_2$), using a high temperature flux method. By optimizing the flux composition and the geometry and orientation…

Optics · Physics 2025-01-23 Alexandra Pena , Corinne Felix , Bertrand Menaert , Benoit Boulanger

High quality large Bi$_2$Sr$_{2-x}$La$_{x}$CuO$_6$(La-Bi2201) single crystals have been successfully grown by the traveling solvent floating zone technique. The samples are characterized by compositional and structural analyzes and their…

Superconductivity · Physics 2009-11-13 Jianqiao Meng , Guodong Liu , Wentao Zhang , Lin Zhao , Haiyun Liu , Wei Lu , Xiaoli Dong , X J Zhou

The peculiar properties of zinc oxide (ZnO) make this material interesting for very different applications like light emitting diodes, lasers, and piezoelectric transducers. Most of these applications are based on epitaxial ZnO layers grown…

Materials Science · Physics 2009-11-13 D. Klimm , S. Ganschow , D. Schulz , R. Fornari

The physics of ice crystal growth from the liquid phase, especially in the presence of salt, has received much less attention than the growth of snow crystals from the vapour phase. The growth of so-called frazil ice by solidification of a…

Materials Science · Physics 2017-11-22 David W. Rees Jones , Andrew J. Wells

We report the successful synthesis of single-crystalline cuprate superconductors HgBa$_{2}$CaCu$_{2}$O$_{6+\delta}$ and HgBa$_{2}$Ca$_{2}$Cu$_{3}$O$_{8+\delta}$. These compounds are well-known for their high optimal superconducting critical…

Single crystals of A$_{1-x}$K$_x$Fe$_2$As$_2$ (A=Ba, Sr) with high quality have been grown successfully by FeAs self-flux method. The samples have sizes up to 4 mm with flat and shiny surfaces. The X-ray diffraction patterns suggest that…

Superconductivity · Physics 2009-11-13 Huiqian Luo , Zhaosheng Wang , Huan Yang , Peng Cheng , Xiyu Zhu , Hai-Hu Wen

Recent theoretical and experimental findings suggest that the long-known but not well understood low temperature resistance plateau of SmB6 may originate from protected surface states arising from a topologically non-trivial bulk band…

Single crystals of SmFeAsO1-xFy of a size up to 120 micrometers have been grown from NaCl/KCl flux at a pressure of 30 kbar and temperature of 1350-1450 C using the cubic anvil high-pressure technique. The superconducting transition…

Superconductivity · Physics 2009-11-13 N. D. Zhigadlo , S. Katrych , Z. Bukowski , S. Weyeneth , R. Puzniak , J. Karpinski

SmB6 has recently been predicted to be a Topological Kondo Insulator, the first strongly correlated heavy fermion material to exhibit topological surface states. High quality crystals are necessary to investigate the topological properties…

Strongly Correlated Electrons · Physics 2013-10-31 M. Ciomaga Hatnean , M. R. Lees , D. McK. Paul , G. Balakrishnan

A series of Yb2Ti2O7 doped samples demonstrates the effects of off-stoichiometry on Yb2Ti2O7's structure, properties, and magnetic ground state via x-ray diffraction, specific heat, and magnetization measurements. A stoichiometric single…

Strongly Correlated Electrons · Physics 2017-03-15 K. E. Arpino , B. A. Trump , A. O. Scheie , T. M. McQueen , S. M. Koohpayeh

A macroscopic single crystal of $\gamma_{\rm II}$-Li\(_2\)FeSiO\(_4\) has been grown by means of the high-pressure optical floating-zone technique. Static magnetic susceptibility $\chi$ implies that the tetrahedrally-coordinated Fe$^{2+}$…

Large high-quality single crystals of Bi2Sr2Can-1CunO2n+4+d (n = 2, 3) were successfully grown using an improved traveling solvent floating zone (TSFZ) method, which features a slow growth rate and steep temperature gradient along the…

Superconductivity · Physics 2007-05-23 Takao Watanabe , Takenori Fujii , Azusa Matsuda

The thermoelectric properties between 10 and 300 K and the growth of single crystals of n-type and p-type GeBi4Te7, GeSb4Te7, and the Ge(Bi1-xSbx)4Te7 solid solution are reported. Single crystals were grown by the modified Bridgman method,…

Materials Science · Physics 2013-01-28 Fabian von Rohr , Andreas Schilling , Robert J. Cava
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