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Fast-cooling after sintering or annealing of BiFeO3-BaTiO3 mixed oxide ceramics yields core-shell structures that give excellent functional properties, but their precise phase assemblage and nanostructure remains an open question. By…

In a comprehensive study on several samples we demonstrate for our laboratory-based computed tomography system resolutions down to 150nm. The achieved resolution is validated by imaging com-mon test structures in 2D and Fourier Shell…

Instrumentation and Detectors · Physics 2021-02-15 Dominik Müller , Jonas Graetz , Andreas Balles , Simon Stier , Randolf Hanke , Christian Fella

Direct electron detectors in scanning transmission electron microscopy give unprecedented possibilities for structure analysis at the nanoscale. In electronic and quantum materials, this new capability gives access to, for example, emergent…

Materials design has traditionally evolved through trial-error approaches, mainly due to the non-local relationship between microstructures and properties such as strength and toughness. We propose 'alloy informatics' as a machine learning…

Materials Science · Physics 2025-04-08 Dario Massa , Efthimios Kaxiras , Stefanos Papanikolaou

Digital holographic microscopy is a powerful tool for characterizing transparent and reflective phase objects. Its ability to reconstruct amplitude and phase can also offer great insight into wavefront shaping and design of all-dielectric…

Microstructure characterisation has been greatly enhanced through the use of electron backscatter diffraction (EBSD), where rich maps are generated through analysis of the crystal phase and orientation in the scanning electron microscope…

Materials Science · Physics 2018-11-15 Vivian S Tong , Alexander J Knowles , David Dye , T Ben Britton

Precession electron diffraction has in the past few decades become a powerful technique for structure solving, strain analysis, and orientation mapping, to name a few. One of the benefits of precessing the electron beam, is increased…

Instrumentation and Detectors · Physics 2025-12-12 Gregory Nordahl , Lewys Jones , Emil Frang Christiansen , Kasper Aas Hunnestad , Magnus Nord

The nature of stacking faults - whether intrinsic or extrinsic - plays a pivotal role in defect-mediated processes in crystalline materials. Yet, current electron microscopy techniques for their reliable analysis remain limited to either…

Investigating metal organic systems with time-resolved photocrystallography poses a unique challenge while interpreting the time dependent photodifference maps. In these difference Fourier maps, the signals correspond to the movement of…

Data Analysis, Statistics and Probability · Physics 2020-10-13 J. J. Velazquez-Garcia , J. Wong , K. Basuroy , D. Storozhuk , S. Saouane , R. Henning , S. Techert

To leverage advancements in machine learning for metallic materials design and property prediction, it is crucial to develop a data-reduced representation of metal microstructures that surpasses the limitations of current physics-based…

Orientation determination does not necessarily require complete knowledge of the local atomic arrangement in a material. We present a method for microstructural phase discrimination and orientation analysis of phases for which there is only…

Materials Science · Physics 2019-06-06 Aimo Winkelmann , Grzegorz Cios , Tomasz Tokarski , Gert Nolze , Ralf Hielscher , Tomasz Kocieł

Incorporation of $\mathrm{Al_{y}Ga_{1-y}N}$ (AGN) semiconductors into high power electronics offers efficiency improvements in power transmission, generation, and use, if approaches to eliminate the defects arising from film-lattice…

We demonstrate a neutron tomography technique with sub-micrometer spatial resolution. Our method consists of measuring neutron diffraction spectra using a double crystal diffractometer as a function of sample rotation and then using a phase…

Instrumentation and Detectors · Physics 2020-11-13 B. Heacock , D. Sarenac , D. G. Cory , M. G. Huber , J. P. W. MacLean , H. Miao , H. Wen , D. A. Pushin

A popular method for designing digital models is transforming the transfer function of the corresponding analog models from continuous domain (s-domain) into discrete domain (z-domain) using the s-to-z transformation. The…

Systems and Control · Electrical Eng. & Systems 2025-09-15 Shen Chen , Jisong Wang , Dejun Liu , Jiaxi Ying , Shuai Wang

Scanning electron microscopy with polarization analysis is a powerful lab-based magnetic imaging technique offering parallel imaging of multiple magnetization components and a very high spatial resolution. However, one drawback of the…

Instrumentation and Detectors · Physics 2018-08-22 Daniel Schönke , Andreas Oelsner , Pascal Krautscheid , Robert M. Reeve , Mathias Kläui

We demonstrate an application of retardation-modulation polarimetry in studies of nanocomposite materials. Molecular ordering is explored on both nonchiral and chiral liquid crystals (LCs) in the bulk state and embedded into parallel-arrays…

Mesoscale and Nanoscale Physics · Physics 2019-04-24 Andriy V. Kityk , Patrick Huber , Anatoliy Andrushchak , Przemysław Kula , Wiktor Piecek

Aluminum nanocrystals offer a promising platform for plasmonic photocatalysis, yet a detailed understanding of their electron dynamics and consequent photocatalytic performance has been challenging thus far due to computational limitations.…

Mesoscale and Nanoscale Physics · Physics 2025-04-29 Nikhil S. Chellam , George C. Schatz

The direct detection and characterization of planetary and substellar companions at small angular separations is a rapidly advancing field. Dedicated high-contrast imaging instruments deliver unprecedented sensitivity, enabling detailed…

Earth and Planetary Astrophysics · Physics 2019-01-25 Tomas Stolker , Markus J. Bonse , Sascha P. Quanz , Adam Amara , Gabriele Cugno , Alexander J. Bohn , Anna Boehle

Nanoindentation is vital for probing mechanical properties, yet traditional grid-based workflows are inefficient for targeting specific microstructural features. We present an automated nanoindentation framework that integrates machine…

Instrumentation and Detectors · Physics 2025-04-28 Vivek Chawla , Dayakar Penumadu , Sergei Kalinin

Atom probe tomography (APT), electron probe microanalysis (EPMA) and nanoindentation were used to characterise the oxygen-rich layer on an in-service jet engine compressor disc, manufactured from the titanium alloy TIMETAL 834. Oxygen…