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SnO2 nanoparticles with different percentage of Al (5%, 15%, and25%) were synthesized by sol-gel method. The structure and nature of nanoparticles are determined by of X-ray diffraction analysis. Also morphology of the samples is evaluated…

Mesoscale and Nanoscale Physics · Physics 2025-03-05 Ali Reza Razeghizadeh , Lila Zalaghi , Iraj Kazeminezhad , Vahdat Rafee

The structure-property relation of nanostructured Al-doped ZnO thin films has been investigated in detail through a systematic variation of structure and morphology, with particular emphasis on how they affect optical and electrical…

Materials Science · Physics 2013-11-28 P. Gondoni , M. Ghidelli , F. Di Fonzo , M. Carminati , V. Russo , A. Li Bassi , C. S. Casari

In this paper, the effects of changes in Sol concentration on the structural and optical properties of SnO2 Nanoparticles are studied through the Sol-Gel method. SnO2 Nanoparticles are produced from different SnO2 solution concentrations…

Mesoscale and Nanoscale Physics · Physics 2025-03-05 Ali Reza Razeghizadeh , Lila Zalaghi , Iraj Kazeminezhad , Vahdat Rafee

The present article describes the size induced changes in the structural arrangement of intrinsic defects present in chemically synthesized ZnO nanoparticles of various sizes. Routine X-ray diffraction (XRD) and Transmission Electron…

Materials Science · Physics 2011-09-15 S K Chaudhuri , Manoranjan Ghosh , D Das , A K Raychaudhuri

This investigation deals with the effect of annealing temperature on the structural, topographical and optical properties of Zinc Oxide thin films prepared by sol gel method. The structural properties were studied using X-ray diffraction…

Applied Physics · Physics 2019-08-19 Joydip Sengupta , R. K. Sahoo , K. K. Bardhan , C. D. Mukherjee

Because of their high photon flux, X-ray free-electron lasers (FEL) allow to resolve the structure of individual nanoparticles via coherent diffractive imaging (CDI) within a single X-ray pulse. Since the inevitable rapid destruction of the…

We report the crystallographic texture of ZnO thin films comprising nanorods grown by a microwave irradiation assisted method. Different substrates were used, namely Si, Ge, metal coated Si, PMMA coated Si and ITO coated glass, to examine…

Materials Science · Physics 2017-09-29 Piyush Jaiswal , Sanjaya Brahma , K. S. Suresh , S. A. Shivashankar , Satyam Suwas

Cr-doped ZnO films were fabricated by a new but feasible method, that is, annealing Cr-Zn layers deposited via DC magnetron sputtering in air. Microstructures of the films were investigated using X-ray diffraction, scanning electron…

Materials Science · Physics 2025-08-19 Men Guo , Gilad Orr , Paul Ben Ishai , Xia Zhao , Shlomo Glasser

Direct observation of organic molecular nanocrystals and their evolution using electron microscopy is extremely challenging, due to their radiation sensitivity and complex structure. Here, we introduce 4D-scanning confocal electron…

Materials Science · Physics 2022-06-15 Mingjian Wu , Christina Harreiss , Colin Ophus , Erdmann Spiecker

Nanotechnology has already made indelible dents in the fields of communication, computation, electronics, photonics, gas sensors, diagnostic technologies, catalysis, drug delivery systems and imaging. In particular, ZnO nanostructures have…

A comparative study of the physical properties of undoped Zinc Oxide (ZnO) and Al doped Zinc Oxide (AZO) thin films were performed as a function of annealing temperature. The structural properties were analyzed using X-ray diffraction and…

Applied Physics · Physics 2019-09-06 Joydip Sengupta , R. K. Sahoo , C. D. Mukherjee

Dependence of structural parameters on the size of nanoparticles is a topic of general interest where the effect of shape is often neglected. We report a comprehensive study on size dependent structural parameters of ZnO nanostructures (NS)…

Materials Science · Physics 2014-03-05 Manoranjan Ghosh , Debjani Karmakar , S. Basu , S. N. Jha , D. Bhattacharyya , S. C. Gadkari , S. K. Gupta

Thin films of magnesium doped zinc oxide (MZO) were synthesized using the sol gel method and annealed at different temperatures under ambient condition. The morphological properties of the post annealed MZO films were investigated using X…

Materials Science · Physics 2019-09-09 Joydip Sengupta , Arifeen Ahmed , Rini Labar

Structural rearrangement of polystyrene colloidal crystals under dry sintering conditions has been revealed by in situ grazing incidence X-ray scattering. Measured diffraction patterns were analysed using distorted wave Born approximation…

The interaction of high-energy electrons and X-ray photons with soft semiconductors such as halide perovskites is essential for the characterisation and understanding of these optoelectronic materials. Using nano-probe diffraction…

We present an original approach for predicting the static recrystallization texture development during annealing of deformed crystalline materials. The microstructure is considered as a population of subgrains and grains whose sizes and…

Materials Science · Physics 2021-02-22 Arthur Després , Jean-Denis Mithieux , Chad. W. Sinclair

Iron oxide nano particles with nominal Fe2O3 stoichiometry were synthesized by a wet, soft chemical method with the heat treatment temperatures from 250{\deg}C to 900{\deg}C in air. The variation in the structural properties of the nano…

Materials Science · Physics 2011-11-29 Debajeet K. Bora , Artur Braun , Selma Erat , Olga Safonova , Thomas Graule , Edwin C. Constable

The mechanism of the evolution of the deformed microstructure at the earliest stage of annealing where the existence of the lowest length scale substructure paves the way to the formation of the so-called subgrains, has been studied for the…

Materials Science · Physics 2010-07-02 P. S. Chowdhury , N. Gayathri , P. Mukherjee , M. Bhattacharya , A. Chatterjee , A. Dutta+ , P. Barat

The effect of Mg-substitution on the crystal structure of wurtzite ZnO is presented based on synchrotron X-ray diffraction studies of polycrystalline Zn1-xMgxO (0 <= x <= 0.15). Increase in Mg concentration results in pronounced c-axis…

Materials Science · Physics 2007-05-23 Young-Il Kim , Katharine Page , Ram Seshadri

Direct electron detectors in scanning transmission electron microscopy give unprecedented possibilities for structure analysis at the nanoscale. In electronic and quantum materials, this new capability gives access to, for example, emergent…

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