English
Related papers

Related papers: High-pressure hydrothermal growth and characteriza…

200 papers

We report the optimized conditions for growing the high quality single crystals of candidate quantum spin-ice Pr2Hf2O7 using the optical floating-zone method. Large single crystals of Pr2Hf2O7 have been grown under different growth…

Strongly Correlated Electrons · Physics 2019-01-02 V. K. Anand , A. T. M. N. Islam , A. Samartzis , J. Xu , N. Casati , B. Lake

Single crystals of the metallic Ruddlesden-Popper trilayer nickelates R$_4$Ni$_3$O$_{10}$ (R=La, Pr) were successfully grown using an optical-image floating zone furnace under oxygen pressure (pO$_2$) of 20 bar for La$_4$Ni$_3$O$_{10}$ and…

Materials Science · Physics 2020-08-19 Junjie Zhang , Hong Zheng , Yu-Sheng Chen , Yang Ren , Masao Yonemura , Ashfia Huq , J. F. Mitchell

SmCrO$_3$ single crystals were successfully grown utilizing the high-pressure optical floating-zone method and their crystal structure, magnetization behavior, and magnetic phase diagrams were thoroughly investigated. Magnetic studies were…

Strongly Correlated Electrons · Physics 2025-06-05 Ning Yuan , Erik Walendy , Nour Maraytta , Waldemar Hergett , Luca Bischof , Michael Merz , Rüdiger Klingeler

By using high pressure and high temperature (3.7 GPa, 1120 $^{\circ}$C) synthesis technique, we have grown (Cu,C)Ba$_2$Ca$_3$Cu$_4$O$_{11+\delta}$ single crystals. X-ray diffraction, scanning electron microscopy, resistivity and…

Superconductivity · Physics 2022-01-05 Chengping He , Xue Ming , Jin Si , Xiyu Zhu , Jinhua Wang , Hai-Hu Wen

Single crystals of a new twinned hexagonal perovskite compound Sr8Os6.3O24 have been synthesized, and structural and magnetic properties have been determined. The compound crystallizes in a hexagonal cell with lattice parameters a =…

We report on the first successful growth of single crystals of the noncentrosymmetric superconductor Mo$_3$Al$_2$C obtained by means of a cubic-anvil, high-pressure and high-temperature technique. Composition, structure, and normal-state…

Superconductivity · Physics 2018-06-27 N. D. Zhigadlo , D. Logvinovich , R. S. Gonnelli , V. A. Stepanov , D. Daghero

Single crystals of SrFe2-xPtxAs2 (0 < x < 0.36) were grown using the self flux solution method and characterized using x-ray crystallography, electrical transport, magnetic susceptibility, and specific heat measurements. The…

Superconductivity · Physics 2010-10-21 Kevin Kirshenbaum , Shanta R. Saha , Tyler Drye , Johnpierre Paglione

Single crystals of SmFeAsO1-xFy of a size up to 120 micrometers have been grown from NaCl/KCl flux at a pressure of 30 kbar and temperature of 1350-1450 C using the cubic anvil high-pressure technique. The superconducting transition…

Superconductivity · Physics 2009-11-13 N. D. Zhigadlo , S. Katrych , Z. Bukowski , S. Weyeneth , R. Puzniak , J. Karpinski

Single crystals of MgB2 with a size up to 1.5x0.9x0.2 mm3 have been grown with a high pressure cubic anvil technique. The crystal growth process is very peculiar and involves an intermediate nitride, namely MgNB9. Single crystals of BN and…

Single crystals of LaNiSb$_3$ were grown using the Sn flux method. Structural characterization confirms that LaNiSb$_3$ crystallizes in the orthorhombic $Pbcm$ space group with lattice parameters $a = 13.0970(2)\,\mathrm{\AA}$, $b =…

Materials Science · Physics 2026-03-24 Haribrahma Singh , Aarti Gautam , Prabuddha Kant Mishra , Rie Y. Umetsu , Ashok Kumar Ganguli

Superconducting Sm(O,F)BiS2 single crystals were successfully grown using KI-KCl flux. The obtained single crystals were flat-shaped and their size was 500um. The structure and composition of the obtained single crystals were obtained using…

A comprehensive bulk and surface investigation of high-quality In$_2$O$_3$(001) single crystals is reported. The transparent-yellow, cube-shaped single crystals were grown using the flux method. Inductively coupled plasma mass spectrometry…

An optically high-quality single crystal of sodium mesitylene sulfonate crystal was successfully grown by a slow evaporation method using methanol as solvent at room temperature. Single-crystal XRD has characterized the material and belongs…

Magneto-transport measurements of Pr$_4$Ni$_3$O$_{10}$ single crystals performed under externally applied pressures up to 73 GPa in diamond anvil cells with either KBr or Nujol oil as pressure media yield signatures of superconductivity…

The magnetization, crystal structure, and thermal expansion of a nearly stoichiometric Sr$_{1.04(3)}$Er$_{2.09(6)}$O$_{4.00(1)}$ single crystal have been studied by PPMS measurements and in-house and high-resolution synchrotron X-ray powder…

Strongly Correlated Electrons · Physics 2014-10-27 Hai-Feng Li , Andrew Wildes , Binyang Hou , Cong Zhang , Berthold Schmitz , Paul Meuffels , Georg Roth , Thomas Brückel

We report the synthesis, and structural and physical properties of CaFe4As3 single crystals. Needle-like single crystals of CaFe4As3 were grown out of Sn flux and the compound adopts an orthorhombic structure as determined by X-ray…

Superconductivity · Physics 2015-05-27 A. B. Karki , G. T. McCandless , S. Stadler , Y. M. Xiong , J. Li , Julia Y. Chan , R. Jin

Single crystals of the three-dimensional frustrated magnet and spin liquid candidate compound PbCuTe$_2$O$_6$ were grown using both the Travelling Solvent Floating Zone (TSFZ) and the Top-Seeded Solution Growth (TSSG) techniques. The growth…

Materials Science · Physics 2021-11-25 A. R. N. Hanna , A. T. M. N. Islam , R. Feyerherm , K. Siemensmeyer , K. Karmakar , S. Chillal , B. Lake

Single crystals of BaRh_2As_2 have been synthesized from a Pb flux. We present the room temperature crystal structure, single crystal x-ray diffraction measurements as a function of temperature T, anisotropic magnetic susceptibility \chi…

Superconductivity · Physics 2010-11-17 Yogesh Singh , Y. Lee , S. Nandi , A. Kreyssig , A Ellern , S. Das , R. Nath , B. N. Harmon , A. I. Goldman , D. C. Johnston

The superconducting and structural properties of elemental strontium metal were investigated under pressures up to 60 GPa while maintaining cryogenic conditions during pressure application. Applying pressure at low temperatures reveals…

Here we report successful growth of mm scale single crystals of stoichiometric FeSc2S4. Single crystal X-ray diffraction yields a cubic structure, spacegroup Fd-3m, with a=10.5097(2) angstroms at T=110(2) K consistent with previous…

Materials Science · Physics 2016-09-07 Jennifer R. Morey , Kemp W. Plumb , Chris M. Pasco , Tyrel M. McQueen , Seyed M. Koohpayeh