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Alkoxide-intercalated NiFe-layered double hydroxides were synthesized via the nonaqueous methanolic route. These nanoplatelets exhibit high crystalline quality as demonstrated by atomic resolution scanning transmission electron microscopy…

Nickel-iron layered double hydroxide (NiFe LDH) platelets with high morphological regularity and sub-micrometre lateral dimensions were synthesized using a homogeneous precipitation technique for highly efficient catalysis of the oxygen…

Nickel-based layered double hydroxides (LDHs) are promising electrode materials in the fields of energy storage (supercapacitors) and conversion (urea oxidation). The rational construction of atomic and electronic structure is crucial for…

Applied Physics · Physics 2024-03-27 Yuchen Wang , Yaoyu Liu , Man Zhang , Biying Liu , Zhiyue Zhao , Kai Yan

Highly active, durable and cost-effective electrocatalysts for water oxidation to evolve oxygen gas hold a key to a range of renewable energy solutions including water splitting and rechargeable metal-air batteries. Here, we report the…

Layered double-hydroxides (LDHs) are superior to the conventional (Transition Metal Oxides) TMOs as their lamellar morphology accommodates higher active sites contributing to the facile electron transfer towards the material degradation…

Polyhedral nanocrystals of <alpha>-Fe2O3 are successfully synthesized by annealing FeCl3 on silicon substrate at 1000 oC in the presence of H2 gas diluted with argon (Ar). Uniformly shaped polyhedral nanoparticles (diameter ~50-100 nm) are…

Materials Science · Physics 2011-11-22 Rajesh Kumar , S. Gautam , In-Chul Hwang , K. H. Chae , Nagesh Thakur

FeNi L10 (tetrataenite) phase has great perspectives for hard magnetic materials production. In this paper it was synthesized in chemically co-precipitated FeNi nanopowder by means of thermal treating included cycling of oxidation and…

Materials Science · Physics 2020-08-10 V. L. Kurichenko , D. Yu. Karpenkov , A. Yu. Karpenkov , M. B. Lyakhova , V. V. Khovaylo

Transition-metal-based layered double hydroxides (TM-LDHs) nanosheets are promising electrocatalysts in the renewable electrochemical energy conversion system, which are regarded as alternatives to noble metal-based materials. In this…

Applied Physics · Physics 2024-03-26 Yuchen Wang , Man Zhang , Yaoyu Liu , Zhikeng Zheng , Biying Liu , Meng Chen , Guoqing Guan , Kai Yan

Thermal stability of hydrogenated amorphous Si/Ge multilayers has been investigated by Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM) and Small-Angle X-Ray Diffraction (SAXRD) techniques. Amorphous H-Si/Ge…

Materials Science · Physics 2009-02-11 A. Csik , M. Serenyi , Z. Erdelyi , A. Nemcsics , C. Cserhati , G. A. Langer , D. L. Beke , C. Frigeri , A. Simon

Two-dimensional semiconducting materials are particularly appealing for many applications. Although theory predicts a large number of two-dimensional materials, experimentally only a few of these materials have been identified and…

Bottom-up synthesis of two-dimensional transition-metal silicates has been challenging due to strong overlayer-substrate interactions, which prevents the exfoliation of the overlayer. Here, using density functional theory calculations, we…

Materials Science · Physics 2022-02-14 Kayahan Saritas , Nassar Doudin , Eric I. Altman , Sohrab Ismail-Beigi

Continuous hydrothermal flow synthesis (CHFS) is a facile, upscalable and cost-efficient synthetic method enabling the nanostructuring of advanced functional materials in steady conditions, i.e. not in batch synthesis. In this paper, we use…

The present work reported a novel L12-strengthening NiCoCrAlTi high entropy alloy (HEA) with an outstanding synergy of tensile strength and ductility at both ambient and high temperatures. Transmission electron microscopy (TEM)…

Hydrogen sensors have been prepared using nickel oxide (NiO) and lithium-doped nickel oxide (NiO:Li) thin films, deposited on glass substrates by the sol-gel spin coating technique. The surface morphology, structure, optical and electrical…

Materials Science · Physics 2014-12-23 I. Sta , M. Jlassi , M. Kandyla , M. Hajji , P. Koralli , R. Allagui , M. Kompitsas , H. Ezzaouia

Hydrothermal synthesis is described of layered lithium iron selenide hydroxides Li1-xFex(OH)Fe1-ySe (x ~ 0.2; 0.02 < y < 0.15) with a wide range of iron site vacancy concentrations in the iron selenide layers. This iron vacancy…

Reaching pressures in the 100 GPa range enables the synthesis of hydrogen-rich compounds, with nontraditional H stoichiometries and H sublattices, called superhydrides. Record-breaking superconductivity temperature in some superhydrides…

Materials Science · Physics 2025-05-23 M. Caussé , L. Toraille , G. Geneste , P. Loubeyre

We report an easy and versatile one-step route of synthesis for newly discovered Fe based superconductor LaFeAsO1-d with d = 0.0 to 0.15. Instead of widely used high-pressure-high-temperature (HPHT) synthesis, we applied the normal…

Low-temperature synthesis is a promising and potentially effective method for improving superconducting properties. We report on the fabrication of polycrystalline samples of SmFeAsO1-xFx with nominal x content varying in a wide range of x…

Superconductivity · Physics 2013-03-19 S. J. Singh , J. Shimoyama , A. Yamamoto , H. Ogino , K. Kishio

Rational synthesis of robust layered double hydroxides (LDHs) nanosheets for high-energy supercapacitors is full of challenges. Herein, we reported an ultrasonication-assisted strategy to eco-friendly fabricate NiFe-LDHs nanosheets for the…

Applied Physics · Physics 2024-03-26 Yuchen Wang , Zuo Chen , Man Zhang , Yaoyu Liu , Huixia Luo , Kai Yan

As low as 900 oC, iron-based layered quaternary compound NdFeAsO0.75 was synthesized through solid state reaction method. XRD measurements illustrate almost pure phase of tetragonal phase NdFeAsO was formed. The synthesis temperature in our…

Superconductivity · Physics 2008-06-06 Qingping Ding , Yangguang Shi , Hongbo Huang , Shaolong Tang , Shaoguang Yang
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