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We present a Coherent X-ray Diffraction study of the antiferrodistortive displacive transition of SrTiO$_3$, a prototypical example of a phase transition for which the critical fluctuations exhibit two length scales and two time scales.…

Materials Science · Physics 2015-06-25 S. Ravy , D. Le Bolloc'h , R. Currat , A. Fluerasu , C. Mocuta , B. Dkhil

In the Bi cuprates, the presence of a near 1$\times$5 superstructure is well known. Usually, this superstructure is suppressed by the substitution of lead, but there have been reports of a phase separation in so called {\alpha} and {\beta}…

Superconductivity · Physics 2016-03-25 O. Lübben , L. Dudy , A. Krapf , C. Janowitz , R. Manzke

We report a structural phase transition found at Ts = 200 K in a pyrochlore oxide Cd2Re2O7 which shows superconductivity at Tc = 1.0 K. X-ray diffractionexperiments indicate that the phase transition is of the second order, from a…

Superconductivity · Physics 2009-11-07 M. Hanawa , J. Yamaura , Y. Muraoka , F. Sakai , Z. Hiroi

We report here on physical properties and lattice distortion in the new quasi-one-dimensional spin system TiOBr by x-ray diffraction experiment using synchrotoron radiation. Comparing the crystal structure between TiOBr and TiOCl, the…

Strongly Correlated Electrons · Physics 2007-05-23 Tomoyuki Sasaki , Masaichiro Mizumaki , Kenichi Kato , Yasuo Watabe , Yoshiki Nishihata , Masaki Takata , Jun Akimitsu

The nonstoichiometric NaxCoO2 system exhibits extraordinary physical properties that correlate with temperature and Na concentration in its layered lattice without evident long-range structure modification when conventional crystallographic…

Strongly Correlated Electrons · Physics 2009-11-10 H. X. Yang , C. J. Nie , Y. G. Shi , H. C. Yu , S. Ding , Y. L. Liu , D. Wu , N. L. Wang , J. Q. Li

We present the single-crystalline x-ray diffraction study on the Ba4Ru3O10 consisting of the corner-shared Ru3O12 trimers. The crystal structure is re-determined from 78 to 300 K across an antiferromagnetic transition at 105 K. The…

Strongly Correlated Electrons · Physics 2013-10-18 Taichi Igarashi , Yoshio Nogami , Yannick Klein , Gwenaelle Rousse , Ryuji Okazaki , Hiroki Taniguchi , Yukio Yasui , Ichiro Terasaki

The investigation of the penetration depth \lambda_{ab}(T,p) in YBa_2Cu_3O_{7-x} crystals allowed to observe the following features of the superfluid density n_s(T,p)\propto \lambda_{ab}^{-2}(T,p) as a function of temperature T<Tc/2 and…

Superconductivity · Physics 2007-05-23 M. R. Trunin , Yu. A. Nefyodov , A. F. Shevchun

The cubic symmetry of pyrochlore iridium oxides R2Ir2O7 (R = Nd, Eu, and Pr) has been investigated by high resolution X-ray diffraction experiments down to 4 K,in order to clarify the relationship between the metal-insulator transition…

Strongly Correlated Electrons · Physics 2014-12-12 Hiroshi Takatsu , Kunihiko Watanabe , Kazuki Goto , Hiroaki Kadowaki

In a previous article (Beanland & Sjokvist, 2024), we derived Boolean conditions for the appearance of superstructure reflexions in diffraction patterns from perovskites with tilted oxygen octahedra, using the structure factor equation.…

Materials Science · Physics 2025-01-28 Richard Beanland , Robin Sjokvist

We demonstrate that powder diffraction data can be collected from sub-micron crystals of a mbrane protein with nearly two orders of magnitude more atoms than the molecules commonly used for powder diffraction. The crystals of photosystem-1…

The diffraction peaks of Zircaloy-2 and Zr-2.5%Nb alloys at various deformations are found to be asymmetric in nature. In order to characterize the microstructure from these asymmetric peaks of these deformed alloys, X-Ray Diffraction Line…

Materials Science · Physics 2007-05-23 A. Sarkar , P. Mukherjee , P. Barat

We have performed a single crystal neutron scattering experiment on Ce0.7La0.3B6 to investigate the order parameter of phase IV microscopically. Below the phase transition temperature 1.5 K of phase IV, weak but distinct superlattice…

Strongly Correlated Electrons · Physics 2009-11-13 K. Kuwahara , K. Iwasa , M. Kohgi , N. Aso , M. Sera , F. Iga

The pyrochlore oxide Pb2Re2O7-{\delta} (PRO) is a candidate spin-orbit-coupled metal (SOCM) that exhibits a structural phase transition with inversion symmetry breaking. In this study, we report the results of detailed X-ray diffraction…

A scan of the superconductor -- nonsuperconductor transformation in single crystals YBa_2Cu_3O_{6+x} (x about 0.37) was done in two alternative ways, namely, by applying the magnetic field and by reducing the hole concentration through the…

Superconductivity · Physics 2008-02-03 V. F. Gantmakher , L. P. Kozeeva , A. N. Lavrov , D. A. Pushin , D. V. Shovkun , G. E. Tsydynzhapov , .

Quantitative phase analysis is one of the major applications of X-ray powder diffraction. The essential principle of quantitative phase analysis is that the diffraction intensity of a component phase in a mixture is proportional to its…

Materials Science · Physics 2022-02-22 Hui Lia , Meng Hebcd , Ze Zhange

We performed femtosecond reflection spectroscopy on a series of perovskite-type cobalt oxide $R$BaCo$_2$O$_{6-\delta}$ ($R$=Sm, Gd, and Tb) crystals, in which the electronic transfer was controlled by $R$. The transient reflectivity and the…

Strongly Correlated Electrons · Physics 2011-03-08 Y. Okimoto , T. Miyata , M. S. Endo , M. Kurashima , K. Onda , T. Ishikawa , S. Koshihara , M. Lorenc , E. Collet , H. Cailleau , T. Arima

D. J. Antonio et al. report an x-ray diffraction experiment on uranium dioxide at high-magnetic field and low temperature. The authors have apparently not realized that the diffraction data actually shows unambiguously the presence of a…

Materials Science · Physics 2021-04-14 G. H. Lander , R. Caciuffo

The oxygen-exchange behavior has been studied in half-doped manganese and cobalt perovskite oxides. We have found that the oxygen diffusivity in Gd_{0.5}Ba_{0.5}MnO_{3-\delta} can be enhanced by orders of magnitude by inducing…

Materials Science · Physics 2007-05-23 A. A. Taskin , A. N. Lavrov , Yoichi Ando

High resolution low angle x-ray data are reported for the gel phase of DPPC lipid bilayers, extending the previous q range of 1.0 {\AA}-1 to 1.3 {\AA}-1, and employing a new technique to obtain more accurate intensities and form factors…

Biological Physics · Physics 2019-03-27 John F Nagle , Pierre Cognet , Fernando G. Dupuy , Stephanie Tristram-Nagle

We present high-resolution capacitance dilatometry studies from 5 - 500 K of untwinned YBa2Cu3Ox (Y123) single crystals for x ~ 6.95 and x = 7.0. Large contributions to the thermal expansivities due to O-ordering are found for x ~ 6.95,…

Superconductivity · Physics 2009-10-31 Peter Nagel , Volker Pasler , Christoph Meingast , Alexandre I. Rykov , Setsuko Tajima