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The electronic structure of Cu hexafluoroacetylacetonate, crystallized with a stable nitronyl nitroxide radical [Ovcharenko et al., Russ. Chem. Bull. 53, 2406 (2004)], is calculated from first principles within the density functional theory…

Materials Science · Physics 2007-05-23 A. V. Postnikov , A. V. Galakhov , S. Bluegel

Two different silicate/water ice mixtures representing laboratory analogues of interstellar and circumstellar icy grains were produced in the laboratory. For the first time, optical constants, the real and imaginary parts of the complex…

Astrophysics of Galaxies · Physics 2018-07-25 Alexey Potapov , Harald Mutschke , Phillip Seeber , Thomas Henning , Cornelia Jäger

We present a fast method to fabricate high quality heterostructure devices by picking up crystals of arbitrary sizes. Bilayer graphene is encapsulated with hexagonal boron nitride to demonstrate this approach, showing good electronic…

Mesoscale and Nanoscale Physics · Physics 2015-06-18 P. J. Zomer , M. H. D. Guimarães , J. C. Brant , N. Tombros , B. J. van Wees

Hydrides are simple compounds containing one or a few hydrogen atoms bonded to a heavier atom. They are fundamental precursor molecules in cosmic chemistry and many hydride ions have become observable in high quality for the first time…

In-situ white light Laue diffraction has been successfully used to interrogate the structure of single crystal materials undergoing rapid (nanosecond) dynamic compression up to megabar pressures. However, information on strain state…

The erythrocyte sedimentation rate is one of the oldest medical diagnostic methods whose physical mechanisms remain debatable up to date. Using both light microscopy and mesoscale cell-level simulations, we show that erythrocytes form a…

The free standing solid polymer nanocomposite films has been prepared through standard solution cast technique. The improvement in structural, microstructural and electrochemical properties has been observed on the dispersion of nanofiller…

Materials Science · Physics 2018-07-16 Anil Arya , A. L. Sharma

Water-free NH4V3O8 microcrystals have been successfully synthesized by a microwave-assisted hydrothermal method. The products were characterized by means of X-ray diffraction, scanning electron microscopy, Fourier transform infrared…

Materials Science · Physics 2016-09-21 G. S. Zakharova , A. Ottmann , B. Ehrstein , R. Klingeler

Gas hydrates are systems of prime importance. In particular, hydrogen hydrates are potential materials of icy satellites and comets, and may be used for hydrogen storage. We explore the H2O-H2 system at pressures in the range 0-100 GPa with…

Materials Science · Physics 2014-04-01 Guang-Rui Qian , Andriy O. Lyakhov , Qiang Zhu , Artem R. Oganov , Xiao Dong

In this work we investigate the effects of the environment on the X-ray photoelectron spectra of hydrogen chloride and the chloride ions adsorbed on ice surfaces, as well as of chloride ions in water droplets. In our approach, we combine a…

Chemical Physics · Physics 2023-09-18 Richard A. Opoku , Céline Toubin , André Severo Pereira Gomes

An approach combining the Rietveld method and pairs distribution function analysis was developed and can help to understand the effect of temperature and/or high-pressure on crystalline materials. It was applied to orthorhombic Ta2O5…

Materials Science · Physics 2018-02-14 J. C. de Lima , Z. V. Borges , C. M. Poffo , S. M. Souza , D. M. Trichês , R. S. de Biasi

Fully exploiting the properties of 2D crystals requires a mass production method able to produce heterostructures of arbitrary complexity on any substrate, including plastic. Solution processing of graphene allows simple and low-cost…

Ultrafast lattice deformation of tens to hundreds of nanometer thick metallic crystals, after femtosecond laser excitation, was measured directly using 8.04 keV subpicosecond x-ray and 59 keV femtosecond electron pulses. Coherent phonons…

Materials Science · Physics 2018-03-09 Runze Li , Kyle Sundqvist , Jie Chen , H. E. Elsayed-Ali , Peter M. Rentzepis

Polycrystalline samples of Z-type hexaferrites, having nominal compositions $\mathrm{Ba_3Co_{2+x}Fe_{24-2x}M_xO_{41}}$ where M = $\mathrm{Ir^{4+}, Hf^{4+}, Mo^{4+}}$ and x=0 and 0.05, were processed via ceramic processing protocols in…

We describe an experimental platform that generates infrared images of micrometer-sized samples in the high pressure region of a diamond anvil cell. Using a 2.3 micron laser as a source of radiation, the system will be particularly useful…

Superconductivity · Physics 2021-11-24 Tarun Patel , A. Drozdov , V. S. Minkov , M. I. Eremets , E. J. Nicol , J. P. Carbotte , T. Timusk , A. W. Tsen

A new method for identifying crystalline phases in X-ray diffraction data has been proposed, which is especially useful for the study of multiphase materials (more than eight - ten phases) with a relatively low content (less than 1 - 3…

Materials Science · Physics 2021-08-17 A. D. Skorbun , S. V. Gabielkov , I. V. Zhyganiuk

This paper presents a simple and effective wideband method for the determination of material properties, such as the complex index of refraction and the complex permittivity and permeability. The method is explicit (non-iterative) and…

Instrumentation and Detectors · Physics 2010-12-02 Khattiya Chalapat , Kari Sarvala , Jian Li , G. S. Paraoanu

We have prepared powder samples of NaxCoO2 x yH2O using a new synthesis route. Superconductivity was observed in Na0.3CoO2 x 1.3H2O between 4 and 5K as indicated by the magnetic susceptibility. The bulk compressibilities of Na0.3CoO2 x…

Superconductivity · Physics 2009-11-10 Sangmoon Park , Yongjae Lee , Arnie Moodenbaugh , Thomas Vogt

In the present study, structural changes due to gradual doping of Sr in BaTiO3 were investigated by both x-ray and neutron powder diffraction techniques. Ba1-xSrxTiO3 (x=0.0, 0.5 and 1.0) samples were synthesized by PVA evaporation method…

Materials Science · Physics 2020-07-03 I. B. Elius , B. M. Asif , J. Maudood , T. K. Datta , A. K. M. Zakaria , S. Hossain , M. S. Aktar , I. Kamal

We present a first experiment combining high pression and coherent X-ray diffraction. By using a dedicated diamond anvil cell, we show that the degree of coherence of the X-ray beam is preserved when the X-ray beam passes through the…

Other Condensed Matter · Physics 2015-05-14 D. Le Bolloc'h , J. P. Itié , A. Polian , S. Ravy