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An isolated calcium (Ca) atom has empty d-orbitals under ambient conditions. However, s-d band hybridization has been observed in both elemental Ca and compounds by manipulating thermodynamic conditions. Here, we reveal that the Ca 3d-band…

Materials Science · Physics 2025-10-24 Yang Lv , Junwei Li , Jianfu Li , Yong Liu , Jianan Yuan , 1 Jiani Lin , Saori Kawaguchi-Imada , Qingyang Hu , Xiaoli Wang

We report experimental and theoretical evidence that solid molecular ammonia becomes unstable at room temperature and high pressures and transforms into an ionic crystalline form. This material has been characterised in both hydrogenated…

Materials Science · Physics 2014-01-08 S. Ninet , F. Datchi , P. Dumas , M. Mezouar , G. Garbarino , A. Mafety , C. J. Pickard , R. J. Needs , A. M. Saitta

We report the pressure dependence of the structural parameters of the non-oxide perovskite superconductor MgCNi$_{3}$ up to 32 GPa using a diamond anvil cell and synchrotron x-rays at room temperature. The structure of the compound remains…

Crystallization from an amorphous atomic structure is usually seen as a spontaneous process in pursuit of a lower energy state, but for alloy systems it is often hard to elucidate because of the intrinsic structural and compositional…

Materials Science · Physics 2020-04-10 Y. Huang , L. Xie , D. S. He , J. Q. He

Alkali doped aromatic compounds have shown evidence of metallic and superconducting phases whose precise nature is still mysterious. In potassium and rubidium doped phenanthrene, superconducting temperatures around 5 K have been detected,…

Materials Science · Physics 2014-08-28 S. Shahab Naghavi , Erio Tosatti

Understanding high-pressure transitions in prototypical linear diatomic molecules, such as hydrogen, nitrogen, and oxygen, is an important objective in high-pressure physics. Recent ultrahigh-pressure study on hydrogen revealed that there…

Materials Science · Physics 2019-10-31 Shan Liu , Meifang Pu , Qiqi Tang , Feng Zhang , Binbin Wu , Li Lei

The behaviour of alkaline carbonates at high pressure is poorly understood. Indeed, theoretical and experimental investigations of general trends of pressure induced structural changes appear in the literature only sporadically. In this…

The vibrational and structural properties of a hydrogen-rich Group IVa hydride, Ge(CH$_3$)$_4$, are studied by combining Raman spectroscopy and synchrotron X-ray diffraction measurements at room temperature and at pressures up to 30.2 GPa.…

Superconductivity · Physics 2015-06-11 Zhen-Xing Qin , Chao Zhang , Ling-Yun Tang , Guo-Hua Zhong , Hai-Qing Lin , Xiao-Jia Chen

The orthorhombic crystal structure of the novel molecular-inorganic polymer $\mathrm{K_{2}SeO_{4}\cdot H_{2}SeO_{3}}$ was elucidated using single-crystal X-ray diffraction with MoK$\alpha$ radiation ($\lambda$= 0.71073 {\AA}), performed at…

The structural and vibrational properties of phenanthrene are measured at high pressures up to 30.2 GPa by Raman spectroscopy and synchrotron x-ray diffraction techniques. Two phase transitions are observed in raman spectra under pressures…

Through powder x-ray diffraction we have investigated the structural behavior of SmVO3, in which orbital and magnetic degrees of freedom are believed to be closely coupled to the crystal lattice. We have found, contrary to previous reports,…

A sequence of structural transitions occurring in the quasi-one-dimensional (1D) 3d1 system BaVS3 at low temperature was investigated by high resolution synchrotron X-ray diffraction. The orthorhombic Cmc21 structure of the…

Strongly Correlated Electrons · Physics 2009-11-10 S. Fagot , P. Foury-Leylekian , S. Ravy , J. P. Pouget , M. Anne , G. Popov , M. V. Lobanov , M. Greenblatt

There is renewed interest in the structure of the essential amino acid Phenylalanine in the solid state. Three new polymorphs were found in the years 2012 to 2014. Here, we investigate the structure, stability, and energetical ordering of…

Chemical Physics · Physics 2024-12-18 Thomas A. Niehaus , Emilien Prost , Vincent Loriot , Franck Lépine , Luc Bergé , Stefan Skupin

We report on the crystallographic structure of the layered compound Pb3Mn7O15. Previous analysis based on laboratory X-ray data at room temperature gave contradictory results in terms of the description of the unit cell. Motivated by recent…

Pressure-induced phase transitions of multiferroic BiFeO3 have been investigated using synchrotron radiation X-ray diffraction with diamond anvil cell technique at room temperature. Present experimental data clearly show that rhombohedral…

Materials Science · Physics 2013-08-30 Zhang XiaoLi , Wu Ye , Zhang Qian , Dong JunCai , Wu Xiang , Liu Jing , Wu ZiYu , Chen DongLiang

The behavior of identical particles interacting through the harmonic-repulsive pair potential has been studied in 3D using molecular dynamics simulations at a number of different densities. We found that at many densities, as the…

Soft Condensed Matter · Physics 2017-10-11 V. A. Levashov

We investigate the distorted face-centered-cubic (dfcc) phase of yttrium (Y) using a data-assimilation-based structure search that combines high-resolution powder x-ray diffraction (XRD) data with machine-learning interatomic potentials. By…

Materials Science · Physics 2026-05-28 Yuuki Kubo , Takahiro Ishikawa , Yuta Tanaka , Yuki Nakamoto , Masafumi Sakata , Shinji Tsuneyuki

We report on the development of all-fiber stand-alone Iodine-filled Photonic Microcells demonstrating record absorption contrast at room temperature. The microcell s fiber is made of inhibited coupling guiding hollow-core photonic crystal…

The palladium-iron-arsenides Ca10(Fe1-xPdxAs)10(Pd3As8) were synthesized by solid state methods and characterized by X-ray powder and single crystal diffraction. The triclinic crystal structure (space group P-1) is isotypic to the homologue…

Superconductivity · Physics 2014-10-29 C. Hieke , J. Lippmann , T. Stürzer , G. M. Friederichs , F. Nitsche , F. Winter , R. Pöttgen , D. Johrendt