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The preparation of Ag 2+x Se thin films with thicknesses between 4 nm and 3000 nm by pulsed laser deposition on single crystalline NaCl and MgO substrates is reported. The films are perfectly dense and show a good lateral uniformity with a…

Other Condensed Matter · Physics 2007-11-22 B. Mogwitz , C. Korte , M. von Kreutzbruck , L. Kienle , J. Janek

We summarize our recent results that model the formation of uniform spherical silver colloids prepared by mixing iso-ascorbic acid and silver-amine complex solutions in the absence of dispersants. We found that the experimental results can…

Soft Condensed Matter · Physics 2010-09-22 Ionel Halaciuga , Daniel T. Robb , Vladimir Privman , Dan V. Goia

We present results of computational modeling of the formation of uniform spherical silver particles prepared by rapid mixing of ascorbic acid and silver-amine complex solutions in the absence of a dispersing agent. Using an accelerated…

Soft Condensed Matter · Physics 2010-10-12 Daniel T. Robb , Ionel Halaciuga , Vladimir Privman , Dan V. Goia

Vacuum heat treatment of mechanically-alloyed powders of boron and aluminum leads to formation of a metastable Al-rich phase, which can be quenched. Its structure, composition, and thermal stability are established. With chemical formula…

We have grown MgB2 films in a postannealing process. Precursors were prepared on Al2O3(0001) substrates by codeposition of Mg and MgB2 using pulsed laser deposition technique. Superconducting MgB2 thin films were obtained via an ex situ…

Superconductivity · Physics 2007-05-23 Yi Zhao , Yuemeng Chi , Ruijuan Nie , Furen Wang

High energy milling of MgB2 pre-reacted powder renders the material largely amorphous through extreme mechanical deformation and is suitable for mechanically alloying MgB2 with dopants including carbon. Bulk samples of milled C and MgB2…

Superconductivity · Physics 2009-11-10 B. J. Senkowicz , J. E. Giencke , S. Patnaik , C. B. Eom , E. E. Hellstrom , D. C. Larbalestier

In this paper we report a new synthesis route to produce boron powders characterized as being amorphous and having very fine particle size. This route has been developed to improve the performances of superconducting MgB2 powders, which can…

The MgB2 bulks were prepared by high energy milling of Mg and B powder. The correlations among milling times, microstructure and superconducting properties were investigated in MgB2 bulks. Samples were characterized by x-ray diffraction…

Superconductivity · Physics 2008-01-14 Y. F. Wu , Y. F. Lu , G. Yan , J. S. Li , Y. Feng , H. P. Tang , S. K. Chen , H. L. Xu , C. S. Li , P. X. Zhang

Dewetting of a binary alloy thin film is studied using a continuum many-parameter model that accounts for the surface and bulk diffusion, the bulk phase separation, the surface segregation and the particles formation. Analytical solution is…

Materials Science · Physics 2018-01-19 Mikhail Khenner

A c-axis oriented thin film and a high density sintered pellet of MgB2 have been studied by x-ray photoemission spectroscopy, and compared to measurements from MgO and MgF2 single crystals. The as-grown surface has a layer which is Mg-rich…

Superconductivity · Physics 2009-11-07 R. P. Vasquez , C. U. Jung , Min-Seok Park , Heon-Jung Kim , J. Y. Kim , Sung-Ik Lee

Precipitation of the \gamma' (AlAg2) phase was investigated in Al-Ag(-Cu) alloys using high resolution transmission electron microscopy and scanning transmission electron microscopy. Precipitation commenced with segregation of silver to…

Materials Science · Physics 2012-01-09 Julian M. Rosalie , Laure Bourgeois , Barrington C. Muddle

We introduce a simple method of an MgB2 film preparation using sequential electron-beam evaporation of B-Mg two-layer (followed by in-situ annealing) on the NbN buffered Si(100) substrate. The Transmission Electron Microscopy analyses…

In the present paper we report an in-situ high-energy X-ray diffraction analysis of MgB2 tapes during the preparation process. The experiment was performed in a specifically designed furnace working in reducing atmosphere, compatible with…

NbO2 is a potential material for nanometric memristor devices, both in the amorphous and the crystalline form. We fabricated NbO2 thin films using RF-magnetron sputtering from a stoichiometric target. The as-deposited films were amorphous…

Materials Science · Physics 2019-10-08 Ali Fakih , Johan Biscaras , Abhay Shukla

B and N K-edge x-ray absorption spectroscopy measurements have been performed on three BN thin films grown on Si substrates using ion-assisted pulsed laser deposition. Comparison of the films' spectra to those of several single-phase BN…

Condensed Matter · Physics 2007-05-23 A. Chaiken , L. J. Terminello , J. Wong , G. L. Doll , T. Sato

Superconducting thin films have been prepared in a two-step in-situ process, using the Mg-B plasma generated by pulsed laser ablation. The target was composed of a mixture of Mg and MgB2 powders to compensate for the volatility of Mg and…

Superconductivity · Physics 2009-11-07 D. H. A. Blank , H. Hilgenkamp , A. Brinkman , D. Mijatovic , G. Rijnders , H. Rogalla

We report on the results of a comparative investigation of highly dense bulk MgB$_2$ samples prepared by three methods: (i) hot deformation; (ii) high pressure sintering; and (iii) mechanical alloying of Mg and B powders with subsequent hot…

In this paper we report a new sol-gel method for the fabrication of MgB2 films. Polycrystalline MgB2 films were prepared by spin-coating a precursor solution of Mg(BH_4)_2 diethyl ether on (001)Al2O3 substrates followed with annealing in Mg…

Superconductivity · Physics 2015-05-27 Liping Chen , Chen Zhang , Yinbo Wang , Yue Wang , Qingrong Feng , Zizhao Gan , Junzhi Yang , Xingguo Li

Magnesium diboride bulk pellets were fabricated from pre-reacted MgB2 powder ball milled with different amounts of exposure to air. Evidence of increased electron scattering including increased resistivity, depressed Tc, and enhanced Hc2 of…

Superconducting MgB(2) films with Tc = 38.6 K were prepared using a precursor-deposition, ex-situ post-processing approach. Precursor films of boron, ~0.5 micrometer thick, were deposited onto Al(2)O(3) (102) substrates by e-beam…

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