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We are reporting a new synthetic strategy to grow large size black phosphorus (Black-P) crystals through a ternary clathrate Sn$_{24}$P$_{22-x}$I$_8$, under lower synthetic temperature and pressure. The Black-P crystals are found grown in…

The oscillating temperature technique was successfully employed to grow large and composition homogeneous CaFeAsF single crystals due to the reduction of nuclei number by temperature oscillation. The largest as-grown CaFeAsF single crystal…

Superconductivity · Physics 2022-03-02 Ming-Wei Ma , Binbin Ruan , Menghu Zhou , Yadong Gu , Qingsong Yang , Junnan Sun , Zhi-An Ren

Growth of two-dimensional van der Waals layered single-crystal (SC) films is highly desired to manifest intrinsic material sciences and unprecedented devices for industrial applications. While wafer-scale SC hexagonal boron nitride film has…

Inorganic-organic interfaces are important for enhancing the power conversion efficiency of silicon-based solar cells through singlet exciton fission (SF). We elucidated the structure of the first monolayers of tetracene (Tc), a SF…

Two single crystal phases of tantalum nitride were stabilized on c-plane sapphire using molecular beam epitaxy. The phases were identified to be $\delta$-TaN with a rocksalt cubic structure and $\gamma$-Ta$_2$N with a hexagonal structure.…

Here, we report successful single crystal growth of SnSb2Te4 using the self-flux method. Unidirectional crystal growth is confirmed through X Ray Diffraction (XRD) pattern taken on mechanically cleaved crystal flake while the rietveld…

Materials Science · Physics 2021-07-08 Ankush Saxena , M. M. Sharma , Prince Sharma , Yogesh Kumar , Poonam Rani , M. Singh , S. Patnaik , V. P. S. Awana

We report high quality single crystalline growth of SmBi using flux method. The compound crystallizes in the simple rock salt structure with space group Fm3m. The cubic structure of the single crystal was confirmed by Laue diffraction…

Measurements of the anisotropic properties of single crystals play a crucial role in probing the physics of new materials. Determining a growth protocol that yields suitable high-quality single crystals can be particularly challenging for…

Materials Science · Physics 2017-06-20 W. R. Meier , T. Kong , S. L. Bud'ko , P. C. Canfield

Single crystals of Zn_(1-x)Mn_xIn_2Se_4 were grown by the chemical vapour phase transport technique (CVT). The Mn concentration was varied from x=1 to x=0.01. Through X-rays powder diffraction patterns and Laue diagrams of single crystals…

Materials Science · Physics 2007-05-23 J. Mantilla , G. E. S. Brito , E. ter Haar , V. Sagredo , V. Bindilatti

High-quality and sizable single crystals are crucial for studying the intrinsic properties of unconventional superconductors, which are lacking in the 1111 phase of the Fe-based superconductors. Here we report the successful growth of…

Superconductivity · Physics 2015-07-03 Yonghui Ma , Hui Zhang , Bo Gao , Kangkang Hu , Qiucheng Ji , Gang Mu , Fuqiang Huang , Xiaoming Xie

We have successfully grown large and good-quality single crystals of the La$_{0.75}$Sr$_{0.25}$Cr$_{0.90}$O$_{3-\delta}$ compound using the floating-zone method with laser diodes. We investigated the crystal quality, crystallography,…

The bulk single crystals of $S = 1$ chain compound Ni(C$_3$H$_{10}$N$_2$)$_2$NO$_2$ClO$_4$ are grown by using a slow evaporation method at a constant temperature and a slow cooling method. It is found that the optimum condition of growing…

Strongly Correlated Electrons · Physics 2013-11-13 W. Tao , L. M. Chen , X. M. Wang , C. Fan , W. P. Ke , X. G. Liu , Z. Y. Zhao , Q. J. Li , X. F. Sun

Superconductivity was discovered in a Ni0:05TaS2 single crystal. A Ni0:05TaS2 single crystal was successfully grown via the NaCl/KCl flux method. The obtained lattice constant c of Ni0:05TaS2 is 1.1999 nm, which is significantly smaller…

Superconductivity · Physics 2015-05-13 X. D. Zhu , Y. P. Sun , S. B. Zhang , H. C. Lei , X. B. Zhu , Lijun Li , Z. R. Yang , W. H. Song , J. M. Dai

We report on the indigenous design and development of laboratory scale travelling heater method (THM) system to grow detector grade Cd0.9Zn0.1Te (CdZnTe) single crystals. THM system mainly consists of two-zone furnace with a tuneable…

Diamond thin films were growth using Tequila as precursor by Pulsed Liquid Injection Chemical Vapor Deposition (PLI-CVD) onto both silicon (100) and stainless steel 304 at 850 C. The diamond films were characterized by Scanning Electron…

Materials Science · Physics 2009-04-23 Javier Morales , Miguel Apátiga , Victor M. Castaño

This article reports the experimentally clarified crystal structure of a recently discovered sulfur hydride in high temperature superconducting phase which has the highest critical temperature Tc over 200 K which has been ever reported. For…

Millimeter-sized single crystals of LaFeAsO, LaFeAsO1-xFx, and LaFe1-xCoxAsO were grown in NaAs flux at ambient pressure. The detailed growth procedure and crystal characterizations are reported. The as-grown crystals have typical…

Well-separated mercury sulfide (HgS) nanocrystals are synthesized by a wet chemical route. Transmission electron microscopy studies show that nanocrystals are nearly spherical in shape with average size of 9 nm. Grazing angle X-ray…

Materials Science · Physics 2011-11-15 A. K. Mahapatra , A. K. Dash

MgO single crystals with diameters between 3.5 and 5 mm and lengths up to 40 mm were grown by the optical floating zone technique (OFZ). Despite challenging material properties such as the high melting point of 2825 {\deg}C, very high…

A layer of monodisperse circular steel disks in a nearly square horizontal cell forms, for shear amplitudes SA $\le$ 0.08, hexagonal close-packed crystallites that grow and merge until a single crystal fills the container. Increasing the…

Soft Condensed Matter · Physics 2024-11-07 Siyuan Su , Jie Zhang , Charles Radin , Harry L. Swinney