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We present the first world-wide inter-laboratory comparison of small-angle X-ray scattering (SAXS) for nanoparticle sizing. The measurands in this comparison are the mean particle radius, the width of the size distribution and the particle…

Data Analysis, Statistics and Probability · Physics 2017-08-22 Brian R. Pauw , Claudia Kästner , Andreas F. Thünemann

Mechanical stress control is becoming one of the major challenges for the future of micro and nanotechnologies. Micro scanning X-ray diffraction is one of the promising techniques that allows stress characterization in such complex…

Materials Science · Physics 2025-01-22 P. Goudeau , N. Tamura , B. Lavelle , S. Rigo , T. Masri , A. Bosseboeuf , T. Sarnet , J. -A. Petit , J. -M. Desmarres

Glass forming liquids exhibit structural relaxation behaviors, reflecting underlying atomic rearrangements on a wide range of timescales. These behaviors play a crucial role in determining many material properties. However, the relaxation…

Complex fluids such as emulsions, colloidal gels, polymer or surfactant solutions are all characterized by the existence of a "microstructure" which may couple to an external flow on timescales that are easily probed in experiments. Such a…

Soft Condensed Matter · Physics 2015-02-11 Christophe Perge , Marc-Antoine Fardin , Sebastien Manneville

Many low-density nanoparticles show a radial inner structure. This work proposes a novel approach to contrast variation with SAXS based on the constitution of a solvent density gradient in a glass capillary in order to resolve this internal…

Soft Condensed Matter · Physics 2014-10-28 Raul Garcia-Diez , Christian Gollwitzer , Michael Krumrey

We report small angle X-ray scattering (SAXS) measurements of the skyrmion lattice in two 200~nm thick Cu$_2$OSeO$_3$ lamellae aligned with the applied magnetic field parallel to the out of plane [110] or [100] crystallographic directions.…

We investigate by scattering techniques the structure of water-based soft composite materials comprising a crystal made of Pluronic block-copolymer micelles arranged in a face-centered cubic lattice and a small amount (at most 2% by volume)…

Soft Condensed Matter · Physics 2012-06-07 Elisa Tamborini , Neda Ghofraniha , Julian Oberdisse , Luca Cipelletti , Laurence Ramos

Understanding and ultimately controlling the transformations and properties of nanoscale systems, from proteins to synthetic nanomaterial assemblies, is limited by the inability to uncover their dynamics on their characteristic length and…

The increased availability and brilliance of new X-ray facilities have in the recent years opened up the possibility to characterize the motion of dispersed nanoparticles in various microfluidic applications. One of these applications is…

Soft Condensed Matter · Physics 2018-04-24 Tomas Rosén , Christophe Brouzet , Stephan V. Roth , Fredrik Lundell , L. Daniel Söderberg

Flow-induced configuration dynamics and scission of rodlike micelles are studied for the first time using molecular dynamics simulations in presence of explicit solvent and salt. Predicted dependence of tumbling frequency and orientation…

Soft Condensed Matter · Physics 2015-05-20 Abhinanden Sambasivam , Ashish V. Sangwai , Radhakrishna Sureshkumar

Non-polar magnetic nanoparticles agglomerate upon cooling. This process is followed by in-situ small angle X-ray scattering to assess structural properties of the emerging agglomerates. On the length scale of a few particle diameters, no…

Soft Condensed Matter · Physics 2020-11-30 Christian Appel , Björn Kuttich , Tobias Kraus , Bernd Stühn

Microfluidic mixing is an important means for in-situ sample preparation and handling while Small Angle X-Ray Scattering (SAXS) is a proven tool for characterising (macro-)molecular structures. In combination those two techniques enable…

Small-angle X-ray scattering (SAXS) and X-ray diffraction (XRD) techniques are widely used as analytical tools in the optimization and control of nanomaterial synthesis processes. In crystalline nanoparticle systems with size distribution,…

The structure of the transient layer at the interface between air and the aqueous solution of silica nanoparticles with the size distribution of particles that has been determined from small-angle scattering has been studied by the X-ray…

Context. Scaling relations between cluster properties embody the formation and evolution of cosmic structure. Intrinsic scatters and correlations between X-ray properties are determined from merger history, baryonic processes, and dynamical…

Cosmology and Nongalactic Astrophysics · Physics 2019-12-04 Mauro Sereno , Stefano Ettori , Dominique Eckert , Paul Giles , Ben J. Maughan , Florian Pacaud , Marguerite Pierre , Patrick Valageas

The structure of silica-latex nanocomposites of three matrix chain masses (20, 50, and 160 kg/mol of poly(ethyl methacrylate)) are studied using a SAXS/TEM approach, coupled via Monte Carlo simulations of scattering of fully polydisperse…

Wide-angle x-ray scattering (WAXS) is emerging as a powerful tool for increasing the resolution of solution structure measurements of biomolecules. Compared to its better known complement, small angle x-ray scattering (SAXS), WAXS targets…

Offering high-brilliance X-ray beams on micrometer length scales, the microfocus-SAXS at SSRF BL16B1 was established with a KB mirror system for studying small sample volumes, or probing micro-scopic morphologies. The SAXS minimum q value…

Instrumentation and Detectors · Physics 2017-01-05 Wenqiang Hua , Yuzhu Wang , Ping Zhou , Tao Hu , Xiuhong Li , Fenggang Bian , Jie Wang