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Kelvin probe microscopy (KPFM) is a well-established scanning probe technique, used to measure surface potential accurately; it has found extensive use in the study of a range of materials phenomena. In its conventional form, KPFM…

Kelvin probe force microscopy (KPFM) adapts an atomic force microscope to measure electric potential on surfaces at nanometer length scales. Here we demonstrate that Heterodyne-KPFM enables scan rates of several frames per minute in air,…

Mesoscale and Nanoscale Physics · Physics 2016-06-22 Joseph L. Garrett , Jeremy N. Munday

We compare the three most commonly used scanning probe techniques to obtain a reliable value of the work function in graphene domains of different thickness. The surface potential (SP) of graphene is directly measured in Hall bar geometry…

Mesoscale and Nanoscale Physics · Physics 2013-05-03 Vishal Panchal , Ruth Pearce , Rositza Yakimova , Alexander Tzalenchuk , Olga Kazakova

Moir\'e patterns arising from twisted van der Waals stacks fundamentally reshape their electronic properties, enabling band-structure engineering that has driven rapidly growing interest in this field. In studying electronic properties,…

Mesoscale and Nanoscale Physics · Physics 2025-11-12 Namkyung Lee , Hangyeol Park , Seungwon Jung , Baeksan Jang , Seonyu Lee , Joonho Jang

Optoelectronic phenomena in materials such as organic/inorganic hybrid perovskites depend on a complex interplay between light induced carrier generation and fast (electronic) and slower (ionic) processes, all of which are known to be…

Kelvin probe force microscopy (KPFM) is a powerful tool for studying contact electrification at the nanoscale, but converting KPFM voltage maps to charge density maps is non-trivial due to long-range forces and complex system geometry. Here…

Soft Condensed Matter · Physics 2022-11-30 Felix Pertl , Juan Carlos Sobarzo , Lubuna Shafeek , Tobias Cramer , Scott Waitukaitis

Kelvin probe force microscopy (KPFM) is a powerful tool for studying contact electrification, using an tiny tip to image voltages caused by transferred charge. It has been used in stationary studies focused on finding patterns (e.g.…

Soft Condensed Matter · Physics 2025-02-19 Felix Pertl , Isaac C. D. Lenton , Tobias Cramer , Scott Waitukaitis

We report a Kelvin probe force microscopy (KPFM) implementation using the dissipation signal of a frequency modulation atomic force microscopy that is capable of detecting the gradient of electrostatic force rather than electrostatic force.…

Mesoscale and Nanoscale Physics · Physics 2017-04-21 Yoichi Miyahara , Peter Grutter

In 2014, Charge Gradient Microscopy (CGM) was first reported as a new scanning probe imaging mode, particularly well-suited for the characterisation of ferroelectrics. The implementation of the technique is straightforward; it involves…

Reducing the dimensions of ferroelectric materials down to the nanoscale has strong implications on the ferroelectric polarization pattern and on the ability to switch the polarization. As the size of ferroelectric domains shrinks to…

High-quality spatially-resolved measurements of electric fields are critical to understanding charge injection, charge transport, and charge trapping in semiconducting materials. Here, we report a variation of frequency-modulated Kelvin…

Mesoscale and Nanoscale Physics · Physics 2017-10-30 Ryan P. Dwyer , Louisa M. Smieska , Ali Moeed Tirmzi , John A. Marohn

In 2D field effect transistors the gate electrostatically dopes the 2D semiconductor (2DSC) channel, tuning the Fermi level. In principle, Kelvin probe force microscopy (KPFM) can detect the Fermi level, and its dependence on gate bias as…

Fundamental mechanisms of energy storage, corrosion, sensing, and multiple biological functionalities are directly coupled to electrical processes and ionic dynamics at solid-liquid interfaces. In many cases, these processes are spatially…

Materials Science · Physics 2017-01-25 Liam Collins , Jason Kilpatrick , Sergei V. Kalinin , Brian J. Rodriguez

Correlative nanoscale surface characterization benefits from simultaneously measuring electronic and structural properties in the same environment, a capability that is essential for modern-day materials science and semiconductor failure…

Mesoscale and Nanoscale Physics · Physics 2026-05-18 Prabhu Prasad Swain , Nahid Hosseini , Eveline. S Mayner , Aleksandra Radenovic , Marcos Penedo , Georg E. Fantner

Devices made from two-dimensional (2D) materials such as graphene or transition metal dichalcogenides possess interesting electronic properties that can become accessible to experimental probes when the samples are protected from…

Mesoscale and Nanoscale Physics · Physics 2019-07-16 Michael A. Altvater , Tianhui Zhu , Guohong Li , Kenji Watanabe , Takashi Taniguchi , Eva Y. Andrei

We report experimental demonstration of the feasibility of reaching temperatures below 1 mK using cryogen-free technology. Our prototype system comprises an adiabatic nuclear demagnetisation stage, based on hyperfine-enhanced nuclear…

Instrumentation and Detectors · Physics 2015-06-16 Graham Batey , Andrew Casey , Michael Cuthbert , Anthony Matthews , John Saunders , Aya Shibahara

Graphene, a two-dimensional (2D) material with unique electronic properties, appears to be an ideal object for the application of surface-science methods. Among them, a family of scanning probe microscopy methods (STM, AFM, KPFM) and the…

Materials Science · Physics 2015-03-30 Yuriy Dedkov , Elena Voloshina , Mikhail Fonin

Local domain structures of ferroelectrics have been studied extensively using various modes of scanning probes at the nanoscale, including piezoresponse force microscopy (PFM) and Kelvin probe force microscopy (KPFM), though none of these…

Materials Science · Physics 2017-09-20 Ehsan Nasr Esfahani , Xiaoyan Liu , Jiangyu Li

We report the design and performance of a cryogen-free, pulse-tube refrigerator (PTR)-based scanning probe microscopy (SPM) system capable of operating at the base temperature of near 5K. We achieve this by combining a home-made interface…

Materials Science · Physics 2022-04-29 Jun Kasai , Tomoki Koyama , Munenori Yokota , Katsuya Iwaya

We report variation of the work function for single and bi-layer graphene devices measured by scanning Kelvin probe microscopy (SKPM). Using the electric field effect, the work function of graphene can be adjusted as the gate voltage tunes…

Mesoscale and Nanoscale Physics · Physics 2015-05-14 Young-Jun Yu , Yue Zhao , Sunmin Ryu , Louis E. Brus , Kwang S. Kim , Philip Kim
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