Related papers: Crystal growth and characterization of MgB2: Relat…
Here we report the growth of sub-millimeter MgB2 single crystals of various shapes under high pressure in Mg-B-N system. Structure refinement using a single-crystal X-ray diffraction analysis gives lattice parameters a=3.0851(5) A and…
Single crystals of MgB2 have been grown at high pressure via the peritectic decomposition of MgNB9. The crystals are of a size up to 1.5x0.9x0.2 mm3 with a weight up to 0.23 mg, and typically have transition temperatures between 37 and 39…
Single crystals of MgB2 with a size up to 1.5x0.9x0.2 mm3 have been grown with a high pressure cubic anvil technique. The crystal growth process is very peculiar and involves an intermediate nitride, namely MgNB9. Single crystals of BN and…
Single crystals of MgB2 have been grown with a high-pressure cubic anvil technique. They grow via the peritectic decomposition of the MgNB9 ternary nitride. The crystals are of a size up to 2x1x0.1mm3 with a weight up to 230 micrograms.…
A new method for preparation of single crystals of the superconducting intermetallic MgB2 compound from a Mg-Cu-B melt flux is presented. The high vapour pressure of Mg at elevated temperature is a serious challenge of the preparation…
In-plane electrical transport properties of MgB2 single crystals grown under high pressure of 4-6 GPa and temperature of 1400-1700oC in Mg-B-N system have been measured. For all specimens we found sharp superconducting transition around…
Single crystals of Mg1-xAlxB2 have been grown at a pressure of 30 kbar using the cubic anvil technique. Precipitation free crystals with x < 0.1 were obtained as a result of optimization of already developed MgB2 crystal growth procedure.…
The review considers bulk MgB2-based materials in terms of their structure, superconducting and mechanical properties. Superconducting transition temperatures of 34.5-39.4 K, critical current densities of 1.8-1.0 x E6 A/sq.cm in self field…
We report the study of the polycrystalline MgB2 phase formation during the fabrication processes. Three major phases are identified in different sintering temperature ranges according to the corresponding superconducting properties and the…
Clarifying the impact of Fe doping on the structural and superconducting properties of MgB2 is crucial, considering that iron is commonly used as a sheath material for the fabrication of metal-clad MgB2 wires and tapes. To date the effects…
Single crystals of MgB2 and Mg(B1-xCx)2 have been grown using cubic anvil technique. Tc values vary in a wide range (39-9 K) with carbon content varying from 0 up to 16%. Using SiC as the precursor leads to C and not to Si substituted…
We have determined the structural properties of the superconducting compound MgB2 as a function of temperature from 11 K to 297 K and as a function of hydrostatic pressure up to 0.62 GPa using neutron powder diffraction. This compound, when…
We synthesized single crystalline and policrystalline MgB_2 under ambient pressures. The single crystals of MgB_2 were of good quality, where the crystal structure refinements were successfully converged with R = 0.020. The specific heat of…
Despite the intense activity in the year since the discovery of superconductivity in MgB2, key parameters, in particular the upper and lower critical fields Hc2 and Hc1 and their anisotropies, are not well-established, largely because of…
In this paper, we reported the structural properties and superconductivity of Mg(B1-xCx)2 compounds. Powder x-ray diffraction results indicate that the samples crystallize in a hexagonal AlB2-type structure. Due to the chemical activity of…
The effects of high-temperature vacuum-annealing induced Mg deficiency in MgB2 single crystals grown under high pressure were investigated. As the annealing temperature was increased from 800 to 975 C, the average Mg content in the MgB2…
Carbon-substituted MgB2 single crystals, Mg(B_1-xC_x)_2 of 0.3-1.0 mm size were grown for x=0.02-0.15 by a high-pressure technique. The doping dependence of lattice constants studied in a range of x=0.0-0.2 shows a monotonic decrease in a,…
The in-situ growth of superconducting MgB2 thin films was examined from various perspectives. The paper discusses (1) growth temperature, (2) the effect of excess Mg, (3) the effect of residual gas during growth, (4) the effect of in-situ…
The superconducting phase diagram of MgB2 was determined from magnetization, magneto-transport and the first single-crystal specific heat measurements. A zero-temperature in-plane coherence length of 8 nm is determined. The superconducting…
We report the preparation of Mg$_{1-x}$B$_{2}$ (0$\le$x$\le$0.5) compounds with the nominal compositions. Single phase MgB$_{2}$ was obtained for x=0 sample. For 0$<$x$\le$0.5, MgB$_{4}$ coexists with "MgB$_{2}$" and the amount of MgB$_{4}$…