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Grazing incidence X-ray diffraction (GIXD) is widely used for the structural characterization of thin films, particularly for analyzing phase composition and the orientation distribution of crystallites. While various tools exist for…

We developed a setup using a two dimensional camera for Grazing Incidence x-ray Diffraction (GIXD) on Langmuir monolayers and more generally for surface diffraction on two dimensional powders. Compared to the classical setup using a linear…

Soft Condensed Matter · Physics 2009-11-10 Philippe Fontaine , Michel Goldmann Michel Bordessoule , Alain Jucha

Grazing incidence fast atom diffraction (GIFAD, or FAD) has developed as a surface sensitive technique. GIFAD is less sensitive to thermal decoherence but more demanding in terms of surface coherence, the mean distance between defects. Such…

Atomic Physics · Physics 2016-09-21 Maxime Debiossac , Philippe Roncin

We present a computational imaging technique for imaging thin films at grazing-incidence (GI) angles by incorporating structured illumination into existing GI X-ray scattering setups. This method involves scanning a micro-coded aperture…

Grazing incidence X-ray scattering experiments are designed to achieve strong scattering signals from materials, such as molecular monolayers, island films, or thin films that are localized to the surfaces of flat substrates. Optimal…

Instrumentation and Detectors · Physics 2025-07-01 Edward Tortorici , Charles T. Rogers

Resolving how defects emerge and interact within the hierarchical structure of polycrystalline materials remains a core challenge in materials science. Grain-mapping methods such as three-dimensional X-ray diffraction (3DXRD) and…

We have developed a 3 dimensional Coherent Diffraction Imaging (CDI) algorithm to retrieve phases of diffraction patterns of samples in Grazing Incidence Small Angle X-ray Scattering (GISAXS) experiments. The algorithm interprets the…

Instrumentation and Detectors · Physics 2023-07-26 Yi Yang , Sunil K. Sinha

We demonstrate a technique that allows highly surface sensitive imaging of nanostructures on planar surfaces over large areas, providing a new avenue for research in materials science, especially for \textit{in situ} applications. The…

Grazing incidence x-ray scattering provides nanostructural information for thin film samples, but single images generally do not provide information on film thickness or the full complex index of refraction. Additionally, for thin films…

Applied Physics · Physics 2020-11-10 Peter J. Dudenas , Adam Z. Weber , Ahmet Kusoglu

For the reliable fabrication of the current and next generation of nanostructures it is essential to be able to determine their material composition and dimensional parameters. Using the grazing incidence X-ray fluoresence technique, which…

Grazing-Incidence X-ray fluorescence (GIXRF) analysis, which is closely related to total-reflection XRF, is a very powerful technique for the in-depth analysis of many types of technologically relevant samples, e.g. nanoparticle…

The increasing importance of well-controlled ordered nanostructures on surfaces represents a challenge for existing metrology techniques. To develop such nanostructures and monitor complex processing constraints fabrication, both a…

Understanding the processes of perovskite crystallization is essential for improving the properties of organic solar cells. In situ real-time grazing-incidence X-ray diffraction (GIXD) is a key technique for this task, but it produces large…

Even after several decades of systematic usage of X-ray diffraction as one of the major analytical tool for epitaxic layers, the vision of the reciprocal space of these materials is still a simple superposition of two reciprocal lattices,…

Materials Science · Physics 2007-05-23 Jarek Z. Domagala , Sergio L. Morelhao

X-ray reflectivity and grazing incidence diffraction (XGID) from liquid surfaces are described.

Soft Condensed Matter · Physics 2019-06-25 Dvaid Vaknin

A new method for estimation of intragranular strain fields in polycrystalline materials based on scanning three-dimensional X-ray diffraction data (scanning-3DXRD) is presented and evaluated. Given an apriori known anisotropic compliance,…

Materials Science · Physics 2021-06-16 Axel Henningsson , Johannes Hendriks

The characterization of nanostructured surfaces with sensitivity in the sub-nm range is of high importance for the development of current and next generation integrated electronic circuits. Modern transistor architectures for e.g. FinFETs…

X-ray diffraction gratings play an essential role in high-resolution spectroscopy of astrophysical phenomena. We present some scientific highlights from the X-ray grating spectrometers (XGS) on board of the Chandra and XMM/Newton missions,…

Instrumentation and Methods for Astrophysics · Physics 2024-09-05 Ralf K. Heilmann , David P. Huenemoerder , Jake A. McCoy , Randall L. McEntaffer

Laterally periodic nanostructures were investigated with grazing incidence small angle X-ray scattering (GISAXS) by using the diffraction patterns to reconstruct the surface shape. To model visible light scattering, rigorous calculations of…

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