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Measurements of chain conformation in proteins/polyelectrolytes complexes (lysozyme and PSSNa) show that the crossover observed between an open structure -a chain network crosslinked by the proteins, and a globular one - dense globules of ~…

Soft Condensed Matter · Physics 2009-03-31 Jérémie Gummel , Fabrice Cousin , François Boué

We study by Small Angle Neutron Scattering (SANS) the structure of Hyaluronan -Lysozyme complexes. Hyaluronan (HA) is a polysaccharide of 9 nm intrinsic persistence length that bears one negative charge per disaccharide monomer (Mmol =…

Biological Physics · Physics 2012-10-04 François Boué , Eric Buhler , Fabrice Cousin , Isabelle Grillo , Isabelle Morfin

We present an extended structural study of globular complexes made by mixing a positively charge protein (lysozyme) and a negatively charged polyelectrolyte (PSS). We study the influence of all the parameters that may act on the structure…

Soft Condensed Matter · Physics 2010-07-26 Jérémie Gummel , François Boué , Daniel Clemens , Fabrice Cousin

We report on a SANS investigation into the potential for these structural reorganization of complexes composed of lysozyme and small PSS chains of opposite charge if the physicochemical conditions of the solutions are changed after their…

Soft Condensed Matter · Physics 2010-07-26 Fabrice Cousin , Jérémie Gummel , Daniel Clemens , Isabelle Grillo , François Boué

A quantitative understanding of aggregation mechanisms leading to the formation of inorganic nanoparticles (NPs) and protein composites in aqueous media is of paramount interest for colloid chemistry. In particular, the interactions between…

We have studied the structure of salt-free lysozyme at 293 K and pH 7.8 using molecular simulations and experimental SAXS effective potentials between proteins at three volume fractions, 0.012, 0.033, and 0.12. We found that the structure…

Soft Condensed Matter · Physics 2011-06-06 P. Kowalczyk , A. Ciach , P. A. Gauden , A. P. Terzyk

Interactions between actin, an anionic polyelectrolyte, and lysozyme, a cationic globular protein, have been examined using a combination of synchrotron small-angle x-ray scattering and molecular dynamics simulations. Lysozyme initially…

In this work the physicochemical characterization of liposomes loaded with a newly synthesised carboranyl porphyrazine (H2HECASPz) is described. This molecule represents a potential drug for different anticancer therapies, such as Boron…

The dynamics of lysozyme is probed by attaching -SCN to all alanine-residues. The 1-dimensional infrared spectra exhibit frequency shifts in the position of the maximum absorption by 4 cm$^{-1}$ which is consistent with experiments in…

Chemical Physics · Physics 2024-04-30 Sena Aydin , Seyedeh Maryam Salehi , Kai Töpfer , Markus Meuwly

The process of drying is a simple physical mechanism that drives a system to relax from one equilibrium point to another. The native states of the constituent particles in the droplets can be linked to the emergent morphological patterns…

Soft Condensed Matter · Physics 2021-05-14 Anusuya Pal , Amalesh Gope , Germano S. Iannacchione

Small angle neutron scattering intensity distributions taken from cytochrome C and lysozyme protein solutions show a rising intensity at very small wave vector, Q, which can be interpreted in terms of the presence of a weak long-range…

Soft Condensed Matter · Physics 2009-11-11 Yun Liu , Emiliano Fratini , Piero Baglioni , Wei-Ren Chen , Sow-Hsin Chen

Intrinsically Disordered Proteins (IDPs) perform a broad range of biological functions. Their relevance has motivated intense research activity seeking to characterize their sequence/structure/function relationships. However, the…

Assembly of protein complexes like virus shells, the centriole, the nuclear pore complex or the actin cytoskeleton is strongly determined by their spatial structure. Moreover it is becoming increasingly clear that the reversible nature of…

Subcellular Processes · Quantitative Biology 2014-05-13 Heinrich C. R. Klein , Ulrich S. Schwarz

The submicron- and micron-scale structures of composite hydrogels based on bacterial cellulose (BC) and polyacrylamide were studied by spin-echo small-angle neutron scattering (SESANS). These hydrogels were synthesized via free-radical…

Chemical Physics · Physics 2016-08-02 E. V. Velichko , A. L. Buyanov , Yu. O. Chetverikov , C. P. Duif , W. G. Bouwman , R. Yu. Smyslov

Measurements of liquid-liquid phase transition temperatures (cloud points) of mixtures of a protein (lysozyme) and a polymer, poly(ethylene glycol) (PEG) show that the addition of low molecular weight PEG stabilizes the mixture whereas high…

Soft Condensed Matter · Physics 2009-11-11 J. Bloustine , T. Virmani , G. M. Thurston , S. Fraden

Small angle neutron scattering (SANS) on the unilamellar vesicle populations (diameter 500 and 1000 angstrom) was used to characterize lipid vesicles from dimyristoylphosphatidylcholine (DMPC) at three phases (gel, ripple, and liquid).…

Biological Physics · Physics 2007-05-23 M. A. Kiselev , E. V. Zemlyanaya , V. K. Aswal , R. H. H. Neubert

The foaming properties, foaming capacity and foam stability, of soluble complexes of pectin and a globular protein, napin, have been investigated with a "Foamscan" apparatus. Complementary, we also used SANS with a recent method consisting…

Soft Condensed Matter · Physics 2010-05-11 Isabelle Schmidt , Bruno Null Novales , François Boué , Monique A. V. Axelos

In order to inquire the microscopic origin of observed multiple time scales in solvation dynamics we carry out several computer experiments. We perform atomistic molecular dynamics simulations on three protein-water systems namely,…

Soft Condensed Matter · Physics 2017-10-18 Sayantan Mondal , Saumyak Mukherjee , Biman Bagchi

Glutaraldehyde (GA) reacts with amino groups in proteins, forming intermolecular cross-links that, at sufficiently high protein concentration, can transform a protein solution into a gel. Although GA has been used as a cross-linking reagent…

Chemical Physics · Physics 2017-09-13 Shuji Kaieda , Tomás S. Plivelic , Bertil Halle

Fundamental knowledge of scattering in granular compacts is essential to ensure accuracy of spectroscopic measurements and determine material characteristics such as size and shape of scattering objects. Terahertz time-domain spectroscopy…

Optics · Physics 2023-04-24 Keir N Murphy , Mira Naftaly , Alison Nordon , Daniel Markl
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