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Powdered and sintered MgB2 samples have been characterized through magnetic measurements performed from T = 5 K up to few degrees above the transition temperature of about 39 K. We found that the sintered samples behave as well-connected…

Superconductivity · Physics 2009-11-07 M. R. Cimberle , M. Novak , P. Manfrinetti , A. Palenzona

High-pressure (HP) synthesis and sintering are promising methods for manufacturing of the bulk MgB2 superconductive material. The available high-pressure apparatuses with 100 cm3 working volume can allow us to use the bulk MgB2 for…

We have investigated the microstructure, normal-state electrical connectivity, and critical current density of ex-situ MgB2 polycrystalline bulks prepared by systematically varying the sintering conditions under low pressure. Samples heated…

Superconductivity · Physics 2015-06-11 Hiroya Tanaka , Akiyasu Yamamoto , Jun-ichi Shimoyama , Hiraku Ogino , Kohji Kishio

Improving the critical temperature (TC), critical magnetic field (HC), and critical current (JC) of superconducting materials has always been one of the most significant challenges in the field of superconductivity, but progress has been…

Superconductivity · Physics 2023-08-23 Yao Qi , Duo Chen , Yongbo Li , Chao Sun , Qingyu Hai , Miao Shi , Honggang Chen , Xiaopeng Zhao

The effect of high magnetic fields on the current carrying properties of both MgB2 bulks and Fe-sheathed tapes was investigated following different thermal sequences. It is found that application of a large magnetic field during processing…

Superconductivity · Physics 2009-11-11 Yanwei Ma , Aixia Xu , Xianping Zhang , Xiaohang Li , S. Awaji , K. Watanabe

MgB2/Fe tapes with 2.5-15 at.% ZrB2 additions were prepared through the in situ powder-in-tube method. Compared to the pure tape, a significant improvement in the in-field critical current density Jc was observed, most notably for 10 at.%…

Superconductivity · Physics 2009-11-11 Xianping Zhang , Zhaoshun Gao , Dongliang Wang , Zhengguang Yu , Yanwei Ma , S. Awaji , K. Watanabe

Bulk samples of MgB2 were prepared with 5, 10, and 15% wt.% Y2O3 nanoparticles added using a simple solid-state reaction route. Transmission electron microscopy (TEM) showed a fine nanostructure consisting of ~3-5 nm YB4 nanoparticles…

A novel method to prepare bulk Fe(Se0.5Te0.5) samples is presented, based on a melting process and a subsequent annealing treatment. With respect to the standard sintering technique, it produces much more homogeneous and denser samples,…

A new route to the sintering of MgB2 has been identified, based on a reactive infiltration of liquid Mg on a powdered B preform. The technique allows to obtain large bulk manufacts in an inexpensive way, without the need of high pressure…

Superconductivity · Physics 2009-11-07 Giovanni Giunchi

In the present investigation, we report a systematic study of Ag admixing in MgB2 prepared by solid-state reaction at ambient pressure. All the samples in the present investigation have been subjected to structural/ microstructural…

Superconductivity · Physics 2007-05-23 Chandra Shekhar , Rajiv Giri , R. S. Tiwari , S. K. Malik , O. N. Srivastava

The MgB2 - based material high-pressure synthesized at 2 GPa and 800 C for 1 h from Mg and B (taken in the stoichiometry ratio of MgB2) with addition of 2-10 wt% of Ti demonstrated the critical current density (jc) higher than 100 kA/cm^2…

We report the effect of the sintering temperature on the superconductivity of MgB2 pellets prepared under a high pressure of 3 GPa. The superconducting properties of the non-heated MgB2 in this high pressure were poor. However, as the…

Superconductivity · Physics 2009-11-07 C. U. Jung , Min-Seok Park , W. N. Kang , Mun-Seog Kim , Kijoon H. P. Kim , S. Y. Lee , Sung-Ik Lee

Bulk MgB2 samples were prepared under different synthesis conditions and analyzed by scanning and transmission electron microscopy. The critical current densities were determined from the magnetization versus magnetic field curves of bulk…

Materials Science · Physics 2018-07-04 A. Serquis , X. Z. Liao , L. Civale , Y. T. Zhu , J. Y. Coulter , D. E. Peterson , F. M. Mueller

Bulk MgB2 - based materials with the following critical current densities (jc) in 1 T field: 570 kA/cm^2 at 10 K, 350 kA/cm^2 at 20 K and 40 kA/cm^2 at 30 K and in 10 T field: 650 A/cm^2 at 10 K have been high-pressure (HP) synthesized from…

Two sets of MgB2 samples doped with up to 5 at. % of Al were prepared in different laboratories using different procedures. Decreases in the a and c lattice parameters were observed with Al doping confirming Al substitution onto the Mg…

The MgB2 superconductor synthesized in a flowing argon atmosphere using nanometer magnesium powder as the raw materials, denoted as Nano-MgB2, has been studied by the technique of in-situ high temperature resistance measurement (HT-RT…

Superconductivity · Physics 2009-11-10 Chinping Chen , Zeng-jun Zhou , Xing-guo Li , Jun Xu , Yu-hao Wang , Yong-zhong Wang , Qing-rong Feng

We report on the results of a comparative investigation of highly dense bulk MgB$_2$ samples prepared by three methods: (i) hot deformation; (ii) high pressure sintering; and (iii) mechanical alloying of Mg and B powders with subsequent hot…

The influence of the initial MgB2 grain size on critical current density, upper critical fields and irreversibility has been studied on Fe sheathed monofilamentary MgB2 tapes prepared by the Powder-In-Tube technique. The effect of the…

Superconductivity · Physics 2007-05-23 C. Beneduce , H. L. Suo , P. Toulemonde , N. Musolino , R. Flukiger

The powder in tube method has been used to fabricate Ag and Cu clad MgB2 wires using an in-situ reaction method. The effects of short time sintering on the critical current densities of Ag and Cu clad MgB2 wires were studied. All the…

Superconductivity · Physics 2009-11-07 S. Soltanian , X. L. Wang , J. Horvat , A. H. Li , H. K. Liu , S. X. Dou

We have successfully prepared the MgB2 superconducting bulk and powdered materials by the method of combustion synthesis. The starting materials used in this study were powders of Mg and B. X-ray powder diffraction pattern was well assigned…

Superconductivity · Physics 2016-08-31 Yoshihiko Takano , Nobutaka Oguro , Yoshinari Kaieda , Kazumasa Togano
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